• Title/Summary/Keyword: rheological evaluation

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중질유 고도정제 부산물의 도로포장용 역청재료로서의 적용성 평가 (Evaluation of Applicability of Heavy Oil Upgrading By-Product (Pitch) as A Pavement Paving Material)

  • 양성린
    • 한국도로학회논문집
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    • 제16권5호
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    • pp.9-18
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    • 2014
  • PURPOSES : The objective of this study is to evaluate the applicability of the pitch, which is produced during SDA petroleum upgrading process, as a pavement paving material. In order for the purpose, the physical and chemical properties of the pitch are analyzed, and then the various plasticizers are applied in the pitch. METHODS : Two types of pitch are selected from oil refinery companies, which are owned the SDA petroleum upgrading process. Also, two types of asphalt binders, PG 64-22 and PG 58-22, are employed to compare with the pitch because these two types of asphalt binders are currently used as paving materials. For the chemical property of the pitch, the composition of SARA (Saturate, Aromatic, Resin, Asphaltene), the elementary composition, and the functional group are analyzed. For the physical property of the pitch, the basic material property tests, such as penetration test, softening point test, flash point test, ductility test, and rotational viscometer test, are performed. Also, the DSR (Dynamic Shear Rheometer) test and the BBR (Bending Beam Rheometer) test are conducted using asphalt binder specimens obtained by both short term aging (Rolling Thin Film Oven, RTFO) and long term aging (Pressure Aging Vessel, PAV) processes. The rheological property of each pitch type is evaluated as a function of temperatures and loading cycles. PG 64-22 asphalt binder is used as a control material. RESULTS AND CONCLUSIONS : The Pitch may not be suitable for the pavement paving material without modifications, but the pitch can be used as alternatives of modified addictive or asphalt. If low molecular component, such as saturate and aromatic components, are added in the pitch based on the development of various plasticizers, it has a strong possibility for the pitch to be used as a alternative. However, in order to verify the performance property of the pitch, further research is needed.

전립분 첨가시 빵생지의 물성 및 이스트의 가스발생력에 미치는 영향 (Effects of whole wheat flour on the Rheological Properties of dough gassing power of yeast)

  • 노삼현;이명렬
    • 한국조리학회지
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    • 제7권3호
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    • pp.179-191
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    • 2001
  • 밀가루전립분 혼입이 빵생지의 물성 및 yeast(S.cerevisiae)의 가스발생력에 미치는 영향을 검토한 실험은 밀전립분의 혼입비율 0, 25, 50, 75, 100%의 5군으로 구성 해 그 제빵성에 대해서 검토하였다. 1) 패리노그래프에 의해 흡수율을 측정한 결과 밀전립분은 빵용 밀가루에 비해 1.3배의 흡수율을 나타냈다. 2) Texture meter에 의한 dough 정도는 수분일정 생지의 경우는 혼입비율의 증가와 함께 딱딱하게 되고 응집성은 감소하였다. 흡수율에 의해 산출한 최적수분량은 조정한 경우의 dough의 점도 및 응집성은 제빵용 밀가루와 거의 같았다. 3) 밀전립분은 S.cerevisiae의 가스발생력에 좋은 영향을 주지 않고 수분일정생지의 경우 전체 가스 발생량 및 내포잔류 가스량과 혼입비율에서도 거의 비슷한 결과를 얻었다. 그리고 수분조정반죽의 경우는 밀전립분 혼입비율의 증가와 함께 전체 가스발생량 및 내포한 잔류 가스량의 증가가 확인되었다. 4) 빵의 품질평가의 결과 밀전립분을 25-50%혼입하여 수분 조정한 것이 가장 좋은 것으로 확인되었다.

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쑥 분말이 첨가된 식빵의 물성 및 관능성 (Rheological Properties and Sensory Characteristics of White Bread with Added Mugwort Powder)

  • 정인창
    • 동아시아식생활학회지
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    • 제16권3호
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    • pp.332-343
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    • 2006
  • This study was designed to investigate the possible utilization of mugwort as a source of functional ingredients. The approximate composition for mugwort powder was 5.06% moisture, 1.98% crude protein, 4.65% crude fat, 5.85% ash and 82.46% carbohydrate. The highest mineral content was potassium. The contents of total phenolic compounds and condensed tannin were 114 mg% and 11,000 mg%, respectively. The highest electron donating ability(EDA) was observed from the ethyl acetate and butanol fractions of mugwort powder but the lowest was shown by the hexane fraction. In color values, with increasing mugwort powder content, the 'lightness', 'redness' and 'yellowness' decreased in the crust, while in the crumb bread the 'lightness' decreased and the 'redness', and 'yellowness' increased. With the addition of mugwort powder as a substitute for strong flour over the range from 2.5% to 10.0%, the ratio of the volume and specific volume of white bread decreased while its weight increased. In the texture measurements for white breads, the hardness decreased slightly with the addition of 2.5% mugwort powder, but then increased with further additions of mugwort up to 10.0%. The addition of 2.5% mugwort powder increased the springiness and gumminess of white bread. The highest sensory scores for color, flavor, taste, texture and overall acceptance as evaluated by a student sensory panel were obtained from white bread with 2.5% mugwort powder and from the control. The highest sensory scores as evaluated by a baker sensory panel were obtained from white bread with 2.5% mugwort powder. In ranking test, overall acceptability of white bread was the highest in the control. Overall acceptance scores by sensory evaluation of white bread with 2.5% mugwort powder were not significantly different from those of control.

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Evaluation of Acid-treated Fish Sarcoplasmic Proteins on Physicochemical and Rheological Characteristics of Pork Myofibrillar Protein Gel Mediated by Microbial Transglutaminase

  • Hemung, Bung-Orn;Chin, Koo Bok
    • 한국축산식품학회지
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    • 제35권1호
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    • pp.50-57
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    • 2015
  • Fish sarcoplasmic protein (SP) is currently dumped as waste from surimi industry and its recovery by practical method for being the non-meat ingredient in meat industry would be a strategy to utilize effectively the fish resource. This study was aimed to apply pH treatment for fish SP recovery and evaluated its effect on pork myofibrillar protein (MP) gel. The pH values of fish SP were changed to 3 and 12, and neutralized to pH 7 before lyophilizing the precipitated protein after centrifugation. Acid-treated fish SP (AFSP) showed about 4-fold higher recovery yield than that of alkaline-treated SP and water absorption capacity was also about 1.2-fold greater. Because of the high recovery yield and water absorption capacity, AFSP was selected to incorporate into MP with/without microbial transglutaminase (MTG). The effects of AFSP and MTG on the physicochemical and rheological characteristics of MP and MP gel were evaluated. MTG induced an increase shear stress of the MP mixture and increase the breaking force of MP gels. MP gel lightness was decreased by adding AFSP. MP gel with MTG showed higher cooking loss than that without MTG. A reduction of cooking loss was observed when the AFSP was added along with MTG, where the insoluble particles were found. Therefore, AFSP could be contributed as a water holding agent in meat protein gel.

저지방 마요네즈의 물성과 관능적 특성 (Sensory and Physical Properties of Low-fat Mayonnaise Made with Starch-based Fat Replacers)

  • 천정아;송은승
    • 한국식품과학회지
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    • 제27권6호
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    • pp.839-844
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    • 1995
  • 맛, 조직감, 안정성 등에 영향을 미치지 않는 지방대체물질을 이용한 저열량, 저지방 마요네즈를 제조하기 위하여 4종류의 지방대체물질에 대한 점도를 측정하고, 지방대체물질의 식용유에 대한 유지대체비율을 달리하여 제조한 저지방 마요네즈에 대해 물성검사와 관능 검사를 시행하였다. 지방대체물질 paste는 모두 의가소성유체의 특성을 보였고, 의가소성과 항응복력은 Neutral DR(DR), N-Lite L(NL), Sta Slim 150(SS), Stellar 100X(SX)순으로 증가하였다. 지방대체물질이 첨가된 마요네즈의 경도와 부착성도 위와 같은 순으로 증가하였고, 지방대체물질의 첨가비율이 높은 마요네즈일수록 경도와 부착성이 낮았다. DR이 첨가된 마요네즈의 spreadability는 DR paste의 점조도지수를 잘 반영해준다. 지방대체물질의 이용은 마요네즈의 oily odor와 greasy aftertaste를 감소시켰다.

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Rheological Evaluation of Petroleum Jelly as a Base Material in Ointment and Cream Formulations : Linear Viscoelastic Behavior

  • Park, Eun-Kyoung;Song, Ki-Won
    • Journal of Pharmaceutical Investigation
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    • 제41권3호
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    • pp.161-171
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    • 2011
  • The objective of the present study is to systematically characterize a linear viscoelastic behavior of petroleum jelly in small amplitude oscillatory shear flow fields correspondent to the rheological ground state. With this aim, using a strain-controlled rheometer, the dynamic viscoelastic properties of commercially available petroleum jelly have been measured at $37^{\circ}C$ (body temperature) over a wide range of angular frequencies at an extremely small strain amplitude of 0.1 %. In this article, the linear viscoelastic behavior was reported in detail and then explained from a structural view-point of petroleum jelly and discussed in depth with respect to the consumer's requirements. Main findings obtained from this study can be summarized as follows : (1) The storage modulus is always greater than the loss modulus over an entire range of angular frequencies studied, meaning that the linear viscoelastic behavior of petroleum jelly is dominated by an elastic nature rather than a viscous nature. (2) Petroleum jelly shows a desirable linear viscoelastic behavior with respect to the consumer's requirements because it is undesirable for the product to flow down from the skin at an initial stage upon contact with the human skin. (3) A fractional derivative model shows an excellent applicability to describe a linear viscoelastic behavior of petroleum jelly. However, this model should be used with a special caution because there exists no physical meaning for the model parameters. (4) A modified form of the Cox-Merz rule gives a good ability to predict the relationship between steady shear flow properties (nonlinear behavior) and dynamic viscoelastic properties (linear behavior) for petroleum jelly.

초고층 압송계측을 통한 고성능 콘크리트의 유동특성과 압송성능과의 상관관계 (The Correlation between Rheological Properties and Pumpability of High Performance Concrete from High-Rise Pumping Monitoring)

  • 김규동;한천구
    • 한국건축시공학회지
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    • 제15권3호
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    • pp.291-297
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    • 2015
  • 본 연구에서는 초고층 구조물 시공에 사용되는 80MPa의 고성능 콘크리트를 대상으로 높이가 200m부터 350m인 지점까지 압송계측 결과를 근거로 하여 압송성능과 고성능 콘크리트의 유동특성과의 상관관계를 분석하였다. 굳지 않은 콘크리트의 물성과 초기강도 및 기준 재령에서의 압축강도 및 탄성계수는 모두 품질기준을 만족함이 확인되었다. 또한, 높이별 최대 압송압력은 약 10~15%씩 증가하였으며, 시간당 토출량은 최소 $25m^3$를 만족하는 것으로 나타났다. 또한, 압송압력과 마찰계수는 슬럼프 플로우의 크기에 반비례하는 것으로 나타났으며, 압송압력과 마찰계수는 T-500이 높을수록 증가하는 경향을 보였다.

우렁쉥이(멍게) 껍질로부터 정제된 섬유소 첨가 기능성 딸기잼의 품질평가 (Quality Evaluation of Strawberry Jams Prepared with Refined Dietary Fiber from Ascidian(Halocynthia roretzi) Tunic)

  • 변명우;육홍선;안현주;이경행;이현자
    • 한국식품과학회지
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    • 제32권5호
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    • pp.1068-1072
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    • 2000
  • 폐자원의 이용방안으로 우렁쉥이(멍게) 껍질로부터 정제한 섬유소를 첨가하여 일반적인 잼류보다 기능성을 강화한 딸기잼의 제품개발을 위해 우렁쉥이 껍질 섬유소를 각각 1% 및 2% 첨가한 기능성 딸기잼의 기계적 물성 측정 및 관능적 특성을 통하여 제품의 품질평가를 하였다. Back extrusion test에 의해 측정한 4가지 물성치인 견고성, 점조성, 응집성 및 점도는 섬유소 첨가량이 증가할수록 유의적으로 감소하였다. 잼의 점성은 섬유소의 첨가량이 증가할수록 점도가 감소하는 양상을 보여 섬유소의 첨가가 점도저하의 원인이 되었고, 조직감 측정에 의해 얻어진 점도의 수치와 일치하였다. 색도의 경우 섬유소의 첨가량이 증가 할수록 L 및 a값이 유의적으로 증가하여 섬유소를 첨가한 잼이 밝은 적색을 띄는 것을 알 수 있었다. 관능검사 결과 맛 및 전체적인 기호도에서 유의적인 차이를 나타냈으며, 1% 섬유소 첨가군이 높은 기호도를 나타내어 섬유소를 첨가한 딸기잼을 선호하는 것으로 나타났다.

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첨가재료에 따른 증편의 관능적.물성적 특성 (Sensory and Rheological Properties of Jeungpyun made with various Additives)

  • 최영희;전화숙;강미영
    • 한국식품조리과학회지
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    • 제12권2호
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    • pp.200-206
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    • 1996
  • 전통쌀가공식품인 증편의 영양성 및 기호성을 증진시킬 목적으로 콩가루, 전지분유, 탈지분유, 난황, 난백, 쑥가루 등을 첨가하여 증편을 제조하였으며 첨가 재료별 증편의 성형성 및 관능적, 물성적특성을 비교 하였다. 첨가재료를 달리한 증편의 일반성분을 분석한 결과 쑥가루를 제외한 모든구에서 단백질함량이 대조구에 비해 높았으며 콩가루, 전지분유 첨가구는 조지방의 함량이 높았다. 탈지 분유와 전지분유를 첨가한 증편의 loaf volume은 대조구에 비해 낮았으나, 난황, 난백, 쑥가루을 첨가 한 증편은 대조구와 유의적 차이를 보이지 않았다. 쑥 가루 및 난황첨가구는 기공이 균일하지 않았다. 첨가재료별 증편의 관능검사결과 콩가루, 전지분유, 탈지분유, 난백첨가구가 대조구보다 단맛의 정도가 강하고 씹힘성 및 단단한 정도가 낮았으며, 쑥가루첨 가구는 쓴맛이 강하게 느껴지고 단단하였다. Texturometer로 증편의 물성을 측정한 결과, 쑥가루 첨가구는 경도, 탄력성 및 씹힘성이 높아 단단하고 탄력있는 특징을 보였으며, 콩가루, 전지분유, 탈지분유 및 난백첨가구는 이러한 물성이 대체로 낮아 부드럽고 질기지 않는 물성을 나타내었고 이는 관능검사 결과와 유사하였다. 콩가루 및 전지분유첨가구를 4$^{\circ}C$에서 저장했을 때 경도의 변화가 대조구보다 낮아 증편의 노화를 지연시키는 효과가 있었다.

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Stochastic micro-vibration response characteristics of a sandwich plate with MR visco-elastomer core and mass

  • Ying, Z.G.;Ni, Y.Q.;Duan, Y.F.
    • Smart Structures and Systems
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    • 제16권1호
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    • pp.141-162
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    • 2015
  • The magneto-rheological visco-elastomer (MRVE) is used as a smart core to control the stochastic micro-vibration of a sandwich plate with supported mass. The micro-vibration response of the sandwich plate with MRVE core and supported mass under stochastic support motion excitations is studied and compared to evaluate the vibration suppression capability. The effects of the supported mass and localized magnetic field on the stochastic micro-vibration response of the MRVE sandwich plate are taken into account. The dynamic characteristics of the MRVE core in micro-vibration are described by a non-homogeneous complex modulus dependent on vibration frequency and controllable by applied magnetic fields. The partial differential equations for the coupled transverse and longitudinal motions of the MRVE sandwich plate with supported mass are derived from the dynamic equilibrium, constitutive and geometric relations. The simplified ordinary differential equations are obtained for the transverse vibration of the MRVE sandwich plate under localized magnetic fields. A frequency-domain solution method for the stochastic micro-vibration response of sandwich plates with supported mass is developed based on the Galerkin method and random vibration theory. The expressions of frequency-response functions, response power spectral densities and root-mean-square velocity responses of the plate in terms of the one-third octave frequency band are obtained for micro-vibration evaluation. Finally, numerical results are given to illustrate the large response reduction capacity of the MRVE sandwich plate with supported mass under stochastic support motion excitations, and the influences of MRVE parameters, supported mass and localized magnetic field placement on the micro-vibration response.