• Title/Summary/Keyword: residual powder

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Manufacturing Technology for Tape Casting and Soft Magnetic Powder Using by Recycling Scrap of Fe-Si Electrical Sheet (Fe-Si 전기강판 폐스크랩을 이용한 연자성 분말 및 테이프 제조기술)

  • Hong, Won Sik;Kim, Sang Hyun;Park, Ji-Yeon;Oh, Chulmin;Lee, Woo Sung;Kim, Seung Gyeom;Han, Sang Jo;Shim, Geum Taek;Kim, Hwi-Jun
    • Journal of the Microelectronics and Packaging Society
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    • v.23 no.2
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    • pp.11-18
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    • 2016
  • This study focused on examining the possibility for recycling of Fe-Si electric sheet. We manufactured Fe-6.5Si mother alloy using by Fe-Si electric sheet scrap for transformer core materials. And then, soft magnetic alloy powder which diameter and shape were $45{\sim}150{\mu}m$ and sphere type was prepared by gas atomization process. As we compared to commercial Fe-6.5Si powder, its diameter distribution and microstructure of recycled powder was a similar. To investigate the possibility of reusing the soft magnetic composite sheet for electronics, recycled powder was treated to have a high aspect ratio (AR), and we finally obtained the 65~66 AR and $2.3{\mu}m$ thickness powder. To release the residual stress of powder, heat treatment was conducted under $300{\sim}400^{\circ}C$, $N_2$ gas. And then, soft magnetic sheet was made by tape casting process using by those powders. After the density and permeability of tape was measured, and we confirmed that the recycled Fe-Si electric sheet scrap was possible to reuse the soft magnetic materials of electronics.

Preparation of Ultrafine C/N Controled TiCxNy Powders by Magnesium Reduction (마그네슘환원에 의한 C/N 조성제어 초미립 TiCxNy 분말 합성)

  • Lee, Dong-Won;Kim, Byoung-Kee;Yun, Jung-Yeul;Yu, Ji-Hoon;Kim, Yong-Jin
    • Journal of Powder Materials
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    • v.17 no.2
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    • pp.142-147
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    • 2010
  • The ultrafine titanium carbonitride ($TiC_xN_y$) particles below 100 nm in mean size, including various carbon and nitrogen contents (x=0.55~0.9, y=0.1~0.5), were successfully synthesized by new Mg-thermal reduction process. Nanostructured sub-stoichiometric titanium carbide ($TiC_x$) particles were initially produced by the magnesium reduction of gaseous $TiCl_4+x/2C_2Cl_4$ at $890^{\circ}C$ and post heat treatments in vacuum were performed for 2 hrs to remove residual magnesium and magnesium chloride mixed with $TiC_x$. Finally, well C/N-controled $TiC_xN_y$ phases were successfully produced by nitrification heat treatment under normal $N_2$ gas atmosphere at $1150^{\circ}C$ for 2 hrs. The values of purity, mean particle size and oxygen content of produced particles were about 99.3%, 100 nm and 0.2 wt.%, respectively.

Effect of Red Pepper (Capsicum frutescens) Powder or Red Pepper Pigment on the Performance and Egg Yolk Color of Laying Hens

  • Li, Huaqiang;Jin, Liji;Wu, Feifei;Thacker, Philip;Li, Xiaoyu;You, Jiansong;Wang, Xiaoyan;Liu, Sizhao;Li, Shuying;Xu, Yongping
    • Asian-Australasian Journal of Animal Sciences
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    • v.25 no.11
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    • pp.1605-1610
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    • 2012
  • Two experiments were conducted to study the effects of red pepper (Capsicum frutescens) powder or red pepper pigment on the performance and egg yolk color of laying hens. In Exp. 1, 210, thirty-wk old, Hy-line Brown laying hens were fed one of seven diets containing 0.3, 0.6, 1.2, 2.0, 4.8 or 9.6 ppm red pepper pigment or 0.3 ppm carophyll red. Each diet was fed to three replicate batteries of hens with each battery consisting of a row of five cages of hens with two hens per cage (n = 3). In Exp. 2, 180, thirty-wk old, Hyline Brown laying hens, housed similarly to those in Exp. 1, were fed an unsupplemented basal diet as well as treatments in which the basal diet was supplemented with 0.8% red pepper powder processed in a laboratory blender to an average particle size of $300{\mu}m$, 0.8% red pepper powder processed as a super fine powder with a vibrational mill ($44{\mu}m$) and finally 0.8% red pepper powder processed as a super fine powder with a vibrational mill but mixed with 5% $Na_2CO_3$ either before or after grinding. A diet supplemented with 0.3 ppm carophyll red pigment was also included (n = 3). In both experiments, hens were fed the red pepper powder or pigment for 14 days. After feeding of the powder or pigment was terminated, all hens were fed the basal diet for eight more days to determine if the dietary treatments had any residual effects. In Exp. 1, there were no differences in egg-laying performance, feed consumption or feed conversion ratio due to inclusion of red pepper pigment in the diet. Average egg weight was higher (p<0.05) for birds fed 1.2, 2.4 or 9.6 ppm red pepper pigment than for birds fed the diet containing 0.3 ppm red pepper pigment. On d 14, egg color scores increased linearly as the level of red pepper pigment in the diet increased. In Exp. 2, feeding red pepper powder did not affect egg-laying performance, feed consumption or feed conversion ratio (p>0.05). However, compared with the control group, supplementation with all of the red pepper powder treatments increased egg weight (p<0.05). All the red pepper powder treatments also increased (p<0.05) the yolk color score compared with the control. The results of the present study suggest that both red pepper powder and pigment are effective feed additives for improving egg yolk color for laying hens.

Fundamental Properties Polymer-Modified Mortars Using Re-dispersible Polymer Powder (재유화형 폴리머를 혼입한 폴리머 시멘트 모르타르의 내화특성)

  • Jang, Kun-Young;Ryu, Dong-Woo
    • Journal of the Architectural Institute of Korea Structure & Construction
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    • v.35 no.3
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    • pp.35-41
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    • 2019
  • In this study, the fire resistance performance of polymer cement mortars which are used as a representative repair material for section restoration, is evaluated and residual bond strength is measured by considering unity with concrete. According to the evaluation of fire resistance performance of re-emulsification type polymer cement mortars, residual compressive strength was drastically decreased according to heating temperatures with an increase of polymer addition rate, and this seems to be attributable to the application of polymer film. In addition, an explosion phenomenon occurred frequently with an increase of addition rate, so this should be considered when selecting repair materials and processing.

Residual Stress Measurement on T-type Welded Specimen by Neutron Diffraction

  • Jang, D.Y.;Park, M.J.;Choi, H.D.;Kim, J.P.
    • International Journal of Korean Welding Society
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    • v.1 no.2
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    • pp.45-50
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    • 2001
  • This paper presents application of neutron diffraction technique to the measurement of residual stresses in the T-type 20 m thick welded stainless steel plates(100$\times$50 $mm^2$ and 50$\times$50 $mm^2$). The High Resolution Powder Diffractormeter of the Korea Atomic Research Institute was utilized in the measurement. The power of nuclear reactor was 24 MWt and the measured reflection in the 220 plane (2$\theta$)was $92.66^{\circ}$. Poisson ratio of 0.265 and elastic constant of 211 GPa were applied to the calculation of stresses and strains. Three directional components such as normal, transverse, and longitudinal stresses were measured. The results showed that three components were tensile and became compressive along the y axis in the zone away from the welded center. The compressive stresses became tensile in the zone away from the center line of x axis. This may be due to the balance effect caused by the net stress to keep the specimen shape flat.

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Life Prediction of Hydraulic Concrete Based on Grey Residual Markov Model

  • Gong, Li;Gong, Xuelei;Liang, Ying;Zhang, Bingzong;Yang, Yiqun
    • Journal of Information Processing Systems
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    • v.18 no.4
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    • pp.457-469
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    • 2022
  • Hydraulic concrete buildings in the northwest of China are often subject to the combined effects of low-temperature frost damage, during drying and wetting cycles, and salt erosion, so the study of concrete deterioration prediction is of major importance. The prediction model of the relative dynamic elastic modulus (RDEM) of four different kinds of modified concrete under the special environment in the northwest of China was established using Grey residual Markov theory. Based on the available test data, modified values of the dynamic elastic modulus were obtained based on the Grey GM(1,1) model and the residual GM(1,1) model, combined with the Markov sign correction, and the dynamic elastic modulus of concrete was predicted. The computational analysis showed that the maximum relative error of the corrected dynamic elastic modulus was significantly reduced, from 1.599% to 0.270% for the BS2 group. The analysis error showed that the model was more adjusted to the concrete mixed with fly ash and mineral powder, and its calculation error was significantly lower than that of the rest of the groups. The analysis of the data for each group proved that the model could predict the loss of dynamic elastic modulus of the deterioration of the concrete effectively, as well as the number of cycles when the concrete reached the damaged state.

A Study on the Accuracy of Measurement of Residual Urine Amount depending on the Bladder form using Ultrasonic (초음파를 이용한 Bladder형태에 따른 잔뇨량 측정의 정확도 연구)

  • Kim, Y.M.;Park, T.H.;Kim, J.H.;Kim, S.J.;Hoon, J.D.;Heo, J.Y.;Han, D.G.
    • Korean Journal of Digital Imaging in Medicine
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    • v.16 no.2
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    • pp.1-7
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    • 2014
  • This study is to increase the accuracy of the diagnosis of benign prostatic hyperplasia by presenting a method that can accurately measure the residual urine amount of the bladder by using an ultrasound image. Agar powder, Propanol and distilled water were used as materials for making a phantom. In order to measure the volume, a $10m{\ell}$ cylinder, syringe and beaker were used. The image was obtained by scanning phantoms produced into six shapes. Each constant value was obtained by using the expression designed to measure the residual urine amount of the bladder and was compared and analyzed. The measuring method of Bladder volume was presented and a constant value for each shape was obtained and five observers measured it five times. According to the results of clinical application, the errors of Ellipse-beanbag, Shield-shield were 11.0%, 18.2%, respectively. Constant values depending on the shape of each phantom were presented in order to accurately measure the volume of the bladder in measuring the amount of residual urine for the diagnosis of benign prostatic hyperplasia. The accuracy of the volume using this was verified statistically(p > 0.05). Therefore, it is considered to be useful in diagnosing benign prostatic hyperplasia by using the ultrasound imaging measuring method presented.

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Soft Magnetic Property of Ternary Fe-9.8Si-6.0Al Alloy Using by Recycling Fe-Si Electrical Steel Sheet Scrap (Fe-Si 전기강판 폐스크랩을 이용한 3원계 Fe-9.8Si-6.0Al 합금의 연자성 특성)

  • Hong, Won Sik;Yang, Hyoung Woo;Park, Ji-Yeon;Oh, Chulmin;Lee, Woo Sung;Kim, Seung Gyeom;Han, Sang Jo;Shim, Geum Taek;Kim, Hwi-Jun
    • Journal of the Microelectronics and Packaging Society
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    • v.24 no.1
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    • pp.1-8
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    • 2017
  • Fe-9.8Si-6.0Al mother alloy was manufactured using by Fe-3.5Si recycled scrap and Si powder. And then, soft magnetic alloy powder of $D_{50}$ size and sphere type were prepared by gas atomization process. To obtain the soft magnetic powder of a high aspect ratio, in the first, we conducted the ball milling process for 8 hours. And heat treatment was performed under $650^{\circ}C$, 2 hours and $N_2$ atmosphere condition for reducing the residual stress of the powder. Based on these process, we made around $50{\mu}m$ diameter Fe-9.8Si-6.0Al powder, which morphology and shape was a similar to the commercial Fe-Si-Al powder. Finally, the soft magnetic sheets were prepared by tape casting process using by those powders. The permeability of the tape casting sheet was measured, and we confirmed the possibility of reusing to the soft magnetic materials of Fe-Si electric sheet scrap.

Preparation of Highly Efficient Nd-Fe-B Magnetic Powders by Reduction/Diffusion Process (환원/확산 공정에 의한 고성능 Nd-Fe-B 자성분말의 제조)

  • Kim, Dongsoo;Chen, Chunqiang;Baek, Younkyoung;Choi, Chuljin
    • Journal of Powder Materials
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    • v.20 no.3
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    • pp.197-202
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    • 2013
  • A novel route to prepare Nd-Fe-B magnetic particles by utilizing both spray drying and reduction/diffusion processes was investigated in this study. Precursors were prepared by spray drying method using the aqueous solutions containing Nd salt, Fe salt and boric acid with stoichiometric ratios. Precursor particles could be obtained with various sizes from 2 to $10{\mu}m$ by controlling concentrations of the solutions and the average size of $2{\mu}m$ of precursors were selected for further steps. After heat treatment of precursors in air, Nd and Fe oxides were formed through desalting procedure, followed by reduction processes in Hydrogen ($H_2$) atmosphere and with Calcium (Ca) granules in Argon (Ar) successively. Moreover, diffusion between Nd and Fe occurred during Ca reduction and $Nd_2Fe_{14}B$ particles were formed. With Ca amount added to particles after $H_2$ reduction, intrinsic coercivity was changed from 1 to 10 kOe. In order to remove and leach CaO and residual Ca, de-ionized water and dilute acid were used. Acidic solutions were more effective to eliminate impurities, but Fe and Nd were dissolved out from the particles. Finally, $Nd_2Fe_{14}B$ magnetic particles were synthesized after washing in de-ionized water with a mean size of $2{\mu}m$ and their maximum energy product showed 9.23 MGOe.

Quality Characteristics and Consumer Acceptability of Cookies Supplemented with Watermelon (Citrullus vulgaris Schrad) Powder (수박(Citrullus vulgaris Schrad)분말을 첨가한 쿠키의 품질특성 및 관능적 특성)

  • Ock, Ji-Ye;Oh, Ji Eun;Kang, Nam E;Cho, Mi Sook
    • Journal of the Korean Society of Food Culture
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    • v.37 no.1
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    • pp.73-80
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    • 2022
  • The purpose of this study was to evaluate cookies prepared with five different quantities (0, 5, 10, 15, and 20%) of watermelon powder (WP). This study analyzed quality characteristics, consumer liking, and CATA (check-all-that-apply) of the samples. The density and pH of the cookie dough and the L-value of the cookies tended to decrease as the amount of watermelon powder increased (p<0.05), whereas the spread factor, a-value, and hardness of the cookies tended to increase as the amount of watermelon powder increased (p<0.001). The b-value tended to increase up to WP10, but it tended to decrease from WP15 (p<0.001). The results of the evaluation of consumer liking showed that overall liking was the highest for WP5 and lowest for WP20 (p<0.05). In the analysis of the CATA survey, the main reasons for liking for all the samples were 'Appearance', 'Color', 'Sweet taste', 'Nutty odor/flavor', 'Crispiness', and 'Familiarity'. WP5 showed the most diverse reasons for being liked. The common reason for disliking samples with the addition of watermelon powder was 'Residual feel in the mouth'. In the correspondence analysis, attributes of 'Stale taste', 'Clean taste', 'Softness', 'Familiarity', 'Moistness', 'Color', 'Blandness' were detected in the WP0 and WP5. The results indicate that WP5 with a 5% supplementation of watermelon powder is appropriate for improving the quality and consumer acceptability of the cookies.