• Transactions of the Korean Society of Mechanical Engineers A
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• v.24 no.7 s.178
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• pp.1817-1825
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• 2000

The purpose of this study is to examine the fracture toughness of the welded pipe from the viewpoint of FATT for the S38 and S42 steels used widely as the pipe material. Post weld heat treatment(PW HT) was carried out like following conditions: temperature of 67$0^{\circ}C$, I hour of holding time and cooling in furnace. Fracture toughness was obtained by measuring the crack opening displacement(COD) of the notched specimens over the range of temperature from -14$0^{\circ}C$ to -$25^{\circ}C$. Hardness values at fusion line near around were the highest and the microstructures at welded zone were coarsened. Regardless of the pipe materials, COD and temperature curves of the as-welds were moved toward higher temperature compared with those of the parents. However, COD and temperature curves of the PWHT specimens were positioned at lower temperature compared with those of the as-welds. The more heat input causes to decrease the COD values at the constant temperature. It was verified through the recrystallization treatment that PWHT was attributed to move toward lower temperature region considerably due to the improved plastic deformation at the same applied COD value of 0.3mm and softening effect. In case of the weldment of S38 steel, cleavage fracture was observed at -105$^{\circ}C$ unlike the structural steels, in which brittle fracture mode was generally shown at - 196$^{\circ}C$.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2004.08a
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• pp.63-71
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• 2004

Recently, a sheet forming process of Mg alloys is highlighted again due to increasing demand for Mg wrought alloys in the applications of casings of mobile electronics and outer-skins of light-weight transportation. Microstructure control is essential for the enhancement of workability and formability of Mg alloy sheets. In this research, AZ31 Mg alloy sheets were prepared by hot rolling process and the rolling condition dependency of the microstructure and texture evolution was studied by employing a conventional rolling mill as well as an asymmetric rolling mill. When rolled through multiple passes with a small reduction per pass, fine-grained and homogeneous microstructure evolved by repetitive dynamic and static recrystallization. With higher rolling temperature, dynamic recrystallization was initiated in lower reduction. However with increasing reduction per pass, deformation was locallized in band-like regions, which provided favorable nucleation sites f3r dynamic recrystallization. Through post annealing process, the microstructures could be transformed to more equiaxed and homogeneous grain structures. Textures of the rolled sheets were characterized by $\{0002\}$ basal plane textures and retained even after post annealing. On the other hand, asymmetrically rolled and subsequently annealed sheets exhibited unique annealing texture, where $\{0002\}$ orientation was rotated to some extent to the rolling direction and its intensity was reduced.

• Korean Journal of Metals and Materials
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• v.56 no.11
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• pp.779-786
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• 2018

There have been previous attempts to observe the occurrence of dynamic ferritic transformation at temperatures even above $Ae_3$ in a low-carbon steel, and not only in steels, but recently also in titanium alloys. In this study, a new approach is proposed that involves treating true stress-true strain curves in uniaxial compression tests at various temperatures, and different strain rates in 0.1C-6Ni steel, which is a model alloy used to decelerate the kinetics of ferrite transformation from austenite. The initial flow stress up to peak stress was used to analyze the change in dynamic softening phenomena, such as dynamic recovery, dynamic recrystallization, and dynamic transformation. It is worth mentioning that for predicting the occurrence of dynamic transformation, flow stress before reaching peak stress is much more sensitive to the change in the dynamic softening rate due to dynamic transformation, compared to peak stress. It was found that the occurrence of dynamic ferritic transformation could be successfully obtained even at temperatures above $Ae_3$ once the deformation condition was satisfied. This deformation condition is a function of both the strain rate and the deformation temperature, which can be described as the Zener - Hollomon parameter. In addition, the driving force of dynamic ferritic transformation might be much less than that of the dynamic recrystallization of austenite at a given deformation condition. By applying this technique, it is possible to predict the occurrence of dynamic transformation more sensitively compared with the previous analysis method using peak stress during deformation.

• Transactions of Materials Processing
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• v.32 no.5
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• pp.239-246
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• 2023

To reduce the forming load due to the temperature drop, during the hot forging process, a reheating hot forging process design is required that to repeat heating and forging. However, if the critical strain required for recrystallization is not induced during forging and grain growth becomes dominant due to the reduction in dislocation density due to repeated heating, the mechanical properties may deteriorate. Therefore, in this study, Inconel 706 alloy was applied, and the grain refinement behavior was comparatively analyzed according to the number of reheating times and effective strain during reheating hot forging process. Reheating was carried out with a total compression rate of 40% up to 4 times. The Inconel 706 compression test specimens heated once showed finer grains as the effective strain increased due to the dynamic recrystallization phenomenon. However, as the number of heating increases, grain refinement was observed even in a low effective strain distribution of 0.43 due to static recrystallization during reheating. Moreover, grain growth occurs at a relatively low effective strain of 0.43 when the number of reheating is four or more. Therefore, it was effective to apply an effective strain of 0.43 or more during hot forging to Inconel 706 in order to induce crystallization through grain refinement and improve the properties of forged products. In addition, we could notice that up to three reheating times condition was appropriate to prevent grain growth and maintain fine grain size.

• Analytical Science and Technology
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• v.9 no.2
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• pp.179-191
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• 1996

In order to understand the high temperature deformation behavior of superalloy 718, a rotating grade 718 alloy has been compression tested to about 0.7 upset ratio at $927{\sim}1066^{\circ}C$ temperature range and $5{\times}10^{-4}{\sim}5{\times}10^0sec^{-1}$ strain rate. The maximum flow stress was increased with increasing strain rate, and similar behavior was observed with decreasing temperature. At low temperature and high strain rates other than $5{\times}10^{-1}sec^{-1}$, strain softening was occurred mainly by dynamic recovery and deformation twinning processes, while at high temperature and low strain rates strain softening was offseted by dynamic recrystallization. At $5{\times}10^{-1}sec^{-1}$, strain hardening was occurred due to work hardening of the dynamic recrystallized grains. Strain rate sensitivity, m, was varied with strain rates. In the case of lower strain rate tests, m was measured as 0.3 and it was observed that the deformation was mainly controlled by dynamic recrystallization. At higher strain rate, m was lowered to 0.1 and the deformation was controlled by the dynamic recovery and the deformation twinning processes.

• YAKHAK HOEJI
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• v.40 no.3
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• pp.306-310
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• 1996

Five pseudopolymorphic modifications of cefazolin sodium were prepared by recrystallization. They were characterized by DSC and TGA. The solubilities of all modifications were c hecked through the dissolution test.

• Proceedings of the Korea Committee for Ocean Resources and Engineering Conference
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• 2003.10a
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• pp.100-105
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• 2003

25Cr-20Ni series strainless steel have an excellent high temperature strength, high oxidation and high corrosion resistance. However, further improvement can be creep strength by work hardening prior creep. In the present study, the effect of prestraining at room temperature on the creep behavior of a Class M(STS310S) and a Class A(STS310J1TB) alloy containing precipitates have been examined. Prestraining was carried out at room temperature and range of prestrain was $0.5{\sim}2.5$ % at STS310J1TB and $2.0{\sim}7.0$ % at STS310S. Creep behavior and creep rate of pre-strained specimens were compared with that of virgin specimens. Room temperature prestraining produced the creep life that is longer than that of a virgin specimen both for STS310J1TB and STS310S when creep test carried out at the temperature lower than recrystallization temperature. The reason for this improvement of creep life was ascribable to the interaction between dislocations and precipitates in addition to the dislocation-dislocation interaction in STS310J1TB and the dislocation-dislocation interaction in STS310S. The beneficial effect of prestraining in STS310J1TB was larger than that of STS310S.

• Transactions of Materials Processing
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• v.30 no.5
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• pp.219-225
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• 2021

When extruding Al6061 alloys, deformation energy is deposited inside the extruded alloy depending on the deformation and the temperature of extrusion. This creates a Peripheral Coarse Grain (PCG) on the surface, where relatively more deformation energy. of the extruded alloy has been accumulated. Furthermore, since the deformation of materials continues while the materials recrystallize, it is important to examine the effect of deformation energy on dynamic recrystallization in the process of extruding Al alloys along with their microstructure. Prior studies explain the theory behind PCG growth though quantitative analysis on PCG growth of Al alloys during extrusion processes has not yet been addressed. This study aims to measure the generated PCG thickness which determines the correlation between extrusion outlet temperature and its effect on mechanical properties. Surface structure observations were performed using Optical Microscope (OM) and mechanical properties were evaluated through tensile strength and hardness measurement. Throughout this study, we endevoured to find the optimum condition of extrusion exit temperature of Al6061 and confirmed improved d reliability. This study describes the effect of the complex process variables such as exit temperature on the thickness of PCG layer for the Al6061 alloy using the 200 tons extrusion press. We therefore, discovered that the PCG layer thickness was 117 ㎛ at temperatures between 460 ℃ to 520 ℃.

• Transactions of Materials Processing
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• v.15 no.7 s.88
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• pp.504-511
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• 2006

The drawability of AZ31B magnesium sheet is estimated at various temperatures($200,\;250,\;300,\;350\;and\;400^{\circ}C$), and forming speed(20, 50, 100mm/min), thickness(0.5, 0.8, 1.0, 1.4mm). The deep drawing process of circular cup and square cup were used in forming experiments. Experimental and FEM analysis are performed to investigate drawability and affection of controlled blank holding force. Through the controlled blank holding force, drawability was improved. Limit drawing ratio is increased from 2.1 to 3.0 in circular cup drawing and change of thickness is decreased from 16.3 to 6.9%. This result is verified by FEM analysis. Through the observation of microstructure, the main cause is investigated as a quantity of the dynamic recrystallization.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.30 no.4
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• pp.136-142
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• 2020

Crystallization of zinc crystalline glaze requires demanding conditions such as the formation of a nucleating agent and the amount of nucleating agent, and growth of crystalline. Zinc crystalline glaze is hard to utilize in the industry because of its narrow range of the firing temperature, and the crystallization's dependency on the quality of zinc. Stimulation of zinc crystallization and formation of frit enable zinc crystalline glaze to be reconstituted in a various range of firing schedules, leading to the development of a competitive industrial glaze.