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Ductile-Regime Nanopatterning on Pyrex 7740 Glass Surface and Its Application to the Fabrication of Positive-tone PDMS Stamp for Microcontact Printing (${\mu}CP$) (미소접촉인쇄 공정용 철형 PDMS 스템프 제작을 위한 Pyrex 7740 glass 표면의 연성영역 나노패터닝)

  • Kim H. I.;Youn S. W.;Kang C. G.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2004.10a
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    • pp.40-43
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    • 2004
  • Stamps for microcontact processing are fabricated by casting elastomer such as PDMS on a master with a negative of the desired pattern. After curing, the PDMS stamp is peeled away from the master and exposed to a solution of ink and then dried. Transfer of the ink from the PDMS stamp to the substrate occurs during a brief contact between stamp and substrate. Generally, negative-tone masters, which are used for making positive-tone PDMS stamps, are fabricated by using photolithographic technique. The shortcomings of photolithography are a relative high-cost process and require extensive processing time and heavy capital investment to build and maintain the fabrication facilities. The goal of this study is to fabricate a negative-tone master by using Nano-indenter based patterning technique. Various sizes of V-grooves and U-groove were fabricated by using the combination of nanoscratch and HF isotropic etching technique. An achieved negative-tone structure was used as a master in the PDMS replica molding process to fabricate a positive-tone PDMS stamp.

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PDMS Stamp Fabrication for Photonic Crystal Waveguides (광자결정 도파로 성형용 PDMS 스탬프 제작)

  • Oh, Seung-Hun;Choi, Du-Seon;Kim, Chang-Seok;Jeong, Myung-Yung
    • Journal of the Korean Society for Precision Engineering
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    • v.24 no.4 s.193
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    • pp.153-158
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    • 2007
  • Recently nano imprint lithography to fabricate photonic crystal on polymer is preferred because of its simplicity and short process time and ease of precise manufacturing. But, the technique requires the precise mold as an imprinting tool for good replication. These molds are made of the silicon, nickel and quartz. But this is not desirable due to complex fabrication process, high cost. So, we describe a simple, precise and low cost method of fabricating PDMS stamp to make the photonic crystals. In order to fabricate the PDMS mold, we make the original pattern with designed hole array by finding the optimal electron beam writing condition. And then, we have tried to fabricate PDMS mold by the replica molding with ultrasonic vibration and pressure system. We have used the cleaning process to solve the detaching problem on the interface. Using these methods, we acquired the PDMS mold for photonic crystals with characteristics of a good replication. And the accuracy of replication shows below 1% in 440nm at diameter and in 610nm at lattice constant by dimensional analysis by SEM and AFM.

Development of Food Replicas as Dietary Education Materials for Children (음식모형을 활용한 어린이 식생활 교육 매체 개발)

  • Hong, Kyung Hee;Kim, Soon Mi;Um, Min Young
    • Journal of the Korean Society of Food Culture
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    • v.27 no.5
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    • pp.434-444
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    • 2012
  • The purpose of this study was to develop children-friendly education materials based on food replicas for the dietary education of lower grade elementary students. Through a literature review on current dietary problems and dietary education for children, five education themes were chosen: balanced diet, seasonal food, traditional food, noodle culture, and making instant noodles. A total of 304 key food items for food replicas were selected based on the themes: six basic food groups (113 items), balanced meals (37 items), dietary habits (74 items), spring foods (13 items), summer foods (17 items), autumn foods (16 items), winter foods (11 items), Korean traditional foods (52 items), Korean native noodles (18 items), noodles from foreign countries (19 items), and making instant noodles (46 items). Next, a food replica database was developed consisting of name of the food, picture, size, ingredient, recipe, reference, and attached code. Powerpoint slides and teaching plans for all education themes were developed utilizing the food replicas in order to raise interest and understanding of serving size and intake amount. This research provides a basis for the development of food replicas as effective dietary education materials for elementary students and their use in extra-curricular activities, after school programs, community health centers, or food companies.

Morphological Evidence for the Transport of Dehydrocholic Acid in the Hepatocyte as Revealed by Freeze Fracture Replica (급속동결할단법에 의한 간세포내 Dehydrocholic Acid 수송에 관한 형태학적 관찰)

  • Shin, Young-Chul
    • Applied Microscopy
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    • v.28 no.1
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    • pp.83-90
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    • 1998
  • The pathway of intracellular transport of dehydrocholic acid was investigated in the hepatocytes of rats by transmission electron microscopy with conventional and freeze fracture methods. Both in normal and experimental groups, the cis Golgi cisterns were sacculated and faces toward the bile canaliculus. In the experimental group, however, the cis Golgi cisterns showed buds, which were probably separated to be vesicles. Some of the buds were connected to the cisterns with the narrow neck. The vesicles were increased in the vicinity of bile canaliculi. The fusion between vesicles and bile canaliculus were frequently observed in the experimental group. This was particularly well shown in the freeze fracture replica. In the thin section, the vesicles were devoid of visible contents as seen in the bile canaliculli. The evidence suggests that the vesicles are derived from the cis Gogi cistern in the way that buds pinch off, serve as vehicles to transport dehydrocholic acids and fuse to bile canaliculi for exocytosis.

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Fractographic Analysis of Ceramic Composites by Transmission Electron Microscopy using Surface Replication Technique (표면복제법을 이용한 세라믹 복합재료 파괴현상의 투과전자현미경 분석)

  • Jun, Hyeung-Woo;Kim, Gyeung-Ho;Kim, Byung-Ho
    • Applied Microscopy
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    • v.26 no.4
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    • pp.447-456
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    • 1996
  • Fracture surfaces of materials contain useful information ranging from crack path to the mechanism of fracture. Since limitation of electron transparency requires a sample in the form of thin foil for TEM observations, it is impossible to extract such information directly from the fracture surfaces. In this study, the method of surface replication from the ceramic fracture surface is employed to characterize the process of crack propagation in ceramic matrix composites using TEM analysis. The surface replica from the fracture surface in ceramic materials provides detailed surface morphology and more importantly, loosened particles on the fracture surface are collected. Electron diffraction and chemical composition analyses of these particles reveal crack path in the specimen. Furthermore, one can determine the mode of fracture by observing the fracture surface morphology from the image of replica. Two examples are given to illustrate the potential of the surface replication technique. In the first example, apparent toughness increase in $B_{4}C-Al$ composites at high strain rate is investigated by surface replication to elucidate the mechanism of fracture at different strain rates. The polytypes of SiC formed during the sintering of SiC-AlN composite and their effect on the fracture behavior of SiC-AlN composite are analyzed in the second example.

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An Efficient Signal Processing Scheme Using Signal Compression for Software GPS Receivers

  • Cho Deuk-Jae;Lim Deok-Won;Park Chan-Sik;Lee Sang-Jeong
    • International Journal of Control, Automation, and Systems
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    • v.4 no.3
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    • pp.344-350
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    • 2006
  • The software GPS receivers based on the SDR technology provide the ability to easily adapt the other signal processing algorithms without changing or modifying the hardware of the GPS receiver. However, it is difficult to implement the software GPS receivers using a commercial processor because of the heavy computational burden for processing the GPS signals in real-time. This paper proposes an efficient GPS signal processing scheme to reduce the computational burden for processing the GPS signals in the software GPS receiver, which uses a fundamental notion compressing the replica signals and the encoded look-up table method to generate correlation values between GPS signals and replica signals. In this paper, it is explained that the computational burden of the proposed scheme is much smaller than that of the typical GPS signal processing scheme. Finally, the processing time of the proposed scheme is compared with that of the typical scheme, and the improvement in the aspect of the computational burden is also shown.

Structural Properties of Fibril-forming Segments of α-Synuclein

  • Yoon, Je-Seong;Park, Joon-Ho;Jang, Soon-Min;Lee, Kyung-Hee;Shin, Seo-Min
    • Bulletin of the Korean Chemical Society
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    • v.30 no.3
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    • pp.623-629
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    • 2009
  • We have performed replica-exchange molecular dynamics simulations on 41 residue peptide mainly composed of NAC (non A$\beta$ component) sequence in $\alpha$-Synuclein. To investigate conformational characteristics of intrinsically unstructured peptides, we carried out structural analysis on the ‘representative structures’ for ensemble of structures occurring at different temperatures. The secondary structure profile obtained from our simulations suggests that the NAC region of $\alpha$-synuclein can be divided into roughly three helical-like segments. It is found that the overall helix-turn-helix like topology is conserved even though the conformational fluctuations grow as the temperature increases. The coordinate-based and the distance-based representative structures exhibit noticeable differences at higher temperatures while they are similar at lower temperatures. It is found that structural variations for the coordinate-based representative structures are much larger, suggesting that distance-based representative structures provide more reliable information concerning characteristic features of intrinsically unstructured proteins. The present analysis also indicates that the conformational features of representative structures at high temperatures might be related to those in membrane or low pH environment.

Characterization of Microstructure on Porous Silicon Carbide Prepared by Polymer Replica Template Method (고분자 복제 템플릿 방법을 이용하여 제조된 다공성 탄화규소의 미세구조 특성)

  • Lee, Yoon Joo;Kim, Soo Ryong;Kim, Young Hee;Shin, Dong Geun;Won, Ji Yeon;Kwon, Woo Teck
    • Journal of the Korean Ceramic Society
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    • v.51 no.6
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    • pp.539-543
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    • 2014
  • Foam type porous silicon carbide ceramics were fabricated by a polymer replica method using polyurethane foam, carbon black, phenol resin, and silicon powder as raw materials. The influence of the C/Si mole ratio of the ceramic slurry and heat treatment temperature on the porous silicon carbide microstructure was investigated. To characterize the microstructure of porous silicon carbide ceramics, BET, bulk density, X-ray Powder Diffraction (XRD), and Scanning Electron Microscope (SEM) analyses were employed. The results revealed that the surface area of the porous silicon carbide ceramics decreases with increased heat treatment temperature and carbon content at the $2^{nd}$ heat treatment stage. The addition of carbon to the ceramic slurry, which was composed of phenol resin and silicon powder, enhanced the direct carbonization reaction of silicon. This is ascribed to a consequent decrease of the wetting angles of carbon to silicon with increasing heat treatment temperature.

The effect of electrolytes on the preparation of an extraction replica in 3 wt. % Si steel (3% Si 강의 추출복제시료제조에 미치는 전해액의 영향)

  • Park, Shin-Hwa;Kim, Jae-Kwan;Kim, Jae-Nam;An, Byung-Ryang;Lee, Do-Hyung
    • Applied Microscopy
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    • v.23 no.2
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    • pp.1-10
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    • 1993
  • The effect of electrolyte on the extraction replicas of the precipiates in 3% Si steel was investigated. Three Kinds of electrolyte, 2% Nital solution (2% nitric acid+methanol; acid solution),, Sodium Citrate solution (5% sodiumcitrate+1% KBr+0.5KI+$H_{2}O$; aqueous neutral solution) and 10% AA solution (10% acetylacetone+ 1% tetramethylammoniumchloride+methanol; non-aqueous neutral solution), were compared. The preciptiates in 3% Si steel were dissolved in 2% Nital, but they were not dissolved in the Sodium Citrate and 10% AA solution. In Sodium Citrate solution, however, large second artifacts were introduced during sample preparation. Therefore 10% AA solution was found to be most useful for the preparation of extraction replica. The electrolysis condition of a matrix and precipitates were also checked by the measurement of potential-current curve in 10% AA solution. The matrix was electrolyzed at -400mV with respect to SCE(Saturated Calomel Electrode). In contrats precipitates were electrolyzed above 300mV. Precipitates were respected to be stable in 10% AA solution in the range of $-380mV{\sim}-300mV$ usually used to prepare extraction replicas.

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A STUDY OF HYDRAULIC PROPERTIES IN A SINGLE FRACTURE WITH IN-PLANE HETEROGENEITY: AN EVALUATION USING OPTICAL MEASUREMENTS OF A TRANSPARENT REPLICA

  • Sawada, Atsushi;Sato, Hisashi
    • Nuclear Engineering and Technology
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    • v.42 no.1
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    • pp.9-16
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    • 2010
  • Experimental examinations for evaluating fracutres were conducted by using transparent replicas of a single fracture in order to obtain the fracture data to contribute to the methodlogy on how to improve the definitaion of representative parameter values used for a parallel plate fracture model. Quantitative aperture distribution and quantitative tracer concentration data at each point in time were obtained by measuring the attenuation of transmitted light through the fracture in high spatial resolution. the representative aperture values evaluated from the multiple different measurement methods, such as arithmetic mean of aperture distribution measured by the optical method, transport aperture evaluated from the tracer test, and average aperture evaluated from the fracture void volume measurement converged to a unique value that indicates the accuracy of this experimental study. The aperture data was employed for verifying the numerical simulation under the assuption of Local Cubic Law and showed that the calculated flow rate through the fracture is 10%-100% larger than hydraulic test results. The quantitative tracer concentration data is also very valuable for validating existing numerical code for advection dispersion transport in-plane heterogeneous fractures.