• Title/Summary/Keyword: resin ratio

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Synthesis of conducting and magnetic nanocomposite of cross-linked aniline sulfide resin

  • Hosseini, Seyed Hossein
    • Advances in materials Research
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    • v.3 no.4
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    • pp.233-242
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    • 2014
  • Magnetic and conducting aniline sulfide resin cross-linked (ASC-Fe3O4) nanocomposite has been prepared in the presence of aniline sulfide resin (ASR), aniline, $Fe_3O_4$ coated by polyethylene glycol (PEG) and initiator. The magnetic properties of the resulting composites showed ferromagnetic behavior, such as high-saturated magnetization (Ms= 41 emu/g), and coercive force (Hc=1.5 Oe). The saturated magnetization was increased by increasing of $Fe_3O_4$ content and decreased by increasing aniline ratio. The transmission electron micrograph (TEM) and X-ray diffraction proved that nanometer-sized about 20-30 nm $Fe_3O_4$ in the composite. The average size of ASC-$Fe_3O_4$ nanocomposite with core-shell structure was about 50-60 nm, and polydisperse. This approach may also be extended to the synthesis and modification of other polymers. Electrical conductivity of aniline sulfide resin cross-linked (ASC) nanocomposite has been studied by four-point probe method and produced $3.3{\times}10^{-4}S/cm$ conductivity for it. The conductivity of the composites at room temperature depended on the $Fe_3O_4$, aniline ratio and doping degree. The thermogravimetry analysis (TGA) results showed that this resin is thermal resistance near of $500^{\circ}C$. So, It can be used for resistance thermal coating for military applications. $Fe_3O_4$-PASC nanocomposite has been flexible structure with electrical and magnetic properties.

Study on the Effect of Resin Mixture Ratios on the Fatigue Crack Propagation Behavior and Mechanical Property in a FRMLs (수지 혼합비가 FRMLs의 피로균열전파거동과 기계적 성질에 미치는 영향에 관한 연구)

  • Kim, Cheol-Woong;Sohn, Se-Won
    • Journal of the Korean Society for Precision Engineering
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    • v.16 no.8
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    • pp.149-154
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    • 1999
  • FRMLs(Fiber Reinforced Metal Laminates) is a new type of hybrid materials. FRMLs consists of high strength metal and fiber which are laminated using a structural adhesive bond(epoxy resin). The effect of resin mixture ratios on the fatigue crack propagation behavior and mechanical property of Aramid fiber reinforced aluminum composites was investigated. The epoxy, diglycidylether of bisphenol A(DGEBA) was cured with methylene dianiline(MDA) with or without accelerator(K-54). Eight kinds of resin mixture ratio were tested for the experiment ; five kinds of FRMLs(1))epoxy & curing agent) and three kinds of FRMLs(2)(epoxy & curing agent & accelerator). FRMLs(2) have a more effective characteristics on the fatigue crack propagation behavior and mechanical property than FRMLs(1)

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Effect of Resin Impregnation Ratio on the Properties of Ceramics Made from Miscanthus sinensis var. purpurascens Particle Boards (수지함침율이 거대억새 파티클보드로 제조된 세라믹의 성질에 미치는 영향)

  • HWANG, Jung-Woo;PARK, Hee-Jun;OH, Seung-Won
    • Journal of the Korean Wood Science and Technology
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    • v.49 no.4
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    • pp.360-370
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    • 2021
  • For the purpose of finding new uses for Miscanthus sinensis var. purpurascens, this study first constructed boards with the particles of the plant and impregnated them with phenolic resin at resin impregnation rates of 30 ± 2%, 40 ± 2%, 50 ± 2%, and 60 ± 2%. The impregnated boards were then carbonized at the carbonization temperature of 800℃, after which their density and mechanical properties were examined according to the different resin impregnation rates. The results showed that density, flexural strength performance, Brinell hardness, and compressive strength increased as the resin impregnation rate increased, thus affecting the physical and mechanical properties of the ceramics made of M. sinensis var. purpurascens particles.

Pattern Formation by the watersoluble PSR ink (수성 PSR 잉크를 이용한 패턴 형성)

  • Lee, Myung-Su;Kim, Young-Bea;Nam, Su-Yong
    • Journal of the Korean Graphic Arts Communication Society
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    • v.22 no.1
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    • pp.83-94
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    • 2004
  • PSR ink is used to insulation coating material that heat resistance is. The use purpose is used for bridge prevention, circuit protection, stabilization of insulation. Heat-cured resin was used mainly on the materials of PSR inks. But, UV-curing type resin in used. Also, because of recently environmental problem, ink is going to water type. Purpose of this study is to develop PSR ink that can develop in pure water. and experiment did that do from that find suitable oligomer and monomer and does brand ratio differ. Specially Knew that is extent water soluble UV resin develop possible is DPHA 10~50% that A/A1924 is 50~90wt %, monomer. As a result, when ratio of A/A1924 and DPHA low viscosity epoxy resin is 5:1.5:1.5, could get high sensibility pattern repeatability, tack and alkali-resistance.

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Nondestructive Bending Strength Evaluation of Woodceramics Made from Woody Part of Broussonetia Kazinoki Sieb. - Effect of Resin Impregnation Ratio -

  • Byeon, Hee-Seop;Kim, Jae-Min;Won, Kyung-Rok;Oh, Seung-Won
    • Journal of the Korean Wood Science and Technology
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    • v.39 no.5
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    • pp.398-405
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    • 2011
  • Nondestructive evaluation (NDE) technique method using a resonance frequency mode was carried out for woodceramics made by different phenol resin impregnation ratios (40, 50, 60, 70%) for Broussonetia Kazinoki Sieb. Dynamic modulus of elasticity increased with increasing resin impregnation ratios. There was a close relationship between dynamic modulus of elasticity and static bending modulus of elasticity and between dynamic modulus of elasticity and MOR and between static bending modulus of elasticity and MOR. Therefore, the dynamic modulus of elasticity using resonance frequency mode is useful as a nondestructive evaluation method for predicting the MOR of woodceramics made by different impregnation ratios.

The Conduction Properties of Epoxy Resin Composition According to the Content Change of Spherical Hollow Type Silver (중공형 구형 은입자의 함량변화에 따른 에폭시 수지조성물의 전도특성 연구)

  • Kim, Whan Gun;Lim, Ryun Woo
    • Journal of the Semiconductor & Display Technology
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    • v.11 no.2
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    • pp.23-26
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    • 2012
  • The monodispersed polystyrene spheres were prepared by emulsion polymerization in aqueous alcohol system. They coated with silver by reduction of silver ion percolated on the surface of them. The spherical hollow type silver has been prepared by dissolving polystyrene with toluene. Epoxy resin compositions with spherical hollow type silver were manufactured, which were composed of a bisphenol F type epoxy resin (RE-304S), amine type hardener (Kayahard AA), and 1-benzyl 2-methyl imidazole (1B2MI) as catalyst. The electrical conductivity with silver content ratio were investigated after cure, the percolation threshold weight ratio for conductance in this epoxy resin system was obtained above the 70 wt% of silver.

The Manufacture of High-Density Woodceramic through the Secondary Carbonization

  • Oh, Seung Won
    • Journal of the Korean Wood Science and Technology
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    • v.41 no.2
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    • pp.105-110
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    • 2013
  • A repeated impregnation and carbonization process was performed to prepare high-density woodceramics using MDF. The physical properties were estimated to further confirm morphologically structurally occurred changes of one-time and two-time phenolic resin treated and carbonized woodceramics. As compare one-time and two-time carbonized woodceramics, the increasing rate of weight and density declined after second carbonization as the resin impregnation ratio grew higher, and when the resin impregnation ratio was 40 percent, the weight and density of the second carbonization increased more than in the first step by 20.5% and 33.9% respectively which were the highest rates.

The Effect of Thermal Decomposition of Epoxy Resin for a Variation of Hardener (에폭시수지의 경화제 변화량에 따르는 열분해 영향)

  • Park, Keun-Ho;Lee, Yong-Sook;Song, Ju-Yeong;Lee, Soo;Kim, Sung-Il
    • Journal of the Korean Applied Science and Technology
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    • v.24 no.4
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    • pp.393-398
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    • 2007
  • We investigated heat stability of epoxy resin products and epoxy resin according to the influence hardener. The heat flow which shows the degree of thermal decomposition of the epoxy resin product and epoxy resin measured by using the differential scanning calorimeter (DSC). As a result, we found that in the case of heat stability for epoxy resin as hardener was added, the ratio of one to one (epoxy resin : hardener) was the most suitable in air condition and nitrogen atmosphere.

The Effect on Mixed Ratio of Recycled Engineering plastic Resin on the Shrinkage in Molded Parts (엔지니어링 플라스틱 재료의 재활용 혼합비가 성형품 수축에 미치는 영향)

    • Resources Recycling
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    • v.13 no.3
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    • pp.43-49
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    • 2004
  • In this study. an experimental work was performed to mold tensile specimens by using the injection molding machine. Melt temperature, mold temperature and the mixed ratio of recycled resin were selected as processing parameters for studying the effect of those conditions on the shrinkage and weight of molded parts. As a result, the shrinkage was increased with the higher mold and melt temperature and it was more sensitive to the change of mold temperature. On the other hand, the weight of molded parts was decreased with the increment of mold and melt temperature.

Oil Absorptive Properties of Polypropylene Knit Fabric Treated with Oleophilic Acrylic Resin (친유성 아크릴 수지로 처리된 폴리프로필렌 편직물의 유흡착 성질)

  • Jeong, Hwa-Jin
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.17 no.2
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    • pp.528-535
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    • 2016
  • Two types of oleophilic acrylic prepolymers were prepared by the solution copolymerization of either ethyl acrylate (EA) or lauryl acrylate (LA) with hydroxy ethyl acrylate (HEA). For the formation of oil-absorbent materials, a mixed solution of the prepolymer and hexamethylene diisocyanate (HDI) as a cross-linker in toluene was applied to polypropylene knit velvet fabric through the conventional pad-dry-cure procedure. The gel fraction of the crosslinked resin, EA-HEA-HDI, increased with increasing feed ratio of HEA to total acrylate or HDI concentration. The oil absorbancy and retention ratio of the prepared materials were compared according to the add-on ratio of resin to fabric, and were assessed with n-decane, toluene, soybean oil, lubricant and bunker C oil as test oils. The optimal oil absorbancy of the materials were observed at around 6% of the add-on ratio for all these oils except for soybean oil. On the other hand, the oil retention ratio increased as the add-on ratio increased. Futhermore, heavier and more viscous oil generally showed higher oil retention ratios. In addition, the oil absorbancy of the materials treated with LA-HEA-HDI resin was higher than that treated with EA-HEA-HDI resin, which showed that the acrylic resins are more absorptive with increasing length of their side alkyl chain.