• Title/Summary/Keyword: reduction synthesis

Search Result 1,078, Processing Time 0.058 seconds

Squeal Noise Analysis and Reduction of Drum Brake Using Component Mode Synthesis (구분모드합성에 의한 드럼 브레이크 스퀼 소음 해석 및 저감)

  • Kim, Jin-Ho;Bae, Byung-Ju;Lee, Shi-Bok;Kim, Tae-Jong
    • Transactions of the Korean Society for Noise and Vibration Engineering
    • /
    • v.15 no.1 s.94
    • /
    • pp.72-80
    • /
    • 2005
  • Recent studies have dealt with brake squeal in terms of the coupled vibration of brake component parts. In this paper, we assemble the mode models derived from FE analysis of the individual components of the drum brake system into the system model by considering the friction interaction of the lining and drum at the interface. The validity of the component models are backed up by the experimental confirmation work. By scrutinizing the real parts of the complex eigen-values of the system, the unstable modes, which may be strong candidate sources of squeal noise, are identified. Mode participation factors are calculated to examine the modal coupling mechanism. The model predictions for the unstable frequencies pointed well the actual squeal noise frequencies measured through field test. Sensitivity analysis is also performed to identify parametric dependency trend of the unstable modes, which would indicate the direction for the squeal noise reduction design. Finally, reduction of the squeal noise tendency through shape modification is tried.

Production of (R)-Ethyl-4-Chloro-3-Hydroxybutanoate Using Saccharomyces cerevisiae YOL151W Reductase Immobilized onto Magnetic Microparticles

  • Choo, Jin Woo;Kim, Hyung Kwoun
    • Journal of Microbiology and Biotechnology
    • /
    • v.25 no.11
    • /
    • pp.1810-1818
    • /
    • 2015
  • For the synthesis of various pharmaceuticals, chiral alcohols are useful intermediates. Among them, (R)-ethyl-4-chloro-3-hydroxybutanoate ((R)-ECHB) is an important building block for the synthesis of L-carnitine. (R)-ECHB is produced from ethyl-4-chloro-3-oxobutanoate (ECOB) by a reductase-mediated, enantioselective reduction reaction. The Saccharomyces cerevisiae YOL151W reductase that is expressed in Escherichia coli cells exhibited an enantioselective reduction reaction toward ECOB. By virtue of the C-terminal His-tag, the YOL151W reductase was purified from the cell-free extract using Ni2+-NTA column chromatography and immobilized onto Ni2+-magnetic microparticles. The physical properties of the immobilized reductase (Imm-Red) were measured using electron microscopy, a magnetic property measurement system, and a zeta potential system; the average size of the particles was approximately 1 μm and the saturated magnetic value was 31.76 emu/g. A neodymium magnet was used to recover the immobilized enzyme within 2 min. The Imm-Red showed an optimum temperature at 45℃ and an optimum pH at 6.0. In addition, Bacillus megaterium glucose dehydrogenase (GDH) was produced in the E. coli cells and was used in the coupling reaction to regenerate the NADPH cofactor. The reduction/oxidation coupling reaction composed of the Imm-Red and GDH converted 20 mM ECOB exclusively into (R)-ECHB with an e.e.p value of 98%.

Synthesis of $\beta$-Sialon from Wando Pyrophyllite (완도납석으로 부터 $\beta$-Sialon의 합성)

  • 이홍림;신현곤
    • Journal of the Korean Ceramic Society
    • /
    • v.21 no.1
    • /
    • pp.5-10
    • /
    • 1984
  • $eta$-Sialon synthesis was investigated via the simulataneous reduction and nitriding of Wando pyrophyllite. When Wando pyrophyllite-graphite-$Si_3N_4$ seed mixture was heated at 135$0^{\circ}C$ for as long as 10 hours in 80% $N_2$-20%$H_2$ atomsphere $eta$-$Si_3N_4$ solid solution was mainly formed together with a small amount of $\alpha$-$Si_3N_4$ The value z of the forming $Si_{6-x}Al_2O_2N{8-z}$ was decreased with heating time.

  • PDF