• Title/Summary/Keyword: pre-treatment condition

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Thermal Characteristics Analysis of Pre-Treated Rayon Fibers for Preparing Activated Carbon Fibers (활성탄소섬유 제조시 전처리된 레이온 섬유의 열특성 분석)

  • Choi, Sang Seun;Lee, Soon Hong
    • Journal of the Korean Society of Safety
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    • v.29 no.4
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    • pp.61-72
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    • 2014
  • The aim of this study is to define the condition of optimal pre-treatment for preferable activated carbon fibers (ACFs), which are based on rayon fibers. This paper shows the ideal path of ACFs preparation process; implies that rayon fibers are pre-treated by various solvents with different times before the heating process. The pre-treated rayon fibers finally turned into desirable rayon fiber-based ACFs through optimal pre-treatment condition by heating processes. The thermal analysis method of pre-treated rayon fibers by thermo-gravimetry analyser (TGA) is an idealized tool, which analyzes the best thermal condition of pre-treatment process. Surface morphologies of resulting rayon fibers based ACFs were examined by scanning electron microscope(SEM). The results of TGA and SEM analyses show that the optimal pre-treatment condition for preparing ACFs was clearly defined, in terms of thermal stability and surface morphology.

A Study on the Opimization of Process and Operation Condition for Membrane System in Tap Water Treatment (분리막을 이용한 정수처리 System에서 처리공정 및 운전조건의 최적화에 관한연구)

  • 오중교
    • Membrane Journal
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    • v.9 no.4
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    • pp.193-201
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    • 1999
  • The object of study were the development of membrane process and the optimization of operation condition for membrane system, which was used the pre-treatment system of tap water treatment in steady of conventional process such as coagulation, sedimentation. The higher steady flux is very important factor, by a suitable pre-treatment and optimization of operating condition such as fouling control, crossflow and backwashing method, in membrane system. So, we were observed the effect of flux decline for membrane used by 4 type ultrafiltration(UF) membrane pre-treatment process, and optimized the operation condition of filtration system under various MWCO(Molecular weight cut-off), operation pressure, linear velocity and temperature to maintain higher flux. From these experiment, we were identified that UF process showed a slower flux decline rate and a higher flux recovery than microfiltration(MF) membrane. The water quality of UF permeate was better than that of MF, and was not effected pre-treatment process. In the operation condition, the rate of flux decline was diminished by a higher linear velocity and operation temperature, lower pressure.

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Study on the Improvement of Adhesion between Cu Laminate and PSR (동박과 PSR간의 접합력 향상에 관한 연구)

  • 김경섭;정승부;신영의
    • Journal of Welding and Joining
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    • v.17 no.2
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    • pp.61-65
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    • 1999
  • Because of the need for packages which accommodate high pin count, high density and high speed device, PBGA(plastic ball grid array) package gets more spotlight. But the substrate material which is used for PBGA package is in nature susceptible to moisture penetration. The objective of the study is to find out the path of delamination in the stacked structure of substrate. To increase the adhesion between the cooper laminate and PSR(photo solder resist) which is the weakest part, experiments were performed by changing parameters of printing pre-treatment and post-treatment process. As a result of experiments, the factor effects on the adhesion between the cooper laminate and PSR is caused by all of the pre-treatment and post-treatment condition. A considerable change was observed depending on the amount of UV irradiation after thermal cure which is typical of printing post-treatment condition rather than pre-treatment condition.

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Enhanced of Bio-Hydrogen Production from Microalgae by Thermal Pre-Treatment (열처리를 통한 미세조류로부터 바이오수소 생산 향상)

  • Lee, Chaeyoung;Choi, Jaemin
    • Transactions of the Korean hydrogen and new energy society
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    • v.24 no.4
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    • pp.275-281
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    • 2013
  • This study was conducted to increase the amount of bio-hydrogen production from microalgae(Chlorella vulgaris) in batch reactors by thermal pre-treatment. The optimization of thermal pre-treatment was conducted using statistic experimental design of response surface methodology. Two experimental parameters of temperature and reaction time were considered. The optimization condition was founded at the coded variables of <0.52, -0.07> corresponding to the experimental of heating temperature of $95.6^{\circ}C$ and reaction time of 57.9 min, respectively. Under the optimal condition, the maximum hydrogen production was predicted to 25.3mL $H_2/g$ dry cell weight (dcw), which was 9.1 times higher value of control(2.8mL $H_2/g$ dcw).

Effect of Pre-treatment Method on Reactivity of WGS Catalyst for SEWGS System (SEWGS 시스템을 위한 WGS 촉매의 반응성에 미치는 수소 전 처리 방법의 영향)

  • Ryu, Hojung;Park, Jihye;Lee, Dongho;Shun, Dowon;Rhee, Youngwoo
    • Transactions of the Korean hydrogen and new energy society
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    • v.25 no.4
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    • pp.355-363
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    • 2014
  • Thermal shock or overheating of WGS catalyst for SEWGS system during hydrogen pre-treatment can cause reactivity decay of the catalyst. To select appropriate pre-treatment condition, temperature profiles of catalyst bed (or outside fluidized particle bed of bed insert) during pre-treatment were measured and then CO conversions of those catalysts during WGS reaction were also measured and compared. Drastic overheating of catalyst took place when we reduce catalyst at fixed bed condition and these catalysts showed low CO conversion during WGS reaction. On the contrary, there was no overheating of catalyst at fluidized bed condition not only physical mixing case but also bed insert case. Spring type bed insert showed acceptable CO conversion even at low WGS content. Consequently, feasibility of high CO conversion without decay of reactivity of catalyst and holding the WGS catalyst inside the SEWGS reactor as tablet shape were confirmed using spring type bed insert.

Study on pre-bonding according with HF pre-treatment conditions in Si wafer direct bonding (실리콘기판 직접접합에 있어서 HF 전처리 조건에 따른 초기접합에 관한 연구)

  • 강경두;박진성;정수태;주병권;정귀상
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1999.05a
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    • pp.370-373
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    • 1999
  • Si direct bonding (SDB) technology is very attractive for both Si-on-insulator(SOI) electric devices and MEMS applications because of its stress free structure and stability. This paper presents on- pre treatment conditions in Si wafer direct bonding, The paper resents on pre-bonding according to HF pre-treatment conditions in Si wafer direct bonding. The characteristics of bonded sample were measured under different bonding conditions of HF concentration, applied pressure and annealing temperature(200~ 100$0^{\circ}C$) after pre-bonding. The bonding strength was evaluated by tensile strength method. The bonded interface and the void were analyzed by using SEM and IR camera, respectively, Components existed in the interlayer were analyzed by using FT-IR. The bond strength depends on the HF pre-treatment condition before pre-bonding(Min 2.4kgf/$\textrm{cm}^2$~ Max : 14.kgf/$\textrm{cm}^2$)

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Effects of Storage Duration with Low Temperature and Wet Condition, Germination Temperature and Shading Rate on Germination of Aruncus dioicus var. kamtschaticus Seeds (저온습윤 저장기간, 발아온도 및 차광율이 눈개승마 종자의 발아에 미치는 영향)

  • Song, Ki Seon;Jeon, Kwon Seok;Choi, Kyu Seong;Kim, Chang Hwan;Park, Yong Bae;Kim, Jong Jin
    • Korean Journal of Medicinal Crop Science
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    • v.23 no.5
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    • pp.370-378
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    • 2015
  • Background : Aruncus dioicus var. kamtschaticus, functional wild vegetable, is perennial herb and young leaves with soft texture are generally used as edible food. So the demand for the vegetable has increased recently. This study was carried out to determine the effects of temperature and shading on germination characteristics of A. dioicus. Methods and Results : The experiment was performed by temperature and shading treatments. Seed pre-treatment before the germination experiment was carried out by the storage in low temperature ($4^{\circ}C$) under wet condition (LTW) for 0, 15, 30, 45 and 60 days and shading treatment were 35%, 50%, and 75% under control, BA (6-benzyladenine) and $GA_3$ (gibberellic acid) condition for 24 hours. Increasing the length of the storage periods led to increases seed germination percent in low temperature ($4^{\circ}C$) under wet condition (LTW), germination rate of A. dioicus seed was the highest at $15^{\circ}C$ with 60 days of seed pre-treatment. In the case of seeds pre-treatment with LTW, the more temperature went up, the more days to 50% of Germination of Final Germination Rate ($T_{50}$) went down. As a result of surveying shading treatment, germination rate was the highest in control of 35% shading and the next higher was in control of 50% shading. Conclusions : It is concluded that the temperature and shading are important factors to produce A. dioicus. Also, We suggest these results as basic data of A. dioicus for sexual propagation.

Effect of Strain Rate and Pre-strain on Tensile Properties of Heat-treated A5082 and A6060 Aluminium Wrought Alloys (열처리한 A5082와 A6060합금의 인장특성에 미치는 변형율속도 및 예비변형율의 영향)

  • Lee, Choongdo
    • Journal of the Korean Society for Heat Treatment
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    • v.33 no.4
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    • pp.161-172
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    • 2020
  • The tensile property of A5082 and A6060 aluminium wrought alloys was investigated, in terms of the strain rate sensitivity on alloy conditions by heat treatment and bake hardenability on pre-strain prior to strain ageing. The tensile test was carried out in a range of strain rate of 4.17 × 10-5 s-1 ~ 4.17 × 10-5 s-1 in room temperature and the nominal range of pre-strain was 3.0 ~ 10.5%. The tensile deformation of A5082 alloys is characterized as typical case of dynamic strain ageing with negative strain rate sensitivity for all conditions, and the tensile strength indicates a similar level regardless of alloy conditions, except only in full annealed condition. The stress-relief annealing on A6060 alloys can induce practical decrease in strength level of over approximately 100 MPa without any ductility loss, compared to as-rolled condition, while a full annealed and aged condition leads remarkable strengthening effect with the decrease of tensile elongation. Additionally, the bake hardenability of A5082 alloy by strain ageing indicates a negative dependence upon the increase of pre-strain, while A6060 alloy exhibits a positive sign even in low level relatively compared with conventional SPCC.

Influence of Cotton Pre-Treatment on Dyeing with Rubia cordifolia extracts for Cotton (면의 전처리 방법이 Rubia cordifolia 추출물의 염색성에 미치는 영향)

  • Bum Hoon Lee
    • Textile Coloration and Finishing
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    • v.35 no.1
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    • pp.1-7
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    • 2023
  • In this study, the influence of pre-treatment(bleaching, mercerization by liquid ammonia and caustic soda) on cotton fabrics were investigated on dyeing Rubia cordifolia extracts. Aluminium Sulfate, Iron(Ⅱ) Sulfate Heptahydrate, Copper(Ⅱ) Sulfate Pentahydrate, Tin(Ⅱ) Sulfate, Manganese(Ⅱ) Chloride Tetrahydrate were used as mordanting agents. K/S value and washing fastnesses of the dyed cotton fabrics pretreated under different conditions were investigated. The K/S values were increased in the order of bleaching, liquid ammonia and mercerization pre-treatment. It was found that the pre-treatment conditions did not significantly affect the color change. The colorfastness to washing of most of all dyed fabrics were over grade 4 regardless of pre-treatment condition.

A Pre-treatment Process for Natural Dyeing of Wool to Impar t Durable Antimicrobial Efficacy

  • Raja, A.S.M.;Thilagavathi, G.
    • Textile Coloration and Finishing
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    • v.23 no.2
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    • pp.69-75
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    • 2011
  • A pre-treatment process has been developed for natural dyeing of wool by which the dyed materials have been imparted antimicrobial efficacy against both gram-positive and gram-negative bacteria durable up to 20 washes. In this process, wool fabrics were treated with citric acid under oxidizing condition prior to dyeing. The treated fabrics were then dyed with four different types of natural dye powders obtained from leaves of silver oak, wattle, tanner's senna and flame of forest. All the natural dyes produced yellowish brown colour on wool fabrics. The washing and light fastness properties of the fabrics subjected to pre-treatment were one grade higher compared to those of the dyed fabrics without pre-treatment. The pre-treated wool fabrics showed antimicrobial efficacy against both gram-positive bacteria (Staphylococcus aureus) and gram-negative bacteria (Escherichia coli). The fabrics dyed without pre-treatment showed antimicrobial efficacy against gram-positive bacteria (Staphylococcus aureus) only. The durability of antimicrobial efficacy was higher in pre-treated and dyed wool fabrics compared to the dyed fabrics without pre-treatment.