• Title/Summary/Keyword: powder-in-tube

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Preform Design for the Sinter-forging Process of Arc-shaped Powdered Magnets (원호 형상을 가지는 분말자석 단조성형공정에서의 예비성형체 설계)

  • Kim, Seung-Ho;Lee, Choong-Ho;Huh, Hoon
    • Transactions of Materials Processing
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    • v.8 no.2
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    • pp.135-142
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    • 1999
  • Tube Process(TP) is one of the processes to produce permanent magnets. Advantage claimed for this process is that it can accmplish both densification and anisotropication in one step forming. This process is distinguished from other processes since it uses deformable tube for densification of powder magnets. TP has, however, difficulties in manufacturing permanent magnets from Nd-Fe-B green powder due to folding resulted from large height reduction and localized densification. Therefore, an adequate preform is necessary to reduce folding resulted from large height reduction and localized densification. Therefore, an adequate preform is necessary to reduce folding, lead magnets into almost desired final shape and get uniform densification. In this paper, preform design for TP is carried out without a deformable tube to investigate the behaviour of magnet sinter-forging. Preform design is accomplished to increase the effective magnet area with a near net shape and uniform densification.

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The Preparation of Bi-2223 Superconducting Powder and Tape by Emulsion Drying Method (에멀젼 건조법에 의한 Bi-2223 초전도 분말과 테이프 제조)

  • 장중철;이응상;이희균;홍계원
    • Journal of the Korean Ceramic Society
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    • v.34 no.2
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    • pp.115-122
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    • 1997
  • The powder preparation by using emulsion drying method, one of the chemical powder fabrication methods has the advantages; easy to control the chemical stoichiometry and to fabricate homogeneously fine particles. In the present study, the initial morphology and size distribution of the powder fabricated by using emulsion dry-ing method were controlled and were improved the homogeneity. By carefully controlling the mixing ratio of oil phase and aqueous solution and surfactant of preventing emulsion separation, the Bi(Pb)-Sr-Ca-Cu-O su-perconducting powders were prepared. The properties of the superconducting powder fabricated by this method and the microstructures and superconducting properties of the pelletized samples were investigated. The microstructures and electric properties of the tapes prepared by oxide powder-in-tube method were in-vestigated. The fabricated powder was spherical with less than 1$\mu$m but most of them was agglomerated with 2~5$\mu$m in size. The critical temperature of the pelletized sample annealed at 84$0^{\circ}C$ for 72 hours in oxygen par-tial pressure of 1/13atm in Ar atmosphere was 108K. And the critical current of the first and second annealed tapes in air prepared by oxide powder-in-tube process were 0.4A and 1.5A, respectively.

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Experimental performance investigation of compound parabolic cavity receiver having single absorber tube

  • Omar Al-Nabhani;Saud Al-Kalbani;Azzam Al-Alawi;Afzal Husain
    • Advances in Energy Research
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    • v.8 no.3
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    • pp.155-163
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    • 2022
  • The current study presents experimental research on a parabolic trough collector with tube and cavity receivers. The primary concentrating parabolic reflector is designed for an aperture area of 2×2 m2 with mirror-polished stainless steel sheet reflectors. The cavity receiver consists of a compound parabolic secondary reflector and a copper tube. Both the conventional tube receiver and the cavity receiver tube are coated with black powder. The experiments are carried out to compare the efficiency of the cavity receiver with the tube receiver for fluid temperature rise, thermal efficiency, and overall losses. The experiments showed significantly higher fluid temperature rise and overall efficiency and lower thermal losses for the cavity receiver compared to the tube receiver within the parameters explored in this study.

Manufacture of Precsion Model Using Laser Melting Process (레이저 용융 적층 공정을 이용한 정밀 형상 제작)

  • 김재도;전병철;권택열;이영곤;신동훈
    • Laser Solutions
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    • v.3 no.3
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    • pp.21-29
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    • 2000
  • For the direct metal shape processing the powder feed device which is different from the widely used in rapid prototyping. is developed, The three dimensional object is shaped with the melting metal powder. The developed research has applied to rapid prototyping in ultraprecision for MEMS and medical science fields required of rapid manufacture of complex shape. The goal of this study make 3D model which has precision accuracy. Powder spreading apparatus has been more improved because that the control of powder spread is very important in layer manufacturing. It consists of the vibration motor, nozzle and tube which supplies various metal powder. This apparatus could control the spreading velocity that could control powder spreading thickness. Laser on/off switch was adapted because laser scanning velocity must be preserved constantly to prevent heat transformation of laser overheating. The error between sintered thickness md experimental one occurred by shrinkage in sintering melting process. The problem of heat transformation was solved by On/Off switching system.

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Powder Characteristics of $n-TiO_2$ Powder Synthesized by Chemical Vapor Synthesis (화학기상합성에 의해 제조된 $n-TiO_2$ 분말의 분말특성)

  • 김혜경
    • Journal of Powder Materials
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    • v.6 no.3
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    • pp.238-245
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    • 1999
  • The preparation of $n-TiO_2$ powder by the Chemical Vapor Synthesis process (CVS) was studied using the liquid metal organic precursor (TTIP). The residence time and the collection methods were considered as main processing variables through the experiments. The CVS equipment consisted of a micropump and a flashvaporizer, a tube furnace and a tubular collection device. The synthesis was performed at $1000^{\circ}C$ with various sets of collection zone. The residence time and the total system pressure were controlled in the range of 3~20 ms and 10 mbar, respectively. Nitrogen adsorption, X-ray diffraction and electron microscopy were used to determine particle size, specific surface area and crystallographic structure. The grain size of the as-prepared $n-TiO_2$ powder was in the range of 2~8 nm for all synthesis parameters and the powder exhibited only little agglomeration. The relationship between particle characteristics and the processing variables is reviewed based on simple growth model.

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Characteristics of Magnetic Polishing with Magnetic Abrasive Powder Fabricated by Plasma Melting Method (플라즈마 용융법으로 제조된 Fe계 자성분말의 자기연마 특성)

  • 이영란;배승열;안인섭;이용철
    • Journal of Powder Materials
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    • v.8 no.1
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    • pp.20-25
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    • 2001
  • Most of mold manufacturing procedures have been automated by the introduction of NC machine tool and CAD/CAM system. But the three-dimensional surface curvature of the mold must be done by hand work of well-skilled workers. Magnetic abrasive polishing powders were investigated for surface polishing for 3D curvature. This study aims to investigate homogeneously distributed hard phase in Fe matrix and strong bonding between Fe-matrix and hard phase. The NbC powder, $B_4C$ powder and $Al_2O_3$ powder were mixed in Fe-matrix respectively. Mixed Fe-hard phase powders were compacted by press and then these were melted by plasma melting. According to SEM, XRD and OM observation, Fe-NbC magnetic abrsive powder had the most homogeneous distribution and strong bonding. As a result of magnetic polishing, the surface roughness before magnetic polishing, 1 ${\mu}m$ $R_{max}$, was reduced to 0.2 ${\mu}m$ $R_{max}$ over the entire inner surface of the tube.

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형상에 따른 초전도 튜브의 전기적 특성변화

  • Jang, G.E.;Park, C.W.;Ha, D.W.;Seung, T.H.
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2004.07a
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    • pp.527-530
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    • 2004
  • High-temperature Superconductor(HTS) tubes were fabricated in term of different diameter, length and thickness by centrigugal forming method. For powder melting by induction the optimum range of melting temperatures and preheating temperature were $1050^{\circ}C{\sim}1100^{\circ}C\;amd\;550^{\circ}C$ for 30min, respectively. The mould renting speed was 1000rpm. A tube was annealed at $840^{\circ}C$ for 72hours in oxygen atmosphere. The plate-like grains were well developed along the renting direction and typical grain size was about more than $40{\mu}m$. It was found that Ic values increased with increasing the tube diameter while the Ic decreased with increasing tube thickness. Also Ic decreased with increasing the tube length. The measured Ic in $50mm{\times}70mm{\times}25mm$ tube was about 896Amp.

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Bi2212 Tube Characteristics for SCFCL (한류기용 Bi2212 튜브의 특성)

  • Lee, N.I.;Jang, G.E.;Oh, I.S.;Park, G.B.
    • Progress in Superconductivity
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    • v.7 no.2
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    • pp.174-178
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    • 2006
  • For the practical application on SCFCL, Bi2212 tubes were fabricated by Centrifugal Forming Process (CFP) in terms of many different processing parameters. Typical sizes of tubes were 60, 150 mm in length and 2.5, 3.5, 4.8 mm in thickness. Initially powder was melted by induction heating. The optimum range of melting temperatures and preheating temperature were $1100^{\circ}C$ and $500^{\circ}C$ for 30min respectively. The nominal mold rotating speed was around 1000 RPM. A tube was annealed at $840^{\circ}C$ for 80 hours in oxygen atmosphere. The tube of 50mm x 70mm x 2.5mm, rotated with 1000 RPM showed $I_c=890\;A\;and\;T_c=80$. It was found that the tube processed with faster rate of mold rotation speed, thinner tube thickness and shorter tube length shows better electric characteristics as compared with the tube normally processed. In order to study the uniformity heat and fluid flow analysis tool was adopted along tube.

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Improvement of Powder Feeding Characteristics of Fine$5\mu\textrm{m}$ $Al_2O_3$ Powder by Modification of the Powder Feeding Systems and Characterization of the Coating Layer depending on Plasma Spraying Conditions (분말송급장치의 개조에 의한 미세$5\mu\textrm{m}$ $Al_2O_3$분말의 송급 특성개선 및 플라즈마 용사조건에 따른 코팅층의 특성분석)

  • 설동욱;김병희;정민석;임영우;서동수
    • Journal of Welding and Joining
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    • v.15 no.1
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    • pp.116-124
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    • 1997
  • A scope of this study is to establish the optimum plasma spray conditions for fine ($5\mu\textrm{m}$) $Al_2O_3$ powder. However, the flowability of the $Al_2O_3$ powder is not so good because of irregular particle shape and fine particle size. Therefore, powder feeding system was modified by 1) change of powder feeding line material from polymer to copper 2) shorten the powder feeding tube length 3) heating the powder feeding system to $80^{\circ}C$4) vibrating the powder feeding line continuously, in order to feed the fine powder homogeneously. The homogeneous powder feeding conditions were obtained with the modified powder feeding system by controlling the powder carrier gas flow and the powder flow rate indicator. The best plasma spraying conditions for the fine $Al_2O_3$ powder were found out as 40kw gun power, 80 g/min. powder feed rate and 50 mm working distance after characterizing the microstructure, hardness and wear loss of the $Al_2O_3$ coating layer.

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Treatment of Spontaneous Pneumothorax; in Patients 50 Years of Age or Older (노인성 자연 기흉의 치료방법 및 그 결과;50세 이상환자 60례 대상)

  • 조선환
    • Journal of Chest Surgery
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    • v.26 no.7
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    • pp.532-537
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    • 1993
  • To assess the therapy of spontaneous pneumothorax in the aged patients, the treatment methods and results in 60 patients 50 years of age or older were retrospectively reviewed. Most of the patients were male [56 of 60 patients] and the major underlying lung diseases associated with spontaneous pneumothorax were tuberculosis [32 patients] and chronic obstructive lung disease [20 patients]. The recurrence rate of thoracostomy tube drainage with or without chemical pleurodesis using tetracycline was 39.6% [21 of 53 patients], but there was no recurrence in the patients treated with open thoracotomy, pleural abrasion, and chemical pleurodesis using talcum powder[Asbestosis free]. In the patients treated with open thoracotomy, the bullous or bleb lesions were placed in the various sites of both lungs. We concluded that even though thoracostomy tube drainage is the first choice of therapy for spontaneous pneumothorax in the aged patients, the recurrence rate is high, especially in the patients with persistent air leakage for more than 2 days, and the open thoracotomy with pleural abrasion and chemical pleurodesis using talcum powder can prevent the recurrence in the selected patients.

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