• Title/Summary/Keyword: recovery of set

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Simultaneous Determination of Paeoniflorin and Glycyrrhizin in Sayuk-san by HPLC/DAD

  • Lee, Mi-Kyeong;Lee, Ki-Yong;Kim, Seung-Hyun;Jeon, Min-Ji;Cho, Jung-Hee;Oh, Mi-Hyun;Baek, Ju-Hyun;Kim, Hyo-Jin;Sung, Sang-Hyun
    • Journal of Pharmaceutical Investigation
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    • v.39 no.1
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    • pp.23-27
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    • 2009
  • A high performance liquid chromatographic (HPLC) method for the simultaneous determination of marker constituents, paeoniflorin and glycyrrhizin was established for the quality control of traditional herbal medicinal preparation, Sayuk-san (SYS). Separation and quantification were successfully achieved with a Waters XTerra RP18 column ($5{\mu}m$, $4.6mm\;I.D.{\times}150mm$) by gradient elution of a mixture of acetonitrile and water containing 0.03% phosphoric acid (pH 2.03) at a flow rate of 1.0 mL/min. The diode-array UV/vis detector (DAD) was used for the detection and the wavelength for quantification was set at 230 nm. The presence of paeoniflorin and glycyrrhizin in this decoction was ascertained by retention time, spiking with each authentic standard and UV spectrum. All two compounds showed good linearity ($r^2$>0.996) in a relatively wide concentration ranges. The R.S.D. for intra-day and inter-day precision was less than 7.3% and the limits of detection (LOD) were less than 55.7 ng. The mean recovery of each compound was $102.3{\sim}111.1%$ with R.S.D. values less than 4.6%. This method was successfully applied to the determination of contents of paeoniflorin and glycyrrhizin in three commercial products of SYS. These results suggest that the developed HPLC method is simple, effective and could be readily utilized as a quality control method for commercial SYS products.

Hardness and Dimensional Stability of Thermally Compressed Domestic Korean Pine (국내산 잣나무 열압밀화재의 경도와 치수안정성)

  • Hwang, Sung-Wook;Cho, Beom-Geun;Lee, Won-Hee
    • Journal of the Korean Wood Science and Technology
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    • v.43 no.1
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    • pp.68-75
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    • 2015
  • We conducted a thermal compression of domestic Korean pinewood for a use in flooring. For the evaluation of flooring material, we measured dimensional stability and surface hardness of thermally compressed wood. It is possible to make high-specific gravity woods with a range of 0.82-0.92 after the thermal compression with 50% compression set. The surface hardness increased with an increase in the pressing temperature. The highest value of surface hardness was $23.6N/mm^2$, which was obtained from the thermal compressed wood with pressing temperature of $160^{\circ}C$ and 30 minutes of pressing time. However, the surface hardness of woods treated at high temperature of $180^{\circ}C$ or greater decreased. The recovery of thickness decreased with increasing the pressing temperature. For dimensional stability, compression temperature was more dominant than compression time.

Optimization of VIGA Process Parameters for Power Characteristics of Fe-Si-Al-P Soft Magnetic Alloy using Machine Learning

  • Sung-Min, Kim;Eun-Ji, Cha;Do-Hun, Kwon;Sung-Uk, Hong;Yeon-Joo, Lee;Seok-Jae, Lee;Kee-Ahn, Lee;Hwi-Jun, Kim
    • Journal of Powder Materials
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    • v.29 no.6
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    • pp.459-467
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    • 2022
  • Soft magnetic powder materials are used throughout industries such as motors and power converters. When manufacturing Fe-based soft magnetic composites, the size and shape of the soft magnetic powder and the microstructure in the powder are closely related to the magnetic properties. In this study, Fe-Si-Al-P alloy powders were manufactured using various manufacturing process parameter sets, and the process parameters of the vacuum induction melt gas atomization process were set as melt temperature, atomization gas pressure, and gas flow rate. Process variable data that records are converted into 6 types of data for each powder recovery section. Process variable data that recorded minute changes were converted into 6 types of data and used as input variables. As output variables, a total of 6 types were designated by measuring the particle size, flowability, apparent density, and sphericity of the manufactured powders according to the process variable conditions. The sensitivity of the input and output variables was analyzed through the Pearson correlation coefficient, and a total of 6 powder characteristics were analyzed by artificial neural network model. The prediction results were compared with the results through linear regression analysis and response surface methodology, respectively.

A Concept for improving the Level of Autonomy of an LEO Satellite (저궤도 위성의 자율성 수준 향상을 위한 개념 제안)

  • Jeon, Moon-Jin;Kim, Eunghyun;Lim, Seong-Bin
    • Aerospace Engineering and Technology
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    • v.13 no.1
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    • pp.37-43
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    • 2014
  • The ground station which operates the LEO satellite performs monitoring state of health of the satellite, sending the commands for the imaging mission of receiving the images during about 10 minutes of contact time. To finish the planned procedure in limited contact time, specific level of autonomy is applied in the satellite and the ground system. For example, the attitude and orbit control logic has high level of autonomy because it must be operated alone for long period without operator intervention. On the other hand, the fault management logic has relatively low level of autonomy because of that failure detection and safing operation are performed on-board, whereas failure identification and recovery are on-ground operation. The level of autonomy of the satellite affects also the ground operation. The command set for mission operation is generated by ground system. If the satellite has higher level of autonomy, some of operation currently done on-ground can be performed on-board, so the ground operation can be simplified. In this paper, we discuss the level of autonomy and propose a concept for improving the level of autonomy of an LEO satellite.

Thoracoscopy as a safe and effective technique for exploring calves affected with bovine respiratory disease

  • Perez-Villalobos, Natividad;Espinosa-Crespo, Inaki;Sampayo-Cabrera, Jose;Gonzalez-Martin, Juan-Vicente;Gonzalez-Bulnes, Antonio;Astiz, Susana
    • Journal of Animal Science and Technology
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    • v.59 no.3
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    • pp.5.1-5.10
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    • 2017
  • Background: Bovine respiratory disease (BRD) is one of the leading causes of economic losses in the beef and dairy industry. Reliable antemortem tools for diagnosing BRD would improve the efficacy of treatment and reduce costs. Here we examined whether the relatively simple technique of thoracoscopy can support BRD diagnosis under field conditions. We also compared various equipment set-ups in order to optimize the safety and efficacy of the procedure. A total of 24 thoracoscopic procedures were performed in 17 calves diagnosed with BRD and in 2 healthy control calves. Rigid and flexible endoscopes and industrial videoscopes were tested using various insertion approaches. The suitability of the technique was assessed in terms of duration, volume of air extracted, visualization score, and image quality. Safety was assessed in terms of rectal temperature, body weight, breaths/min, presence of fibrinogen, pain score, recovery time, intraoperative complications and risk of laceration or threatening collapse. Results: Insertion of a flexible endoscope via a right, dorso-caudal approach at the $5^{th}$ intercostal space allowed complete examination of the right lung in 15 min, as well as identification of main lung lesions and adherences in calves with BRD, without compromising calf welfare. While the dorso-caudal approach was optimal, it was associated with substantial discomfort when rigid endoscopes were used, minimal complications or mortality due to thoracoscopy were observed up to 28 days after the procedure. Videoscopes were as safe and easy to use as endoscopes, but endoscopes provided better image quality. Conclusion: This study provides the first field evidence that thoracoscopy can be safe to explore BRD-diseased calves. These results justify a larger study to rigorously assess the diagnostic performance of the technique.

Evaluation of Physiological Responses and Comfort of Protective Clothing Using Charcoal Printing (숯 날염가공한 방호복의 인체생리반응 및 쾌적성 평가)

  • Chung Myung-Hee;Park Soon-Ja;Shin Jung-Sook;Koshiba Tomoko;Tamura Teruko
    • Journal of the Korean Society of Clothing and Textiles
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    • v.30 no.6 s.154
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    • pp.981-991
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    • 2006
  • The purpose of this study was to determine the practicability of an experimental protective clothing by identifying the human body's physiological responses to it as well as the human body's comfort level when wearing it, particularly with the use of a processed charcoal material. The experimental protective clothing came in two types: one whose outer side made use of polypropylene film, and the inner side, a non-woven rayon fabric; and one whose inner side made use of a non-woven fabric processed with charcoal with a 10% density. Experiments were conducted on five healthy adult women whose average age was 21. These experiments were conducted at a climatic chamber, in which the temperature and relative humidity were set below $28{\pm}1^{\circ}C\;and\;50{\pm}10%$, respectively, and were measured within a period of 60min, consisting of a 20-min rest period, a 20-min exercise period, and a 20-min recovery period. Based on the results of this study, the efficiency of the processed charcoal material was reviewed, and a database requiring the production of more functional and comfortable protective clothing materials was established.

Solving the Discrete Logarithm Problem for Ephemeral Keys in Chang and Chang Password Key Exchange Protocol

  • Padmavathy, R.;Bhagvati, Chakravarthy
    • Journal of Information Processing Systems
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    • v.6 no.3
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    • pp.335-346
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    • 2010
  • The present study investigates the difficulty of solving the mathematical problem, namely the DLP (Discrete Logarithm Problem) for ephemeral keys. The DLP is the basis for many public key cryptosystems. The ephemeral keys are used in such systems to ensure security. The DLP defined on a prime field $Z^*_p of random prime is considered in the present study. The most effective method to solve the DLP is the ICM (Index Calculus Method). In the present study, an efficient way of computing the DLP for ephemeral keys by using a new variant of the ICM when the factors of p-1 are known and small is proposed. The ICM has two steps, a pre-computation and an individual logarithm computation. The pre-computation step is to compute the logarithms of a subset of a group and the individual logarithm step is to find the DLP using the precomputed logarithms. Since the ephemeral keys are dynamic and change for every session, once the logarithms of a subset of a group are known, the DLP for the ephemeral key can be obtained using the individual logarithm step. Therefore, an efficient way of solving the individual logarithm step based on the newly proposed precomputation method is presented and the performance is analyzed using a comprehensive set of experiments. The ephemeral keys are also solved by using other methods, which are efficient on random primes, such as the Pohlig-Hellman method, the Van Oorschot method and the traditional individual logarithm step. The results are compared with the newly proposed individual logarithm step of the ICM. Also, the DLP of ephemeral keys used in a popular password key exchange protocol known as Chang and Chang are computed and reported to launch key recovery attack.

Performance Characteristics Under Non-Reacting Condition with Respect to Length of a Subscale Diffuser for High-Altitude Simulation (고고도 모사를 위한 축소형 디퓨저의 길이변화에 따른 비연소장에서의 성능특성)

  • Jeong, Bonggoo;Kim, Hong Jip;Jeon, Junsu;Ko, Youngsung;Han, Yeoung-Min
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.38 no.4
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    • pp.321-328
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    • 2014
  • The performance characteristics of a subscale diffuser under non-reacting conditions for high-altitude simulation were numerically investigated with respect to different lengths of the secondary throat diffuser. The ratio of the length of the diffuser entrance to the nozzle exit diameter was set to 0, 50, and 100%. In addition, flow characteristics were studied for a range of length-to-diameter ratios of the secondary throat diffuser. An insufficient diffuser entrance length caused contraction of the plume immediately after the nozzle exit. When the length-to-diameter ratio was less than 8, a strong Mach disk was formed inside the diffuser, resulting in a sharp increase in pressure. In addition, flow characteristics in the diverging part of the diffuser were investigated for a range of diverging part lengths. A short diverging part may lead to abrupt pressure recovery, resulting in the possible application of mechanical load to the diffuser.

Quantitative Analysis of Skarn Ore Using 3D Images of X-ray Computed Tomography (3차원 X-ray 단층 화상을 이용한 스카른 광석의 정량분석 연구)

  • Jeong, Mi-Hee;Cho, Sang-Ho;Jeong, Soo-Bok;Kim, Young-Hun;Park, Jai-Koo;Kaneko, Katsuhiko
    • Journal of the Mineralogical Society of Korea
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    • v.23 no.3
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    • pp.211-217
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    • 2010
  • A micro-focus X-ray computed tomography (CT) was employed to determine quantitative phase analysis of skarn Zn-Pb-Cu ore by nondestructive visualization of the internal mineral distribution of a skarn ore. The micro CT images of the ore were calibrated to remove beam hardening artifacts, and compared with its scanning electron microscope (SEM) images to set the threshold of CT number range covering sulfide ore minerals. The volume ratio of sulfide and gangue minerals was calculated 20.5% and 79.5%, respectively. The quantitative 3D X-ray CT could be applied to analyse the distribution of economic minerals and their recovery.

Residue Dissipation Patterns of Neonicotinoid Acetamiprid and Thiamethoxam in Swiss Chard for the Harvest Periods under Greenhouse Conditions (시설재배 근대 중 Neonicotinoid계 살충제 Acetamiprid 및 Thiamethoxam의 생산단계 잔류특성)

  • Chang, Hee-Ra;You, Jung-Sun;Do, Jung-Ah
    • Korean Journal of Environmental Agriculture
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    • v.37 no.2
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    • pp.97-103
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    • 2018
  • BACKGROUND: Dissipation of acetamiprid and thiamethoxam in greenhouse grown chard samples was evaluated at 5 intervals including the pre-harvest interval after application. This study was conducted to determine the residue levels, the biological half-lives and dissipation rate of acetamiprid and thiamethoxam in chard under controlled conditions. METHODS AND RESULTS: Acetamiprid and thiamethoxam were applied in accordance with good agricultural practices for chard. Chard samples were collected at 0, 1, 2, 3, 5, 7, 10 and 14 days after application. Quantitaion was performed by HPLC-DAD system with C18 column. Limit of quantification (LOQ) of acetamiprid and thiamethoxam were both 0.02 mg/kg for chard. The recovery of acetamiprid and thiamethoxam were 77.8~107.5% and 94.3~108.6% at two concentration levels. The half-lives of pesticide dissipation in chard for two fields were 11.9 and 8.2 days for acetamiprid and 3.6 and 3.3 days for thiamethoxam respectively. The dissipation rate of acetamiprid and thiamethoxam were estimated according to the statistics method with a 95% confidence. CONCLUSION: Dissipation of acetamiprid and thiamethoxam in chard were determined under greenhouse. The concentration of acetamiprid and thiamethoxam in chards at 0 days after application were below specified by Korean MRL. Dissipation rate constant will be useful to set the pre-harvest residue limit for public health and consumer protection.