• 한국세라믹학회지
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• 제35권10호
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• pp.1085-1093
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• 1998

Amorphous alumina powder prepared by the fast calcination of aluminum trihydroxide(Al(OH)3 gibbsite) for 0.5 second at 580$^{\circ}C$ was investigated rehydration propeties. Phase composition crystal size and mor-phology surface area pore volume and pore size distribution of pesudo-boehmite and bayerite crystals changed with temperature time water/alumina ratio and particle size when amorphous alumina rehydrated with water. Phase compositions were examined with XRD and DTA and crystal sized morphologies were investigaed with SEM and TEM. Also rehydration properties of amorphous alumina were in-vestigated by measuring the surface area pore volume and pore size distribution.

• Computers and Concrete
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• 제11권4호
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• pp.317-336
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• 2013

In this study, the pore structure of Portland cement paste is experimentally characterized by MIP (mercury intrusion porosimetry) and nitrogen adsorption, and simulated by a newly developed status-oriented computer model. Cement pastes with w/c=0.3, 0.4 and 0.5 at ages from 1 day to 120 days are comprehensively investigated. It is found that MIP cannot generate valid pore size distribution curves for cement paste. Nevertheless, nitrogen adsorption can give much more realistic pore size distribution curves of small capillary pores, and these curves follow the same distribution mode. While, large capillary pores can be effectively characterized by the newly developed computer model, and the validity of this model has been proved by BSE imaging plus image analysis. Based on the experimental findings and numerical simulation, a hypothesis is proposed to explain the formation mechanism of the capillary pore system, and the realistic representation of the pore structure of hydrated cement paste is established.

• 한국세라믹학회지
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• 제36권6호
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• pp.662-670
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• 1999

Porous alumina was fabricated from pressureless powder packing forming method using powders granulated by spray drying. It was investigated the pore size distribution of fabricated porous alumina. The results of microstructural observation showed that intraganular pore size and intragranular pore size. At 1700$^{\circ}C$ there were no intragranular pores but it showed homogeneous distribution of intergranular pore size. The bending strength and shrinkage increased as porosity decreased. In case of thermal shock resistance sudden decrease of bending strength to $\Delta$T was not shown because intergranular large pore prevented sudden crack propagation.

• 한국세라믹학회지
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• 제40권6호
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• pp.572-576
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• 2003

$UO_2$-20 wt% CeO$_2$ 소결 펠렛의 밀도에 따른 개/폐 기공도, 기공의 크기 및 그 분포 그리고 기공의 형태를 조사하였다. 이론 소결밀도 약 96% 이상에서는 기공도는 개기공이 거의 없는 폐기공으로 나타났다. 반면에 기공크기 분포는 소결밀도에 관계없이 bimodal 형태를 보이나, 소결밀도가 증가할수록 기공 개수만 적게 나타났다. 기공의 형태는 소결밀도가 증가할수록 불규칙한 형태에서 둥근 형태로 바뀌었다.

• Restorative Dentistry and Endodontics
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• 제46권4호
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• pp.57.1-57.9
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• 2021

Objectives: This study aimed to compare and evaluate the porosity and pore size distribution of high-viscosity glass ionomer cements (HVGICs) and conventional glass ionomer cements (GICs) using micro-computed tomography (micro-CT). Materials and Methods: Forty cylindrical specimens (n = 10) were produced in standardized molds using HVGICs and conventional GICs (Ketac Molar Easymix, Vitro Molar, MaxxionR, and Riva Self-Cure). The specimens were prepared according to ISO 9917-1 standards, scanned in a high-energy micro-CT device, and reconstructed using specific parameters. After reconstruction, segmentation procedures, and image analysis, total porosity and pore size distribution were obtained for specimens in each group. After checking the normality of the data distribution, the Kruskal-Wallis test followed by the Student-Newman-Keuls test was used to detect differences in porosity among the experimental groups with a 5% significance level. Results: Ketac Molar Easymix showed statistically significantly lower total porosity (0.15%) than MaxxionR (0.62%), Riva (0.42%), and Vitro Molar (0.57%). The pore size in all experimental cements was within the small-size range (< 0.01 mm³), but Vitro Molar showed statistically significantly more pores/defects with a larger size (> 0.01 mm³). Conclusions: Major differences in porosity and pore size were identified among the evaluated GICs. Among these, the Ketac Molar Easymix HVGIC showed the lowest porosity and void size.

• 한국의류학회지
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• 제26권7호
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• pp.1078-1084
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• 2002

Cotton fabrics were treated with 1,2,3,4-butanetetracarboxylic acid(BTCA) to impart durable press performance, which is formaldehyde-free DP finishing reagent. The pore structures of BTCA treated cottons were compared using a reverse gel permeation chromatographic technique(reverse GPC). A series consisting 4 kinds of water soluble sugars was used to study the elution characteristics of columns prepared from cotton fibers. From these data, differences in pore size distribution in the control and BTCA treated cottons were distinguished. BTCA crosslinks cellulose molecules provided wrinkle resistance to the treated cotton fabrics through ester linkages. Although crosslinking of cotton with BTCA reduced accessible internal volume across the entire range of pore size, differences in line pores were larger than in small pores. BTCA treated cotton exhibited reductions over 40% in large pore sizes.

• 한국막학회:학술대회논문집
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• 한국막학회 1991년도 추계 총회 및 학술발표회
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• pp.4-8
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• 1991

The characterization of pore properties (mean pore size and pore size distribution) of the active layer in a UF membrane is important not only in order to obtain information about the factors affecting pore formation during membrane manufacturing but also to understand deeply the mechanism of solute and solvent transport through pores. Many methods of characterizing quantitatively the pore properties of UF membranes have been suggested in the literature: solvent and gas flow measurement, bubble point determination, electron microscopy, gas adsorption/desorption measurement, rejection measurement etc. But most of these methods involve time-consuming procedures and involve some wellknown problems and uncertainties.

• 한국결정학회지
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• 제9권1호
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• pp.64-70
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• 1998

석탄회 70 wt%-점토 30wt%인 슬립으로부터 DCC(Direct Coagulation Casting)법을 이용하여 다공체를 제조하였다. 각각 1.55, 1.60, 1.65g/cm3의 비중을 갖는 슬립으로부터 제조한 다공체의 미세구조 관찰 및 기공크기 분포 측정을 통해 슬립의 비중이 기공크기 및 분포에 미치는 영향에 대해서 연구하였다. 슬립의 비중에 관계없이 평균기공의 크기는 약 2.5μm이었으며, 1.60g/cm3의 비중을 갖는 슬립으로부터 제조된 다공체의 미세구조 및 기공분포가 가장 균일하였다. 슬립비중 1.55g/cm3인 경우에는 고체의 양이 작아 겔화의 진행이 느려 기공분포가 넓어졌으며, 비중 1.65g/cm3인 슬립은 해교제의 첨가량이 많아 응집제 첨가시 점도의 변화가 매우 컸으며 불안정한 슬립 특성을 보였다.

• 한국세라믹학회지
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• 제31권2호
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• pp.137-146
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• 1994

This experiments were focused on a modification of mechamical properties and structure in porous aluminum titanate ceramics by new additives which have been not researched yet. These were consisted of four kinds of additives i.e. Bi2O3, FeO, ZnO and NiO by addition amount of 1 wt% and 5 wt% respectively. The addition of Bi2O3 retarded a degree of syntehsis of aluminum titanate and accelerated in FeO, ZnO, NiO additives. Also, the most effective accelerator in synthesis of alunium titanate was FeO. A additives for the most effective of modification of microstructure, sharp distribtion of pore size and mechanical proterties was on ZnO addition and showed the lowest average pore size and narrowed pore size distribution. In order to improve of microstructure and pore size distribution in porous aluminum titanate ceramics was desired the addition amount of 1 wt% compare to 5 wt%.

• 한국염색가공학회지
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• 제21권4호
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• pp.57-62
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• 2009

N-Halamines are compounds which have covalent bonding between nitrogen and halogen. N-Halamine materials possess strong antimicrobial properties against wide spectrum of bacteria. The aim of this study is to prepare N-halamine membranes using m-aramid and poly(vinyl alcohol) (PVA). Surface characteristics using scanning electron microscope (SEM), pore size distribution, liquid permeability and mean pore size were measured to confirm feasibility as membrane. The results indicated that increased PYA portion up to 15% in the m-aramid/PVA blend resulted in improved pore size distribution, liquid permeability as well as mean pore size. Furthermore, antibacterial efficacy of the membranes after chlorination was confirmed and the results showed that bacteria in water were inactivated.