• Title/Summary/Keyword: pulp properties

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Comparative Analysis of the Physical and Biochemical Properties of Light-cure Resin-modified Pulp Capping Materials

  • Tae Gyeom Kim;Jongsoo Kim;Joonhaeng Lee;Jisun Shin;Mi Ran Han;Jongbin Kim;Yujin Kim;Jae Hee Park
    • Journal of the korean academy of Pediatric Dentistry
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    • v.51 no.2
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    • pp.149-164
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    • 2024
  • This study compared the solubility, water absorption, dimensional stability, release of various ions (hydroxyl, calcium, sulfur, strontium, and silicon), and cytotoxicity of light-cured resin-modified pulp-capping materials. Resin-modified calcium hydroxide (Ultra-blendTM plus, UBP), light-cured resin-modified calcium silicate (TheraCal LCTM, TLC), and dual-cure resin-modified calcium silicate (TheraCal PTTM, TPT) were used. Each material was polymerized; solubility, 24-hour water absorption, and 30- day dimensional stability experiments were conducted to test its physical properties. Solubility was assessed according to the ISO 6876 standard, and 24 hours of water absorption, 30 days of dimensional stability were assessed by referring to the previous protocol respectively. Eluates at 3 and 24 hours and on 7, 14, and 28 days were analyzed according to the ISO 10993-12 standard. And the pH, Ion-releasing ability, cell proliferation rate, and cell viability were assessed using the eluates to evaluate biochemical characteristics. pH was measured with a pH meter and Ion-releasing ability was assessed using inductively coupled plasma atomic emission spectrometry (ICP-AES). Cell proliferation rate and cell viability were assessed using human dental pulp cells (hDPCs). The former was assessed by an absorbance assay using the CCK-8 solution, and the latter was assessed by Live and Dead staining. TPT exhibited lower solubility and water absorption than TLC. UBP and TPT demonstrated higher stability than TLC. The release of sulfur, strontium, calcium, and hydroxyl ions was higher for TLC and TPT than for UBP. The 28-day release of hydroxyl and silicon ions was similar for TLC and TPT. TLC alone exhibited a lower cell proliferation rate compared to the control group at a dilution ratio of 1 : 2 in cell proliferation and dead cells from Live and Dead assay evaluation. Thus, when using light-cure resin-modified pulp-capping materials, calcium silicate-based materials can be considered alternatives to calcium hydroxide-based materials. Moreover, when comparing physical and biochemical properties, TPT could be prioritized over TLC as the first choice.

The Development of Pulp Mold Tray for Melon Packaging (멜론 포장용 펄프몰드 난좌 개발)

  • Choi, Seung Ryul;Jung, Hoon;Choi, Dong Soo
    • KOREAN JOURNAL OF PACKAGING SCIENCE & TECHNOLOGY
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    • v.19 no.3
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    • pp.125-131
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    • 2013
  • In order to protect agricultural products against damage by physical load, various shock absorbing materials is used. As the demands of environment protection increase, the use of plastic materials have been restricted. On the other hand, Pulp mold products have some benefits - easy manufacturing, superior shock absorbing and eco-friendly. In order to develop pulp mold tray for melon packaging as shock absorbing packaging material, we investigated physical properties and vibration transmission characters of 180, 200 and 220 g pulp mold tray for melon. As the weight of pulp increased, compression strength and shock absorbing performance increased, while vibration transmissibility decreased. Especially in case of 180g pulp mold tray, it is not suitable for melon packaging because the transmitted vibration acceleration was higher than the forced vibration acceleration. And 200g pulp mold tray is suitable for melon packaging because the vibration transmissibility was lowest in three trays. And the vibration acceleration transmitted to the melon in edge of pulp mold tray was higher than to the melon in center of pulp mold tray. As the result of the simulated transportation test, the firmness of melon packaging using pulp mold tray was higher than that of conventional packaging. Therefore, these results suggest that pulp mold tray packaging could be suitable for melon packaging.

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Properties of Pectin Extracted from By-product in Citrus Processing (밀감 가공부산물에서 추출한 펙틴의 특성)

  • 박용곤;강윤한;차환수;김흥만;석호문
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.25 no.4
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    • pp.659-664
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    • 1996
  • The amount and characteristics of pectin in the albedo and flavedo layers of the citrus peels, and those of the pulp were investigated. Alcohol insoluble solid(AIS) content was the highest in albedo layer(18.1%), and the lowest in pulp(5.7%). The pulp and the albedo layer showed a potential pectin sources as containing pectins of 40.5% and 35.2% of the total polysaccharides of the pulp and the albedo layer, respectively. Total pectin contents were about 30% of the AIS and showed comparatively constant values among the byproducts. Hydrochloric acid soluble pectin contents were the hightest in the flavedo layer, 14.0%, and the lowest in the pulp, 4.4%. Over 90% of the total pectin could be extracted after 60min with 0.05N HCI at $85^{\circ}C.$ Microwave treatment reduced the extraction time significantly ; a comparable extraction yield was acquired after 10min with microwave treatment. The degree of esterification of the extracted pectin also increased with microwave treatment. Neutral sugars in the hydrolysate of the pectin were rhamnose, arabinose, galactose, glucose and xylose. No differences in molecular weight distribution of the pectin were found between the albedo and flavedo layers. Pectin of the pulp showed different molecular weight distribution from that of the peels.

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Analysis of Compression and Cushioning Behavior for Specific Molded Pulp Cushion

  • Jongmin Park;Gihyeong Im;Kyungseon Choi;Eunyoung Kim;Hyunmo Jung
    • KOREAN JOURNAL OF PACKAGING SCIENCE & TECHNOLOGY
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    • v.30 no.1
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    • pp.53-62
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    • 2024
  • Molded pulp products has become more attractive than traditional materials such as expanded polystyrene foam (EPS) owing to low-priced recycled paper, environmental benefits such as biodegradability, and low production cost. In this study, various design factors regarding compression and cushioning characteristics of the molded pulp cushion with truncated pyramid-shaped structural units were analyzed using a test specimen with multiple structural units. The adopted structural factors were the geometric shape, wall thickness, and depth of the structural unit. The relative humidity was set at two levels. We derived the cushion curve model of the target molded pulp cushion using the stress-energy methodology. The coefficient of determination was approximately 0.8, which was lower than that for EPS (0.98). The cushioning performance of the molded pulp cushion was affected more by the structural factors of the structural unit than by the material characteristics. Repeated impacts, higher static stress, and drop height decreased the cushioning performance. Its compression behavior was investigated in four stages: elastic, first buckling, sub-buckling, and densification. It had greater rigidity during initial deformation stages; then, during plastic deformation, the rigidity was greatly reduced. The compression behavior was influenced by structural factors such as the geometric shape and depth of the structural unit and environmental conditions, rather than material properties. The biggest difference in the compression and cushioning characteristics of molded pulp cushion compared to EPS is that it is greatly affected by structural factors, and in addition, strength and resilience are expected to decrease due to humidity and repetitive loads, so future research is needed.

Fiber Dimensions and Chemical Properties of Various Nonwood Materials and Their Suitability for Paper Production

  • lahan M. Sarwar;Mun Sung Phil;Rashid Mamunur
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.36 no.5 s.108
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    • pp.29-35
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    • 2004
  • Fiber dimensions, their derived values and chemical properties of cotton stalks (Gosypium hirsutum L), jute stick (Corchorus capsularis) and dhancha (Sesbania aculeate) have been examined to assess their suitability for paper production. Cotton stalks have a good derived values especially slender ratio, which is comparable to hardwood. The flexibility coefficient of these three non wood plants is better than hardwood. Anatomical analysis shows higher percentage of fibers and vessels than in general non wood plants. Lignin, $\alpha$-cellulose and pentosan contents in these three nonwood plants are within the range of hardwood. Neutral sugar analysis of cotton stalks, jute stick and dhancha shows that the glucose in the major sugar followed by xylose and mannose. The arabinose and galactose are present in minor amount. Alkaline nitrobenzene oxidation of cotton stalks, jute stick and dhancha wood meal exhibits that these nonwood plant lignins mainly consist of syringyl (S) and guaiacyl (V) units. The S/V ratios are 1.6, 1.2 and 2.1 for cotton stalks, jute stick and dhancha, respectively.

Characteristics of pre-extracted hemicelluloses from Korean mixed wood by hot water and alkali solution and its effect on handsheet properties (열수 및 알칼리 용액을 이용하여 국산 목재 칩으로부터 선추출한 헤미셀룰로오스의 특성과 이에 따른 수초지 물성 변화)

  • Seo, Dong-Il;Lee, Sang-Hoon;Sim, Kyu-Jeong;Lee, Hak-Lae;Youn, Hye-Jung
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.43 no.5
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    • pp.60-67
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    • 2011
  • Hemicelluloses pre-extracted from Korean mixed wood chip were investigated as a wet-end additive. Hemicelluloses dissolved in hot water and alkali solution were isolated by ethyl alcohol precipitation from pre-extractives. They showed molecular weight of 9,000 ~ 27,000 g/mol as revealed by size exclusion chromatography. The reduction of molecular weight through hot water extraction was caused by autohydrolysis. Chemical composition of the hemicelluloses were analyzed with high-performance liquid chromatography and UV-Vis spectroscopy. As the surface charge of isolated hemicelluloses were negative, the adsorption of hemicelluloses onto softwood unbleached kraft pulp fiber was promoted by poly-DADMAC. The physical properties of handsheets increased as the molecular weight of hemicellulose increased. On the other hands, the optical property decreased with hemicellulose adsorption.

Manufacture of Environmentally-friendly Flame-retardant Paper with Polyethylene Terephthalate (PET) Short Cut Fiber (PET 섬유를 사용한 친환경 난연지 제조방법에 대한 연구)

  • Kim, Ji-Seop;Lee, Myoung-Ku
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.44 no.5
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    • pp.14-20
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    • 2012
  • In this paper, the flame-retardant wall paper was successfully prepared with recycled polyethylene terephthalate (PET) short cut fiber with flame-retardant property and wood pulp using polyvinyl alcohol (PVA) as binder followed by treatment of non-halogen flame retardant. Physical properties such as formation index, tensile strength, elongation, and burst strength increased as defibrillation increased except tear strength. Bulk increased but formation index, tensile strength, elongation and burst strength decreased along with addition of PET short cut fiber. It was also found that tear strength rose significantly up to 30% of PET short cut fiber and then declined (fell) rapidly. As addition level of PVA increased tensile strength, elongation and burst strength increased, but tear strength decreased slightly. Addition of 20% of PET short cut fiber and 13% of PVA provided the flame-retardant wall paper with both improved flameproofing and physical properties.

New Korean Traditional Papermaking From Morus spp.(II) -Properties of the Hanjis Made from Bast Fiber and Whole Stalk Fiber- (뽕나무를 이용한 새로운 한지의 제조(제 2 보) -인피부 및 전간부 섬유.한지의 특성)

  • 최태호;조남석
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.31 no.4
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    • pp.84-92
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    • 1999
  • Excellence of the Korean traditional paper(Hanji) can be proved by literatures and legacies handed down from generations. However, with the problems pertaining to a majority of traditional manufactures, Hanji industry was declined because of low productivity, insufficient supply of raw material , and reduced demand. therefore, modernizxation of the Hanji technology and development of new uses are very important. This study was carried to investigated the papermaking characteristics of Morus spp.(M.alba, M.Bombycis, and M.Ihou) for new Hanji, modernize manufacturing process of Hanji by grafting on developed modern pulping and papermaking technology, develop the various uses, and establish the foundation for development of high value-added products. Hanji is made from M.Ihou, while stalk , and sulfomethylated pulp gave better sheet formation and higher brightness than those of the others. Physical properties of Hanji which made from bast fiber pulps were better than those of whole stalk pulps. Hanji which made from M.bombycis bast fiber and whole stalk pulps were not so good sheet strength as other species. Sulfomethylated whole stalk pulps were shown better sheet strength than alkali and alkali-hydrogen peroxide whole stalk pulps.

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High Consistency Pulping Treatment of Fractionated OCC Pulp for Improving Strength (강도 개선을 위한 분급된 OCC펄프의 고농도 펄핑 처리 기술)

  • Hur Young Dae;Lee Sang Gil;Lee Hak Lae;Youn Hye Jung
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.37 no.4 s.112
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    • pp.18-25
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    • 2005
  • The mechanical strength is the prime requisite for linerboard and corrugating mediums. Repeatedly recycled OCC fibers show less suitable property for papermaking mostly due to hornification and reduced fiber length. To overcome these problems many researches including fractionation, enzymatic treatment, and chemical or mechanical treatments of fibers have been carried out. In this study, the effect of mechanical treatment by high consistency pulping on the characteristics of recycled fibers as well as mechanical properties of sheets were investigated. Results on the strength properties of handsheets made of recycled fibers that were treated to same freeness level by beating and high consistency pulping, respectively, showed that beating treatment was more efficient in improving strength. Drainage and recycling potential of the fibers treated by high consistency pulping, however, were expected to be superior to beating because fines content and fiber length didn't change significantly.

Analysis of Effects of Fiber's Collapse Index on Physical Properties of Paper Using CLSM (종이의 물리적 특성에 미치는 섬유의 찌그러짐 특성의 영향에 대한 CLSM 분석)

  • 김서환;박종문;김철환
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.31 no.1
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    • pp.46-51
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    • 1999
  • The most important effect of refining is believed as the internal fibrillation. The internal fibrillation is the separation of the fiber wall into several lamellae. The internal fibrillation results in fiber swelling as water penetrates the fiber wall. The increase in paper strength as a result of refining was due to delamination which made the fiber more flexible. Pulp fibers are refined to 20, 40, and 70$^{\circ}$SR freeness at Valley beater. Changes of Physical paper properties are analyzed depending on fiber wall thickness and fiber's collapse index at 2.5 and 5.6kg$_f$ refining load. At same $^[\circ}$SR freeness with 2.5kg$_f$ refining load, fiber wall thickness is increased further than at high 5.6kg$_f$ refining load. With higher fiber wall thickness by lower intensity refining load, higher internal fibrillation, flexibility, collapsability of fibers are achieved. Those effects improve WRV, tensile strength, and burst strength. Tear strength shows opposite trend to tensile and burst strength as usual.

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