• Journal of Powder Materials
• /
• v.30 no.2
• /
• pp.140-145
• /
• 2023

Although the Ti-6Al-4V alloy has been used in the aircraft industry owing to its excellent mechanical properties and low density, the low formability of the alloy hinders broadening its applications. Recently, laser-powder bed fusion (L-PBF) has become a novel process for overcoming the limitations of the alloy (i.e., low formability), owing to the high degree of design freedom for the geometry of products having outstanding performance used in high-tech applications. In this study, to investigate the effect of bulk shape on the microstructure and mechanical properties of L-PBFed Ti-6Al-4V alloys, two types of samples are fabricated using L-PBF: thick and thin samples. The thick sample exhibits lower strength and higher ductility than the thin sample owing to the larger grain size and lower residual dislocation density of the thick sample because of the heat input during the L-PBF process.

• Journal of Powder Materials
• /
• v.8 no.2
• /
• pp.117-123
• /
• 2001

Formation of pores in melt-processed $YBa_2Cu_3O_{7-x}$ (123) oxides and its effect on the microstructure were studied. Spherical pores with a size of a few tens of microns were formed due to the evolution of oxygen gas during melting of a 123 oxide. Some of pores were converted into liquid pockets by liquid filling, but others remained unfilled. The liquid pockets were converted into spherical 123 regions with a lower $Y_2BaCuO_5$ (211)density through the peritectic reaction during subsequent cooling, while the pores were entrapped into the periteictically grown 123 grains. The spherical 123 regions often consists of a residual melt due to the unbalanced peritectically reaction.

• Journal of Powder Materials
• /
• v.4 no.1
• /
• pp.9-17
• /
• 1997

The mullite-zirconia composites were prepared by the pressureless sintering with addition of 10~20 vol% ZrO$_2$(TZ3Y) in the fused mullite and sol-gel mullite matrix. The densification rate of sol-gel mullite was higher than that of fused mullite, and the addition of ZrO$_2$(TZ3Y) was effective on the densification of fused mullite. The enhancement of densification and anisotropic growth of mullite in ZrO$_2$added specimen can be explained by the solid solution effect of $Zr^{+4}$ ion in mullite. Both mechanical strength and fracture toughness of mullite-zirconia composite were enhanced compared to those of mullite. The enhancement of mechanical properties is attributed to the hinderance of grain growth and the combined toughening effects of tetra-mono phase transformation and crack deflection due to the residual stress between mullite/ZrO$_2$.

• The Korean Journal of Ceramics
• /
• v.4 no.4
• /
• pp.356-362
• /
• 1998

Hertzian crack suppression phenomena and relatively high damage tolerance were investigated in hard/soft silicon nitride ($Si_3N_4$) bilayers. Coarse $\alpha}-Si_3N_4$ powder was wsed for the hard coating layer and fine $\alpha}-Si_3N_4$ powder was used for the soft substrate layer. The two layers were designed with a strong interface. Hertzian indentation was used to investigate contact fracture and damage tolerance property. Hertzian crack suppression has occurred with increasing applied load and decreasing coating thickness. The crack suppression contributed strength improvement, especially in the bilayers with thinner coatings. Ultimately, the combination of hard coating with soft but tough underlayer improved the damage tolerance of brittle $Si_3N_4$ ceramics.

• Proceedings of the Korean Powder Metallurgy Institute Conference
• /
• 2006.09b
• /
• pp.756-757
• /
• 2006

P/M enables the economical production of components for many kinds of gears. Functionally, the sub gear requires high tooth accuracy and bending fatigue strength. The whole tooth profile was sized after sintering to satisfy the gear tooth accuracy specification. The part was redesigned to reduce machining requirements. The required bending fatigue strength was achieved through appropriate material choice and induction of compressive residual stress by shotpeening after carburizing. The P/M sub gear replaced a forged steel gear, satisfied performance requirements, expanded the use of P/M applications and provided over 30% cost reduction.

• Proceedings of the Korean Powder Metallurgy Institute Conference
• /
• 2002.04b
• /
• pp.11-11
• /
• 2002

Plastic deformation was observed by TEM around the intragranular SiC particles in the $Al_2O_3$ matrix for $Al_2O_3/SiC$ nanocomposite system. The dislocations are generated at selected planes and there is a tendency for the dislocations to form a subgrain boundary structure with low-angel grain boundaries and networks. In this study, dislocation generated in the $Al_2O_3$ matrix during cooling down from sintering temperatures by the highly localized thermal stresses within and/or around SiC particles caused from the thermal expansion mismatch between $Al_2O_3$ matrix and SiC particle was observed. In monolithic $Al_2O_3$ and $Al_2O_3/SiC$ microcomposite system. These phenomena is closely related to the plastic relaxation of the elastic stress and strain energy associated with both thermal misfitting inclusions and creep behaviors. The plastic relaxation behavior was explained by combination of yield stress and internal stress.

• Journal of Powder Materials
• /
• v.17 no.3
• /
• pp.197-202
• /
• 2010

Low temperature degradation behavior in yttria stabilized tetragonal zirconia polycrystal (Y-TZP) ceramics was microscopically observed from the phase contrast between monoclinic surface and tetragonal matrix. The degradation behavior was dependent on the surface treatment of sintered Y-TZP, even if the sintering history is same. In the mirror polished specimen, the monoclinic layer appeared in a uniform thickness from the surface. On the contrary, for the specimen with coarse scratch, the thickness of degraded surface was more than double especially from the coarse scratch. Since the scratch results in local deformation, the residual stress should be induced around the scratch. With the transformation from tetragonal to monoclinic, the volume expansion exerts a stress on a neighboring grains and promotes a successive phase transformation. Such a autocatalytic effect can be triggered from the part of coarse scratch.

• Journal of the Korea Institute of Military Science and Technology
• /
• v.8 no.1 s.20
• /
• pp.14-24
• /
• 2005

A propellant mainly consisting of nitric ester including nitrocellulose, nitroglycerine and nitroguanidine is characteristic of being decomposed naturally. And this phenomenon is known as being affected mostly by its storing temperature. In this research, the effect of storing temperature on self life has been studied by measuring the contained quantity of residual stabilizer of propellant KM30A1, ignition powder and combustible cartridge case, which are parts of 155MM propelling charge K676 and K677; the method for the measurement is acceleration aging test, and decomposition reaction equation and Berthlot Equation were used for the calculation. The result of this research shows that propellant KM30A1, ignition powder, combustible cartridge case in order of decreasing self life, and the self life decreases to 1/3 as the temperature increases by $10^{\circ}C$.

• Proceedings of the Korean Powder Metallurgy Institute Conference
• /
• 2006.09a
• /
• pp.132-133
• /
• 2006

Optimized choice of material for two principally different types of PM components is presented. The first is characterized by high stresses in areas with high stress concentrations (for example synchronizer hubs with very sharp notches, typically <0.25mm in the pre-synchronizer slot and the inner splines). The second type has slightly larger notch radii (small spur gears and sprockets with typically notch radii between 1- 3mm). Diffusion alloyed materials are well suited for sharp notch components. Pre-alloyed materials are also well suited for applications with sharp notches if compressive residual stresses in the notch roots are created by appropriate process control. A free choice of material is available for components with the larger notch radii.

• Journal of Powder Materials
• /
• v.27 no.4
• /
• pp.287-292
• /
• 2020

The subject of this study is a zeolite generated as a by-product of recycling LAS (lithium-aluminum-silicate) resources, a kind of glass and ceramic produced by induction. The zeolite by-product is modified into Mg-zeolite using Mg as a cation to absorb Pb, a heavy metal generated from water pollution caused by recent industrial wastewater. An ion-exchange method is used to carry out the modification process, from zeolite byproduct to Mg-zeolite, and simultaneously absorb the Pb in the heavy-metal solution (99.032 mg/L). It is found that the sodium zeolite in the raw material residue can be modified to magnesium zeolite by reacting it with a mixture solution at 1 M concentration for 24 h. As a result, it is found that the residual Pb (0.130 mg/L) in the heavy metal solution is shown to be absorbed by 99.86%, with successful formation of a Mg-modified zeolite.