• Korean Journal of Materials Research
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• v.2 no.5
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• pp.343-352
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• 1992

The high temperature deformation behavior of microalloyed hot forging steels has been examined as a function of the temperature, the strain rate, and the alloying element by using high temperature compression test. The high temperature deformation mechanism, which was obtained by analyzing the flow stress-strain curve and microstructure, could be considered to dynamic recrystallization. The peak stress of Nb-V-Mo steel was more increased and the dynamic recrystallization of Nb-V-Mo steel was faster than those of Nb-V steel. The peak stress of 1.2Mn-0.09Nb steel was more increased and the dynamic recrystallization of 1.2Mn-0.09Nb was delayed a little bit than those of 1.0Mn-0.05Nb. The peak stress of C-Nb-V steel was more increased and the dynamic recrystallization of C-Nb-V steel was delayed than those of C-steel. The constitutive equation of high temperature deformation had a power law type. The grain size of dynamic recrystallization was refined as the Zener-Hollomon parameter was increased. The relation of the dynamic recrystallization grain size and Zener-Hollomon parameter could be quantified to power law.

• Transactions of Materials Processing
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• v.10 no.7
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• pp.573-578
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• 2001

The flow stress of 304 stainless steel during hot forming process were determined by conducting hot compression tests at the range of 1273 K∼1423 K and 0.05 /s∼2.0 /s as these are typical temperature and strain rate in hot forging operation. In this material, Dynamic recrystallization was found to be the major softening mechanism with this conditions as Previous studies. Based on the observed phenomena, a constitutive model of flow stress was assumed as a function of strain, strain rate, temperature. In the constitutive model, the effects of strain hardening and dynamic recrystallization were taken into consideration. A finite element method connected to constitutive model was performed to predict the dynamic recrystallization behaviors and also stress-strain curves in hot compression of 304 stainless steel.

• Transactions of Materials Processing
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• v.22 no.8
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• pp.450-455
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• 2013

In the current study, a new dynamic recrystallization model for predicting high temperature flow stress is developed based on a physical model and the mean field theory. In the model, the grain aggregate is assumed as a representative volume element to describe dynamic recrystallization. The flow stress and microstructure during dynamic recrystallization were calculated using three sub-models for work hardening, for nucleation and for growth. In the case of work hardening, a single parameter dislocation density model was used to calculate change of dislocation density and stress in the grains. For modeling nucleation, the nucleation criterion developed was based on the grain boundary bulge mechanism and a constant nucleation rate was assumed. Conventional rate theory was used for describing growth. The flow stress behavior of pure copper was investigated using the model and compared with experimental findings. Simulated results by cellular automata were used for validating the model.

• Transactions of Materials Processing
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• v.9 no.1
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• pp.80-87
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• 2000

The static softening behavior of SCM 440 could be characterized by the hot torsion test in the temperature ranges of 90$0^{\circ}C$~110$0^{\circ}C$and strain rate ranges of 0.05/sec~5/sec. Interrupted deformation was performed with 2 pass deformation in the pass strain ranges of 0.25$\varepsilon$p~3$\varepsilon$p and interrupted time ranges of 0.5~100sec. The dependences of process variables, pass strain ($\varepsilon$i), stain rate ($\varepsilon$), temperature (T) and interpass time (ti), on static recrystallization (SRX) and metadynamic recrystallization (MDRX)were individually predicted from the modified Avrami's equations, The dependence of pass strain on MDRX was neglectable. Comparison of the softening kinetics between MDRX and SRX showed that the rate of MDRX was more rapid than that of SRX for the same deformation variables. Controlled multipass deformations were performed using static and metadynamic recrystallization of SCM 440.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2000.10a
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• pp.29-32
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• 2000

The static and metadynamic recrystallization of non-heat treated medium carbon steel(Fe - 0.45wt.$\%C\;-\;0.6wt.\%Si\;-\;1.2wt.\%Mn\;-\;-0.12wt.\%Cr \;-\;0.1wt.\%V \;-\;0.017wt\%$.Ti) were studied by the torsion test in the strain rate range of 0.05 - 5 $sec^{-1}$, and in the temperature range of $900\;-\;1100\;^{\circ}C$. Interrupted deformation was performed with 2 pass deformation in the pass strain range of $0.25 {\varepsilon}_p(peak strain)\;and\;{\varepsilon}_p$, and in the interpass time range or 0.5 - 100 sec. The dependence or pass strain(${\varepsilon}_i$), strain rate( $\dot{\varepsilon}$ ), temperature(T), and interpass time($t_i$) on static recrystallization (SRX) and metadynamic recrystallization (MDRX) were predicted from the modified Avrami's equations respectively. Comparison of the softening kinetics between SRX and MDRX was indicated that the rate of MDRX was more rapid than that of SRX under the same deformation variables.

• Korean Journal of Materials Research
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• v.24 no.5
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• pp.229-235
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• 2014

In this paper, the effects of precipitates and Mn-solute atoms on the recrystallization behavior of an Al-Mn alloy was studied using micro-Vickers hardness, electrical conductivity measurements and optical microscopy. Various thermo-mechanical processes were designed to investigate the different morphologies, and the solute concentration, of Mn in the matrix. The results indicate that the recrystallization temperature, $T_R$ and time, $t_R$, are influenced by the amount of M-solute atoms in the matrix, and that the recrystallization microstructure is influenced by the amount of precipitates. Recrystallization in the Slow-Cooling specimen was rapid due to its low concentration of Mn-solute atoms, and the crystal-grain size was the smallest due to finely distributed precipitates. However, in the case of the No-Holding specimen, elongated grains were observed at the low annealing temperature and the largest recrystallized grains were observed at the high annealing temperatures (compared with Slow-Cooling and Base specimens) due to the high Mn-solute atoms in the matrix.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 1999.08a
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• pp.320-326
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• 1999

In the present investigation, recrystallization occurring during hot rolling of thick steel plate was predicted. The thermo-mechanical history of a material point was traced by the finite element method and the recrystallization was predicted by the Sellars equations. The investigation was performed for 4 different cases; two different pass schedules in conventional rolling and two different pass schedules in controller rolling. Variations of temperature, strain, strain rate and grain size were compared with each other. It was found out that the difference of grain size through thickness was more distinctive in the cases of controller rolling.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2004.05a
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• pp.174-177
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• 2004

The nickel-based alloy Nimonic 80A possesses strength, and corrosion, creep and oxidation resistance at high temperature. These products are used for aerospace, marine engineering and power generation, etc. The control of forging parameters such as strain, strain rate, temperature and holding time is important because the microstructure change in hot working affects the mechanical properties. It is necessary to understand the microstructure variation evolution. The microstructure change evolution occurs by recovery, recrystallization and grain growth phenomena. The dynamic recrystallization evolution has been studied in the temperature range $950-1250^{\circ}C$ and strain rate range $0.05-5s^{-1}$ using hot compression tests. The metadynamic recrystallization and grain growth evolution has been studied in the temperature range $950-1250^{\circ}C$ and strain rate range 0.05, $5s^{-1}$, holding time range 5, 10, 100, 600 sec using hot compression tests. Modeling equations are developed to represent the flow curve, recrystallized grain size, recrystallized fraction and grain growth phenomena by various tests. Parameters of modeling equation are expressed as a function of the Zener-Hollomon parameter. The modeling equation for grain growth is expressed as a function of initial grain size and holding time.

• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2006.09b
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• pp.1157-1158
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• 2006

Internally nitrided dilute W-Ti alloy specimens having a heavily deformed surface microstructure were prepared by a multi-step internal nitriding at 1573-2073 K. Primary nitriding below their recrystallization temperature induced a precipitation of ultrafine TiN particles. After secondary and tertiary nitriding, those precipitates grew into rod-like TiN with a length of 20-60 nm. The recrystallization temperature after nitriding was elevated above 2073 K. The yield strength at 1773 K obtained from nitrided W-0.5 mass% Ti alloy was about 5 times as large as that of the recrystallized specimen. DBTT of the nitrided alloys was about 373 K.

• Transactions of Materials Processing
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• v.6 no.2
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• pp.102-109
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• 1997

The multistage deformation and stress relaxation were carried out to investigate the strain induced precipitation by torsion tests in the range of 1000~80$0^{\circ}C$, 0.05~5/sec for V-microalloyed steel. The starting temperature and time for the initiation of precipitation were determined by stress relaxation tests. The distribution of precipitates increased, as the strain rate increased and the mean size of precipitates was found to be about 10~30nm. The precipitation starting time$(P_s)$ decreased with increasing strain rate and the amount of pre-strain. The effect of deformation conditions on the no-recrystallization temperature$(T_nr)$ was also determined in the multistage deformation. $T_nr$ Tnr decreased with increasing the strain and strain rate. In the controlled rolling simulation, grain refinement and precipitation hardening effects could be achieved by the alternative large pass strain at the latter half pass stage under the condition of low temperature and high strain rate.