• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 1997년도 추계학술대회 논문집
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• pp.167-170
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• 1997

For the optimal net shape forging of semi-solid materials (SSM), it is important to predict the deformation for variation of strain rate. It should be necessruy to conduct a formation of stress-strain curve in semi-solid alloys for analysis of the thixoforming process. Particularly, important problem to application of computer aided engineering in SSM processing is to prevent a segregation of liquid component during compression process. The liquid segregation is studied as multistage change of the strain rate and test piece size to prevent the liquid segregation during the compression process. The compression test for semi-solid aluminium alloy with a controlled solid fraction is performed by dynamic material test system with a furnace. Moreover morphology of structure and fraction of pore are investigated through compression test.

• Macromolecular Research
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• 제14권1호
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• pp.59-65
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• 2006

We report a new approach to fabricate electrospun polymer nonwoven mats with porous surface morphology by varying the collector temperature during electrospinning. Polymers such as poly(L-lactide) (PLLA), polystyrene (PS), and poly(vinyl acetate) (PVAc) were dissolved in volatile solvents, namely methylene chloride (Me) and tetrahydrofuran (THF), and subjected to electrospinning. The temperature of the collector in the electrospinning device was varied by a heating system. The resulting nonwoven mats were characterized by using scanning electron microscopy (SEM), field emission SEM (FESEM), and atomic force microscopy (AFM). We observed that the surface morphology, porous structure, and the properties such as pore size, depth, shape, and distribution of the nonwoven mats were greatly influenced by the collector temperature.

• Bulletin of the Korean Chemical Society
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• 제27권1호
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• pp.53-58
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• 2006

A powder of destructive adsorbent was prepared by impregnating Mn and Cu on the surface of amorphous aluminosilicate. It catalytically dimerized tert-butyl mercaptan into di-tert-butyl disulfide on its surface. Turnover of the dimerization was strongly dependent on the surface morphology of the adsorbent, which could be altered by modification of aluminosilicate support. During the process of impregnation, which involved heat treatment at 500 ${^{\circ}C}$, the shape of the pore was preserved, though large fraction of micropores were eliminated. The reactive sites on the surface were poisoned as dimerization products strongly adhered on them. Therefore, high surface area was not always desirable. When the surface was heavily populated with “inkbottled” pores with a narrow entrance in uniform size, heavy poisoning of the reactive sites turned the destructive adsorbents almost useless.

• 한국재료학회지
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• 제25권10호
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• pp.509-515
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• 2015

MAO ceramic coatings were prepared on AZ61 magnesium alloy for various processing times ranging from 5 to 60 min, in an electrolyte solution based on silicate-fluoride. The mechanical, electrochemical and, microstructural properties and the phase compositions of the coating layers were investigated. In this work, unlike previous studies, coatings with high amounts of the $Mag_2SiO_4$ phase were formed which contained small amounts of MgO and $MgF_2$ at a processing condition of 30 min. A microstructural analysis revealed that the porosity of the coatings was reduced considerably with an increase in the processing time, together with a change in the pore geometry from an irregular to a spherical shape. Potentiodynamic polarization and mechanical testing results showed that the coatings acquired after a processing time of 30 min were superior to all of the others.

• The Korean Journal of Ecology
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• 제26권5호
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• pp.237-246
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• 2003

우리나라 산촌마을의 경관구조를 경관생태학적 패러다임인 토지 모자이크 모형에 의해 해석하였다. 상대적으로 개발의 영향이 적게 작용하여 산림청의 산촌종합개발사업 대상마을로 선정된 전북 김제시 선동리 아직, 산수마을을 연구대상지로 선정하였다. 전형적으로 나타나는 마을유역의 면적(2.8∼2.0㎢), 마을구역 및 농경지의 면적율(27%), 숲의 면적율(73%)이 조사되었다. 패취 경계형태의 깔때기 효과 특성은 3차원적 지형요소와 풍수지리적 형국도를 원용하여 해석할 수 있었다. 패취 경계형태의 깔때기는 동물이동 주요 통로로 보며 하천에 의하여 형성되는 만입부는 물과 대기 흐름의 장소로 동시에 적용될 때 물질흐름이 해석될 수 있었고, 이러한 깔때기 효과의 개념은 풍수지리에서 사용되는 형국도에서 중심축과 지류축으로 나타나고 있었다. 이러한 내용은 산촌생태마을 계획. 설계 시 보전해야 할 숲의 적정 크기와 하천 및 능선의 녹지축 net-working을 하기 위한 기본적 틀로서 적용될 수 있다고 판단된다.

• Journal of Welding and Joining
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• 제33권4호
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• pp.7-16
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• 2015

New lasers such as high power, high brightness and short wavelength laser are using diverse industry. Also new technologies are developing actively to solve various issues such as spattering, process monitoring, deep penetration and key-hole stability. ICALEO is the international congress where recent technology for laser material processing and laser system are present. At 2014, it was held at San Diego in USA and more than 260 papers were presented from 28 country. The effect of the laser beam shape such as Gaussian like and top-hat was investigated on acoustic emission signal and pore formation in welding. Inline penetration depth was measured with ICI(Inline Coherent Imaging) technique and the data was verified with real time X-ray image on laser welding. The laser welding performance at low pressure environment was evaluated for the thick plate alloy steel. UV laser was used to weld various metals such as Cu, Aluminum, steel and stainless steel. The effect of the wavelength of the laser on the formation of the wave at the wall of the key-hole front and the absorptivity was investigated.

• 상하수도학회지
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• 제19권6호
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• pp.713-719
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• 2005

SPME (Soild phase microextraction) has been used in the analysis of many volatile organic compounds, such as geosmin and 2-methylisoborneol (2-MIB), trihalomethanes (THMs) in drinking water. SPME fiber is characterized by high adsorption capacity (DVB/CAR/PDMS, DVB/PDMS etc.). Although the highly active adsorption capacities of the SPME fiber are often to the chemical functional group, surface properties play a significant role in determining the surface adsorption capacities. The objectives of this study were to evaluate effect of residual chlorine on analysis of geosmin and 2-MIB. Image taken by SEM before preloaded with chlorine, the surface and porous media was almost perfect spherical shape and no clogging of pores. However, after preloaded with chlorine the surface was aggregated and pore was blocked. The recovery rate of geosmin and 2-MIB coexisting with chlorine was reduced by 35 to 62%. The recovery rate with preloaded with chlorine was reduced by 25 to 43%. The lower concentration of geosmin and 2-MIB and the higher concentration of chlorine existed in water, the lower the recovery rate was.

• 한국표면공학회지
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• 제49권2호
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• pp.125-129
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• 2016

Anodizing is a technology to generate thicker and high-quality films than natural oxide films by treating metals via electrochemical methods. Electrochemical manufacturing method of nano structure is an efficient technology in terms of cost reduction, high productivity and complicated shapes, which receives the spotlight in diverse areas. Especially, artificial films generated by anodizing technology possess excellent mechanical characteristics including hardness and wear resistance. It is also easy to modify thickness and adjust shape of those artificial films so that they are mainly used in sensors, filters, optical films and electrolytic condensers. In this study, experiment was performed to observe the effect of current density on porous film formation in two-step anodizing for Al alloy. Anodizing process was performed with 10 vol.% sulfuric acid electrolyte while the temperature was maintained at $10^{\circ}C$ using a double beaker. and $10{\sim}30mA/cm^2$ was applied for 40 minutes using a galvanostatic method. As a result, both pore diameters and distances between pores tended to increase as the local temperature and electrolysis activity increased due to the increase in applied current density.

• 한국재료학회지
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• 제2권6호
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• pp.428-435
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• 1992

AISI 4600계 철 분말에 F$e_2$P 분말을 사용하여 인(P)을 0~1.0% 그리고 흑연 분말을 사용하여 탄소를 0~0.8% 첨가하여 회전혼합기를 사용하여 혼합하였다. 흔합분말을 양단압금형에서 800MPa로 가압하여 성형체를 만들었다. 성형체는 진공 또는 수소와 질소 혼합가스 분위기에서 115$0^{\circ}C$에서 30분간 소결하였다. 소결체를 연마하고 2% 질산용액으로 에칭하였다. 소결체 조직을 Image Analyzer와 금속현미경으로 관찰하였다. 밀도는 ASTM B3l2로, 경도는 미세 비커스경도기로 측정하였다. 얻어진 결과는 다음과 같다. (1) F$e_2$P 첨가량이 증가하면, 소결체 조직은 치밀화되고 입자 크기는 더 커졌다. (2) $Fe_2P량과$ 함께 기공의 형상은 둥글고, 그 숫자는 감소하였으나 평균크기는 더 커졌다. (3) 입자의 크기는 F$e_2$P와 흑연분말을 동시에 첨가한 경우가 각각 단독으로 첨가한 경우보다 커졌다. (4) 미세조직에 미치는 소결분위기의 영향은 거의 없었다. (5) 경도는 인과 탄소량이 증가하면 상승하였다.

• Geomechanics and Engineering
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• 제21권5호
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• pp.489-501
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• 2020

This paper conducts a complicated coupled effective stress analysis of X-section-in-place concrete (XCC) pile installation and consolidation processes using the dual-stage Eulerian-Lagrangian (DSEL) technique incorporating the modified Cam-clay model. The numerical model is verified by centrifuge data and field test results. The main objective of this study is to investigate the shape effect of XCC pile cross-section on radial total stress, excess pore pressure and time-dependent strength. The discrepancies of the penetration mechanism and set-up effects on pile shaft resistance between the XCC pile and circular pile are discussed. Particular attention is placed on the time-dependent strength around the XCC pile shaft. The results show that soil strength improved more significantly close to the flat side compared with the concave side. Additionally, the computed ultimate shaft resistance of XCC pile incorporating set-up effects is 1.45 times that of the circular pile. The present findings are likely helpful in facilitating the incorporation of set-up effects into XCC pile design practices.