• Journal of the Korean Ceramic Society
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• v.37 no.1
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• pp.1-5
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• 2000

Cathodoluminescence(CL) properties of ZnO:Zn green phosphor were investigated. ZnO:Zn phosphor was synthesized by varying reducing agents and firing temperatures. ZnS, charcoal and 5% H2 gas mixed with 95% N2 gas(5H2-95N2) were used as the reducing agent and atmosphere. The highest CL intensity of ZnO:Zn phosphor was observed under the condition of 5H2-95N2 atmosphere and firing temperature of 90$0^{\circ}C$ for 1h. Charocal and ZnO as reducing agents in the syntehsis of ZnO:Zn phosphor exhibited about 60% and 40%, respectively, of the CL intensity obtained with 5H2-95N2 atmosphere.

• Textile Coloration and Finishing
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• v.22 no.1
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• pp.51-60
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• 2010

This research works on the effects of drawing conditions on the physical properties of the drawn worsted yarns. The drawn worsted yarns were made by the yarn drawing system under various drawing conditions such as concentration of reducing agent, draw ratio, setting time of drawn yarn, and concentration of oxidizing agent. The drawn worsted yarns from 2/80Nm to 2/90Nm were obtained from 2/60Nm worsted yarns, the surface and cross-sectional shapes and tensile properties of these various specimens were measured and discussed with the various drawing conditions. The drawing of worsted yarn made constituent wool fiber scratched and made it changing to polygonal cross-sectional shape. The tenacity and modulus were increased with draw ratio and concentration of reducing agent. And tensile strain was increased with draw ratio, which decreased with concentration of reducing agent.

• Applied Chemistry for Engineering
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• v.17 no.5
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• pp.517-520
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• 2006

The leaching behaviors of zinc and manganese oxides of spent alkaline manganeses battery in sulfuric acid solution by using $H_{2}O_{2}$ as a reducing agent were investigated according to the concentration of $H_{2}SO_{4}$, temperature, reaction time, and the amount of $H_{2}O_{2}$. The experimental results of zinc and manganeses dissolution rates obtained without a reducing agent at 100 g/L solid/liquid ratio, 3.0 M $H_{2}SO_{4}$, $60^{\circ}C$ and 200 r.p.m. were 97.7% and 43.5%, respectively. On the other hand, zinc and manganeses dissolution rates obtained by adding 30 mL reducing agent at $60^{\circ}C$ were 99.6% and 97.1%, respectively. The addition of the reducing agent increased the leaching of manganese by two-fold compared to the absence of a reducing agent. In case of adding over 30 mL $H_{2}O_{2}$, however, the leaching rates of zinc and manganeses were independent of reducing agent amounts.

• Journal of the Korea institute for structural maintenance and inspection
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• v.24 no.3
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• pp.57-62
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• 2020

Among the sewage pipes installed in Korea, the length of concrete pipes exceeding 20 years is 66,334 km (42.5%). Deteriorated concrete sewer pipes need to be repaired due to the leakage of internal sewage, which causes problems such as sink holes by expanding the cavity around the pipeline. In this study, we tried to apply anti-washout underwater mortar with ultra rapid hardening cement and segregation reducing agent to sewage pipe repair. As a result of the setting time test, the final set time was delayed by up to 172% by incorporating segregation reducing agent. In the test for measuring the degree of mortar segregation in water, it was measured at pH 12 or less under all mixing conditions. In addition, the suspension amount was measured to be 50 mg / l or less to satisfy the KCI-AD102 standard by incorporating a segregation reducing agent. In terms of the average value of mortar compressive strength, by incorporating segregation reducing agent, the strength of the specimens produced in air was more than 80% of that of the specimens produced in water. Conversely, the bond strengths of the specimens produced in water were measured to be higher than those of the specimens produced in air. Water resistance was evaluated by measuring water absorption and water permeability. Water absorption and water permeability were reduced by 42.6% and 36.6%, respectively, by mixing segregation reducing agent.

• Journal of the Korean Ceramic Society
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• v.31 no.8
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• pp.893-901
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• 1994

In this study, AlN powder of fine particle size and of high purity was synthesized by the carbothermal reduction-nitridation of monodisperse, spherical Al(OH)3 which had been prepared by sol-gel method using Al(O-sec-C4H9)3 as the starting material. Depending on the mixing order and kinds of reducing agents, the optimum condition for the preparation of AlN was determined as follows. AlN single-phase was produced by the carbothermal reduction-nitridation of (1) Benzene-washed Al(OH)3 and the reducing agent, carbon, which was mixed in a ball mill: for 5 hours at 140$0^{\circ}C$ under NH3 atmosphere; (2) The mixture prepared by hydrolysis of alkoxide solution into which carbon had been dispersed beforehand: for 5 hours at 135$0^{\circ}C$ ; (3) Al(OH)3 Poly(furfuryl alcohol) composite powder: for 2.5 hours at 135$0^{\circ}C$; (4) The mixture of Al(OH)3 and polyacrylonitrile: for 5 hours at 140$0^{\circ}C$. Addition of CaF2 increased the nitridation rate when carbon or polyacrylonitrile was used as the reducing agent; but it had no effect on the nitridation rate when furfuryl alcohol was used as the reducing agent.

• Proceedings of the Korea Concrete Institute Conference
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• 2006.05b
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• pp.617-620
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• 2006

This study is related to comprehending performance for watertightness and crack control of concrete added with crack reducing agent concerning to high strength concrete mixs. It was confirmed that watertightness of concrete added with agent could be improved by evaluation absorption ratio, permeability ratio and pore size distribution of hardened concrete. As well resistance to crack resulted from shrinkage was transferred to better state by the addition of agent.

• Proceedings of the Korea Concrete Institute Conference
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• 2008.11a
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• pp.729-732
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• 2008

Naphthalenic admixture(PNS) has been widely used as main component of AE reducing agent among superplasticizers for concrete for a long time. However its noxiousness has been appointed because of formaldehyde compound applied during in synthetic process. In this study, AE reducing agent prepared using PNS and substituted-PNS agent(ECO-AEM) without formaldehyde compound added to concrete. For these agent, the basic performance of concrete and ecological affinity properties were evaluated and compared.

• Proceedings of the Korea Concrete Institute Conference
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• 2001.11a
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• pp.232-328
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• 2001

This paper investigates the influences of water content and viscosity agent on the bleeding of concrete. According to test results, fluidity shows decline tendency as water content decreases, and dosage of viscosity agent increases. PEO viscosity agent does not affect the air contents while, MC viscosity agent causes air loss. As for bleeding, bleeding decreases with decrease of water content. As dosage of viscosity agent increase, bleeding decreases, regardless of viscosity kinds. It is thought that viscosity agents have the favorable effect of reducing bleeding, if fluidity and air loss are improved.

• Proceedings of the Korea Concrete Institute Conference
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• 2006.05b
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• pp.157-160
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• 2006

Recently, trouble of sand supply is occurred according to exhaustion of natural sand resources. To solve this problem, sea sand and crushed sand are used. But, necessity of water reducing agent because quality of concrete that use sea sand and crushed sand is deteriorated. Therefore in this study was examined on the engineering properties of concrete with kind of fine aggregate and addition ratio of water reducing agents. As a result, compressive strength appeared similar standard regardless of kind of fine aggregate. Compressive strength, durability was similar in decrease of the unit water content by increase of addition ratio of the water reducing agent. Also, drying shrinkage resistivity was improved because the unit water content decreased.

• Proceedings of the Korea Concrete Institute Conference
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• 1991.04a
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• pp.15-18
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• 1991

This study is designed for analyze the concrete properties according to the over-dosage of AE water-reducing agent; is aimed to analyze the effect of slump, air content, compressive strength of concrete and for presenting the reference data on the practical use.