• 제목/요약/키워드: research instruments

검색결과 1,682건 처리시간 0.03초

Comparison of Real Time Nanoparticle Monitoring Instruments in the Workplaces

  • Ham, Seunghon;Lee, Naroo;Eom, Igchun;Lee, Byoungcheun;Tsai, Perng-Jy;Lee, Kiyoung;Yoon, Chungsik
    • Safety and Health at Work
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    • 제7권4호
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    • pp.381-388
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    • 2016
  • Background: Relationships among portable scanning mobility particle sizer (P-SMPS), condensation particle counter (CPC), and surface area monitor (SAM), which are different metric measurement devices, were investigated, and two widely used research grade (RG)-SMPSs were compared to harmonize the measurement protocols. Methods: Pearson correlation analysis was performed to compare the relation between P-SMPS, CPC, and SAM and two common RG-SMPS. Results: For laboratory and engineered nanoparticle (ENP) workplaces, correlation among devices showed good relationships. Correlation among devices was fair in unintended nanoparticle (UNP)-emitting workplaces. This is partly explained by the fact that shape of particles was not spherical, although calibration of sampling instruments was performed using spherical particles and the concentration was very high at the UNP workplaces to allow them to aggregate more easily. Chain-like particles were found by scanning electron microscope in UNP workplaces. The CPC or SAM could be used as an alternative instrument instead of SMPS at the ENP-handling workplaces. At the UNP workplaces, where concentration is high, real-time instruments should be used with caution. There are significant differences between the two SMPSs tested. TSI SMPS showed about 20% higher concentration than the Grimm SMPS in all workplaces. Conclusions: For nanoparticle measurement, CPC and SAM might be useful to find source of emission at laboratory and ENP workplaces instead of P-SMPS in the first stage. An SMPS is required to measure with high accuracy. Caution is necessary when comparing data from different nanoparticle measurement devices and RG-SMPSs.

타코나이트 광산 공정에서의 실시간 질량측정기기와 실시간 수농도의 환산에 의한 질량농도와의 연관성 (Relationships between a Calculated Mass Concentration and a Measured Concentration of PM2.5 and Respirable Particle Matter Sampling Direct-Reading Instruments in Taconite Mines)

  • 정은교;장재길;송세욱;김정호
    • 한국산업보건학회지
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    • 제24권1호
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    • pp.65-73
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    • 2014
  • Objectives: The purposes of this study are to investigate workers' exposures to respirable particles generated in taconite mines and to compare two metric methods for mass concentrations using direct-reading instruments. Methods: Air monitorings were conducted at six mines where subjects have been exposed primarily to particulate matters in crushing, concentrating, and pelletizing processes. Air samples were collected during 4 hours of the entire work shift for similarly exposure groups(SEGs) of nine jobs(N=37). Following instruments were employed to evaluate the workplace: a nanoparticle aerosol monitor(particle size range; 10-1000 nm, unit: ${\mu}m^2/cc$, Model 9000, TSI Inc.); DustTrak air monitors($PM_{10}$, $PM_{2.5}$, unit: $mg/m^3$, Model 8520, TSI Inc.); a condensation particle counter(size range; 20-1000 nm, unit: #/cc, P-Trak 8525, TSI Inc.); and an optical particle counter(particle number by size range $0.3-25{\mu}m$, unit: #/cc, Aerotrak 9306, TSI Inc.). Results: The highest airborne concentration among SEGs was for furnace operator followed by pelletizing maintenance workers in number of particle and surface area, but not in mass concentrations. The geometric means of $PM_{2.5}$ by the DustTrak and the Ptrak/Aerotrak were $0.04{\mu}m$(GSD 2.52) and $0.07{\mu}m$(GSD 2.60), respectively. Also, the geometric means of RPM by the DustTrak and the Ptrak/Aerotrak were $0.16{\mu}m$(GSD 2.24) and $0.32{\mu}m$(GSD 3.24), respectively. The Pearson correlation coefficient for DustTrak $PM_{2.5}$ and Ptrak/Aerotrak $PM_{2.5}$ was 0.56, and that of DustTrak RPM and Ptrak/Aerotrak RPM was 0.65, indicating a moderate positive association between the two sampling methods. Surface area and number concentration were highly correlated($R^2$ = 0.80), while $PM_{2.5}$ and RPM were also statistically correlated each other($R^2$ = 0.79). Conclusions: The results suggest that it is possible to measure airborne particulates by mass concentrations or particle number concentrations using real-time instruments instead of using the DustTrak Aerosol monitor that monitor mass concentrations only.

벼 생엽의 질소함량 현장분석을 위한 NIRS 검량식 개발 및 검증 (NIRS Calibration Equation Development and Validation for Total Nitrogen Contents Field Analysis in Fresh Rice Leaves)

  • 송영은;이덕렬;조승현;이기권;정종성;권영립;조규채
    • 한국작물학회지
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    • 제58권3호
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    • pp.301-307
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    • 2013
  • 연구용 NIR 장비에서 수집된 벼 생엽의 질소 함량 검량식 및 데이터베이스를 현장용 NIR 장비에 검량식을 이설, 검증함으로서 현장 적용 가능성을 평가하기 위해 수행한 결과는 다음과 같다. 1. 2003년부터 2009년까지 스펙트럼을 수집한 시료 중 선발 된 A 데이터 세트(개체수 454점)의 총 질소범위는 2.041%~4.933%, 2012년 수집된 B 데이터 세트(258점)는 2.180%~3.690%이며 각각의 전체 평균은 3.497%, 2.712%였다. 2. A, B 데이터 세트에서 유도된 검량식 결과 결정계수($R^2$)는 각각 0.845, 0.777,표준오차(SEC)는 0.196, 0.126, SECV는 0.238, 0.150이었다. 3. 연구용 NIR 장비 400 nm~2500 nm 파장에서 얻어진 데이터베이스를 현장용 NIR 장비 1200 nm~2400 nm 파장에 맞게 잘라 이설한 후 2012년 데이터베이스에 업데이트 확장한 후 작성된 검량식 결과 결정계수($R^2$)는 0.880, 표준오차(SEC)는 0.191이었다. 4. 연구용 NIR 장비에 구축된 데이터베이스를 현장용 NIR 장비에 맞춰 데이터베이스를 확장 업데이트하고 검량식을 이설한 결과 연구용 장비와의 표준오차는 0.005%로 거의 동일한 수준의 결과를 얻었다.

광산란 측정장치에 따른 대중교통차량 미세먼지 측정 특성 (Characteristics of PM10 Measured by Different Light-Scattering Instruments in Public Transport Vehicles)

  • 권순박;정우태;박덕신
    • 한국입자에어로졸학회지
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    • 제11권1호
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    • pp.1-8
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    • 2015
  • In this study, indoor $PM_{10}$ concentration was measured by different type of real-time instruments in public transport vehicles. Light-scattering method is widely used in measuring the size of particulate matters and there is two types of light-scattering methods; one is the nephelometer type which measures the light-scattering degree by aerosol cloud, the other is the spectrometer type which measures light-scattering degree by individual particle. We observed the variation of $PM_{10}$ in KTX, subway and express bus carriages by 1-minute resolution and found that there is similar tendency in pattern among 4 light-scattering devices but difference in absolute concentrations. By comparing gravimetric result in a subway cabin, the spectrometer type device, C, was chosen as a reference device. The conversion factors of nephelometer device A-1, A-2, and B were 1.666, 1.463 and 2.125 respectively.

관성 충돌 방식의 액적 분리장치의 수분제거효율 평가 (Evaluation of Removal Efficiency of Water Contents using Inertial Impaction Separator)

  • 이신영;홍원석;신완호;김규진;송동근
    • 한국입자에어로졸학회지
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    • 제9권1호
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    • pp.23-29
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    • 2013
  • Inertial impaction type mist eliminators are the most effective instruments to separate mist from the gas. In this work, the effect of the horizontal chevron type mist eliminators is characterized experimentally. Droplet size distribution and evaluation of removal efficiency of the chevron type mist eliminators at different gas flows were investigated using an aerosol particle size analyzer and a portable aerosol spectrometer, respectively. The experimental investigations showed that the mist removal efficiency in these instruments is dependent in the droplet size, and the pressure drop is nil.

Analysis of Agrochemical Residues in Tobacco Using Solid Phase Microextraction-Gas Chromatography with Different Mass Spectrometric Techniques

  • Lee, Jeong-Min;Jang, Gi-Chul;Kim, Hyo-Keun;Hwang, Geon-Joong
    • 한국연초학회지
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    • 제30권2호
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    • pp.117-124
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    • 2008
  • A solid phase microextraction (SPME) method in combination with gas chromatography/mass spectrometric techniques was used for the extraction and quantification of 12 selected agrochemical residues in tobacco. The parameters such as the type of SPME fiber, adsorption/desorption time and the extraction temperature affecting the precision and accuracy of the SPME method were investigated and optimized. Among three types of fibers investigated, polyacrylate (PA), polydimethylsiloxane (PDMS) and polydimethylsiloxane-divinylbenzene (PDMS-DVB), PDMS fiber was selected for the extractions of the agrochemicals. The SPME device was automated and on-line coupled to a gas chromatograph with a mass spectrometer. Mass spectrometry (MS) was used and two different instruments, a quadrupole MS and triple quadrupole MS-MS mode, were compared. The performances of the two GC-MS instruments were comparable in terms of linearity (in the range of 0.01$\sim$0.5 $\mu$g/mL) and sensitivity (limits of detection were in the low ng/mL range). The triple quadrupole MS-MS instrument gave better precision than that of quadrupole MS system, but generally the relative standard deviations for replicates were acceptable for both instruments (< 15%). The LODs was fully satisfied the requirements of the CORESTA GRL. Recoveries of 12 selected agrochemicals in tobacco yielded more than 80% and reproducibility was found to be better than 10% RSD so that SPME procedure could be applied to the quantitative analysis of agrochemical residues in tobacco.

Factors Associated with Death Acceptance among Thai Patients with Advanced Cancer

  • Krapo, Maliwan;Thanasilp, Sureeporn;Chimluang, Janya
    • Asian Journal for Public Opinion Research
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    • 제6권1호
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    • pp.18-30
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    • 2018
  • Patients with advanced cancer cope with various issues, especially psychological symptoms, such as anxiety about death. Previous research from various countries indicates that most advanced cancer patients perceive distress before death, which means they cannot accept death peacefully. The purpose of this study was to examine the factors associated with death acceptance of Thai patients with advanced cancer. The participants were 242 adult patients with advanced cancer from three tertiary hospitals in Bangkok, Thailand. The research instruments consisted of 7 questionnaires: a personal information questionnaire, the death anxiety questionnaire, Buddhist beliefs about death questionnaire, the unfinished task questionnaire, general self-efficacy scale, family relationship questionnaire, and death acceptance scale. These instruments were tested for their content validity by a panel of experts. All instruments except the first one were tested for reliability, and their Cronbach's alpha coefficient were .86, .72, .74, .74, .89, and .70, respectively. Descriptive statistics, Pearson's correlation, Point-biserial correlation coefficient, and stepwise multiple regression were used to analyze the data. The results revealed that a total of 42% of variance of death acceptance among Thai patients with advanced cancer was explained by death anxiety, Buddhist beliefs about death, and self-efficacy. Knowing these factors provides further information for nurses to help patients to cope with their death. From this crucial knowledge, nurses can develop interventions in decreasing or controlling anxiety about death, promoting Buddhist beliefs about death, and enhancing self-efficacy of advanced cancer patients. Therefore, a better quality of life and good death can be achieved.

COMPARISON OF ENVIRONMENTAL STRESS DIAGNOSIS OF CUCUMBER PLANT USING VARIOUS PHYSIOLOGICAL INSTRUMENTS

  • Suh, S.R.;Chung, G.C.;Sung, J.H.;Ryu, Y.S.;Lee, K.H.
    • 한국농업기계학회:학술대회논문집
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    • 한국농업기계학회 2000년도 THE THIRD INTERNATIONAL CONFERENCE ON AGRICULTURAL MACHINERY ENGINEERING. V.III
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    • pp.736-743
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    • 2000
  • This paper represents our efforts to diagnose environmental stresses using physiological instruments in cucumber plants. The stresses could be detected by measuring and analyzing the difference of chlorophyll content, photosynthetic efficiency(Fv/Fm), differential temperature(DT), stomatal resistance and light absorbance values between treated and controlled plants. From the all over experiments, the stresses could be first diagnosed on the 1st to 5th day after treatment and the overall diagnosis rate was estimated at more than 50%.

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ANALYSIS OF TROPOSPHERIC $NO_2$ BASED ON SATELLITE MEASUREMENTS

  • Kwon Eun-Han;Lim Hyo-Suk
    • 대한원격탐사학회:학술대회논문집
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    • 대한원격탐사학회 2005년도 Proceedings of ISRS 2005
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    • pp.374-377
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    • 2005
  • The distribution and changes of tropospheric nitrogen dioxide ($NO_2$) are analyzed using the satellite measurements data from GOME (Global Ozone Monitoring Experiment) and SCIMACHY (SCanning Imaging Absorption spectroMeter for Atmospheric CHartographY). We produced global maps of tropospheric $NO_2$ for 4 seasons using GOME measurements from January 1997 to June 2003. The global distribution shows high values in regions with dense population and high industrialization. Tropospheric $NO_2$ shows obvious seasonal changes depending on its emission and lifetime. Based on the good agreement between two instruments in the time period of overlapping measurements (January 2003-June2003), we linked SClAMACHY data to the GOME time series. The combined time series over the past decade indicate that $NO_2$ 1evels over China are rapidly increasing while those over Europe are decreasing. We also discussed potential application of spaceborne instruments in detecting and characterizing long-distance transport of $NO_2$.

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