• Title/Summary/Keyword: preparation technique

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Liquefaction susceptibility of silty tailings under monotonic triaxial tests in nearly saturated conditions

  • Gianluca Bella;Guido Musso
    • Geomechanics and Engineering
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    • v.36 no.3
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    • pp.247-258
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    • 2024
  • Tailings are waste materials of mining operations, consisting of a mixture of clay, silt, sand with a high content of unrecoverable metals, process water, and chemical reagents. They are usually discharged as slurry into the storage area retained by dams or earth embankments. Poor knowledge of the hydro-mechanical behaviour of tailings has often resulted in a high rate of failures in which static liquefaction has been widely recognized as one of the major causes of dam collapse. Many studies have dealt with the static liquefaction of coarse soils in saturated conditions. This research provides an extension to the case of silty tailings in unsaturated conditions. The static liquefaction resistance was evaluated in terms of stress-strain behavior by means of monotonic triaxial tests. Its dependency on the preparation method, the volumetric water content, the void ratio, and the degree of saturation was studied and compared with literature data. The static liquefaction response was proved to be dependent mainly on the preparation technique and degree of saturation that, in turn, controls the excess of pore pressure whose leading role is investigated by means of the relationship between the -B Skempton parameter and the degree of saturation. A preliminary interpretation of the static liquefaction response of Stava tailings is also provided within the Critical State framework.

A New Sample Preparation Technique for SEM Observation of Polyolefin Microstructure (주사전자현미경상에서의 고분자 미세구조 관찰)

  • Park, Je-Myung
    • Applied Microscopy
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    • v.29 no.4
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    • pp.405-415
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    • 1999
  • In general, transmission electron microscopy (TEM) is usually used in the investigation of polymer microstructure. Microtoming, solution casting, staining and carbon replica method are frequently introduced to the study of the polymer morphology with TEM, however the sample preparation procedure of those techniques is very difficult, and it takes a long time. The purpose of this study is to develop a new sample preparation technique which is suitable for the investigation of the various shapes and species of polyolefin microstructure by scanning electron microscopy (SEM). By modifying the conventional chemical etching method, we developed a new chemical etching technique and sample preparation procedure that are suitable for SEM study of polymer microstructure. In this study the permanganate etching method is introduced and the optimum etching condition are determined by simply adjusting the etchant formulation, concentration and etching time. This technique has shown good reproducibility and it's morphological results agree well with other works on various types of microstructures such as spherulite characterization of isotatic polypropylene $(\alpha/\beta)$, polyethylene and poly-propylene copolymer characterization, and the study of lamellar growth pattern of unsheared or oriented materials. This technique has also been applied to the industrial fields for characterization of the polyolefin film, automobile products and the others.

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The latest development in the preparation of indium phosphide (InP) poly- crystals and single crystals

  • Guohao Ren;Kyoon Choi;Eui-Seok Choi;Myung-Hwan Oh
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.13 no.5
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    • pp.222-229
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    • 2003
  • InP crystal is an increasingly important semiconductor material in the application of long-wave optoelectronic and high frequency devices. The equilibrium vapor pressure of phosphorus at the melting point of InP is so high that the synthesis process is very difficult. Liquid-encapsulated Czochralski (LEC) pulling from the melt at high pressure is a generally favored technique to grow InP single crystals. This technique involves two steps: the synthesis of polycrystalline powder and the growth of single crystal from the melt at high pressure. This article reviewed the latest development in the preparation of InP crystal and the evaluation on the crystal quality.

Mineral Separation and Sample Preparation Methods Efficient for Subgrain Zircon Analyses (저어콘 아입자분석을 위한 효율적인 광물분리 및 시료준비 방법)

  • 조등룡
    • The Journal of the Petrological Society of Korea
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    • v.13 no.3
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    • pp.126-132
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    • 2004
  • This study provides detailed sample preparation methods for subgrain zircon analyses, and a simple mineral separation technique which overflows light mineral grains out of beaker using the running water from faucet. Excluding separation steps using of the Wilfley table and heavy liquid, this technique is faster and more efficient than conventional one, and remarkably suitable for collecting small amount of zircon for subgrain analyses.

Dielectric Properties of Amorphous and Composite Alkoxi-derived Alumina Thin Films

  • N., Korobova;Soh, Dea-Wha
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2003.07b
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    • pp.772-775
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    • 2003
  • The development of new improved type of dielectric materials on the conception of multiphase structure has been carried out in this paper. Metal alkoxides solutions were used for application of thin film by electrophoretic deposition technique. We succeeded in preparation of amorphous and composite dielectric films from Al alkoxides. Specific features of the preparation technique were considered. Microstructure of the films was examined as well as their dielectric properties. TEM analyses reveals that films deposited from aging sols and heat-treated at temperatures as low as $400^{\circ}C$ contain small whiskers of ${\delta}-Al_2O_3$.

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A STUDY ON CLINICAL APPLICATION OF ENAC ULTRASONIC ROOT CANEL INSTRUMENT (초음파 근관형성기구 ENAC의 임상적 응용에 관한 연구)

  • Lee, Chung-Sik
    • Restorative Dentistry and Endodontics
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    • v.13 no.1
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    • pp.181-184
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    • 1988
  • The purpose of this study was to evaluate the efficacy and safety of ultrasonic root canal preparation technique. 55 patients treated by each of the two techniques - ultrasonic and, hand - were evaluated the complications of two root canal preparation techniques. The results were as follows: 1. There was no difference in the pain incidence between the two groups. 2. There was no formation of performation and ledge in the ultrasonic group. 3. There was no difference in the shortening of working length between the two groups.

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