• Title/Summary/Keyword: powder mixture

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Mechanical Properties of $\beta$-Sialon Ceramics Prepared from Wando Pyrophyllite and an Alkoxide (완도납석과 알콕사이드로부터 제조된 $\beta$-Sialon 세라믹스의 기계적 성질)

  • 이홍림;손연하;임헌진
    • Journal of the Korean Ceramic Society
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    • v.28 no.5
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    • pp.390-398
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    • 1991
  • $\beta$-Sialon powder was prepared from Wando pyrophyllite by the carbothermic reduction and nitridation at 135$0^{\circ}C$ for 10 h nitrogen atmosphere. Amorphous silica prepared from Si(OC2H5)4 was added to Wando pyrophyllite powder in order to control the final Z value. Two different methods were applied for synthesis of $\beta$-sialon powders. In Process A, the amorphous silica prepared from Si(OC2H5)4 was admixed to Wando pyrophyllite powder. Process B was started from the mixture of Wando Y2O3 was added to the synthesized $\beta$-Sialon powders as a sintering aid, and the mixed powders were hot pressed at 175$0^{\circ}C$ for 120 min in nitrogen atmosphere under 30 MPa. Their mechanical properties were compared. The maximum values of M.O.R., hardness and KIC were 667 MPa, 16 GPa and 6.3 MN/m3/2, respectively, and they are the values obtained form $\beta$-Sialon ceramics prepared by process A of Z=0.5.

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Mechanochemical Synthesis of LaNiO3 Crystalline Phase from Mixture of La2O3sub> and NiO (La2O3의 메카노케미컬 합성에 의한 LaNiO3결정상 생성)

  • 김대영;김강언;이명교;정수태
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.16 no.8
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    • pp.681-687
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    • 2003
  • The syntheses of LaNiO$_3$Perovskite crystalline phase from mixtures of La$_2$O$_3$and NiO via it mechanochemical(used planetary mill) and a wet ball mill process were investigated. A single and stable LaNiO$_3$perovskite crystalline phase was successfully prepared by using a heat free mechanochemical process which produced a fine amorphous powder, while that phase was not formed in a wet ball mill process which needed heat treatment ranging from 500 to 150$0^{\circ}C$ and produced a coarse powder. It was shown that the LaNiO$_3$ceramics made of the mechanochemically synthesized powder possesed a good metallic characteristic.

The Effect of the precursor powder composition for Bi-system superconducting thick films on Cu tapes (동테이프 위의 Bi-계 초전도 후막에서 전구체분말 조성의 영향)

  • 한상철;성태현;한영희;이준성;김상준
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1999.05a
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    • pp.65-68
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    • 1999
  • A well oriented Bi2212 superconductor thick films were fabricated by screen printing with a Cu-free Bi-Sr-Ca-O mixture powder on a copper plate and heat-treating at 820-88$0^{\circ}C$ for several minute in air. During the heat-treatment, the printing layer partially melted by reaction between the Cu-free precursor and CuO of the oxidizing copper plate. In the partial melting state, it is believed that the solid phase is Bi-free phase and Cu-rich phase and the composition of the liquid is around Bi : Sr : Ca : Cu = 2 : 2 : 0 : 1. Following the partial melting, the Bi2212 superconducting phase is formed at Bi-free phase/liquid interface by nucleation and grows. With decreasing the Bi composition in the precursor powder, the critical temperature(T$_{c}$) of the fabricated Bi2212 thick film increased to about 79 K.K.

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Strength Properties of High-Strength Polymer Cement Mortars Containing VAE Powder (VAE계 분말을 혼입한 고강도 폴리머 시멘트 모르타르의 강도 특성)

  • Choi, Jung-Gu;Lee, Gun-Cheol;Lee, Gun-Young
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2014.11a
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    • pp.19-20
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    • 2014
  • This study is to find out the tensile strength and bonding strength of VAE powder as a preliminary study for the application of the powder to the high strength concrete. The result of the study showed that the compressive strength decreases when more polymers is put into the concrete. On the other hand, it showed that the tensile strength and the bonding strength get improved when the more polymers are put into the concrete. Especially in case of the mixture for high strength concrete, it was found out that more strength is produced than the ordinary concrete.

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Dry Coated Particle for Plasma Spraying

  • Briones-Rodriguez, C.;Mayagoitia-Barragan, V.;Cuenca-Alvarez, R
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.156-157
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    • 2006
  • The preparation of composite powders for plasma spraying by an in-house designed mechanofusion process is investigated. Results show that dry particle coating depends on the chemical and mechanical properties of powders. In metal/oxide and metal/oxide/carbide powder mixtures, fine ceramic particles coat the surface of the metallic coarser particles. A nearly rounded shape of the final composite particles is induced by the mechanical energy input with no formation of new phases. However with the carbide/metal powdered system, only an intimate mixture of components is achieved. It is suggested that the coating mechanism is governed by agglomeration and rolling phenomena.

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EHect of Carbide Addition on Riping and Wear Properties of HSS (탄화물의 첨가가 고속도강의 HIP과 마모에 미치는 영향)

  • 김득중
    • Journal of Powder Materials
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    • v.3 no.3
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    • pp.188-195
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    • 1996
  • In recent times the potential application of the high speed steel produced by HIP process for wear resistant and cutting materials are increasing. In this work the microstructure of Anval 30 produced by HIP process was investigated and the effect of WC, TiC addition on microstructure formation and wear properties were studied. After HIP process at 1150 $^{\circ}C$, the original feature of spherical raw powders was not removed and consequently, nonuniform microstructure was formed. However the WC added by simple powder mixture incereased the sinterbility of high speed steel and uniform microstructure formed. The wear characteristics of Anval 30 with carbide addition were tested at RT and $600^{\circ}C$. The uniform microstructure played an more important role in wear resistance as compared with the hardness.

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Effect of Atmospheric Gas on the Size and Distribution of Cu Nano Powders Synthesized by Pulsed Wire Evaporation Method (전기 폭발법에 의해 제조된 나노 구리 분말의 크기와 분포에 미치는 조업 가스의 영향)

  • ;;;Y. A. Kotov
    • Journal of Powder Materials
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    • v.11 no.3
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    • pp.210-216
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    • 2004
  • The possibility to decrease agglomeration of Cu nano powders and their separation during pulsed wire evaporation (PWE) process was investigated by controlling the working gas system, i.e., the design of the gas path, the type and pressure of the atmospheric gas. As a result, it was possible to choose the optimal design of the gas path providing large specific surface area and high degree of separation of the synthesized Cu nano powders. It was also shown that an Ar+10∼50$N_2$ mixture can be used in production of Cu nano powders, which do not react with nitrogen.

Pressure-Dependent Yield Model for Metallic Powder Mixtures and Their Densification Behavior During Die Compaction as Analyzed by the Finite Element Method (금속분말 혼합체의 압력의존 항복모델과 유한요소법을 이용한 금형압분 공정 시 고형화 해석)

  • Yoon, Seung Chae;Kim, Taek-Soo;Kang, Seung Koo;Kim, Hyoung Seop
    • Korean Journal of Metals and Materials
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    • v.47 no.9
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    • pp.567-572
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    • 2009
  • The densification behaviors of mixtures of copper and steel powders during cold die compaction were investigated. We proposed the pressure-dependent yield function based on the rule of the mixtures of each yield function of a critical relative density type. The constitutive equations were implemented into a finite element program (DEFORM2D) to analyze the densification and deformation behavior of powder mixtures, and the simulated results are in good agreement with the experimental results in reference studies.

Blood glucose monitoring under the existence of other blood components by a portable type-NIR spectrometer.

  • Baek, Ju-Hyun;Kang , Na-Roo;Woo, Young-Ah;Kim, Hyo-Jin
    • Proceedings of the PSK Conference
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    • 2003.10b
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    • pp.220.2-220.2
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    • 2003
  • Many interference in blood should be considered for non-invasive blood glucose level monitoring by near-infrared spectroscopy because blood glucose concentration is about 0.1% (w/v) in normal state. In this study, we investigated the influence of other blood components on blood glucose level monitoring by near-infrared spectroscopy. It carried out by newly developed portable type-NIR system (1100∼2200 nm). Spectrum features of NIR diffuse spectral data were investigated for some blood compnents powder such as hemoglobin, blood serum albumin, urea, uric acid, ascorbate, glucose, cholesterol and as adding glucose powder into other blood components powder mixture. (omitted)

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Processing of Functional Porridge with Optimal Mixture Ratio of Mulberry Leaf Powder and Mulberry Fruit Powder (뽕잎분말과 오디분말의 최적 혼합비율을 이용한 기능성 죽 제조)

  • Kim, You-Jin;Kim, Min-Ju;Kim, Hyun-Bok;Lim, Jung-Dae;Kim, Ae-Jung
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.46 no.9
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    • pp.1081-1090
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    • 2017
  • The purpose of this study was to develop a functional porridge prepared with mulberry leaf and mulberry fruit powder, which can ameliorate hypertension. The experiment was designed according to the central composite design. For optimization of the mixture ratio of mulberry leaf powder (MLP) and mulberry fruit powder (MFP), the independent variables were defined as MLP (X1) and MFP (X2) and the dependent variables were defined as K (Y1), Na (Y2), ${\gamma}$-aminobutyric acid (GABA) (Y3), cyanidin-3-glycoside (C3G) (Y4), rutin (Y5), and flavonoid (Y6). The optimal MLP to MFP mixture ratio according to the response surface method were 5.41 g of MLP and 2.65 g of MFP. The amounts of K, Na, GABA, C3G, rutin, and flavonoid in the optimal MLP and MFP mixture were 1,844.22 mg/100 g, 52.74 mg/100 g, 139.98 mg/100 g, 1,134.89 mg/100 g, 101.56 mg/100 g, and 201.28 mg/100 g, respectively. The amounts of Ca, K, Mg, and Na in the functional porridge at this optimal point were 27.66 mg/100 g, 131.32 mg/100 g, 19.57 mg/100 g, and 3.59 mg/100 g, respectively. Overall, this functional porridge can help reduce hypertension.