• 제목/요약/키워드: pore depth

검색결과 252건 처리시간 0.028초

The formation of highly ordered nano pores in Anodic Aluminum Oxide

  • Im, Wan-soon;Cho, Kyung-Chul;Cho, You-suk;Park, Gyu-Seok;Kim, Dojin
    • 한국재료학회:학술대회논문집
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    • 한국재료학회 2003년도 춘계학술발표강연 및 논문개요집
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    • pp.53-53
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    • 2003
  • There has been increasing interest in the fabrication of nano-sized structures because of their various advantages and applications. Anodic Aluminum Oxide (AAO) is one of the most successful methods to obtain highly ordered nano pores and channels. Also It can be obtained diverse pore diameter, density and depth through the control of anodization condition. The three types of substrates were used for anodization; sheets of Aluminum on Si wafer and Aluminum on Mo-coated Si wafer. In Aluminum sheet, a highly ordered array of nanoholes was formed by the two step anodization in 0.3M oxalic acid solutions at 10$^{\circ}C$ After the anodization, the remained aluminum was removed in a saturated HgCl$_2$ solution. Subsequently, the barrier layer at the pore bottom was opened by chemical etching in phosphoric acid. Finally, we can obtain the through-channel membrane. In these processes, the effect of various parameters such as anodizing voltage, anodizing time, pore widening time and pre-heat treatment are characterized by FE-SEM (HITACH-4700). The pore size. density and growth rate of membrane are depended on the anodizing voltage and temperature respectively. The pore size is proportional to applied voltage and pore widening time The pore density can be controlled by anodizing temperature and voltage.

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Comparison of Soil Pore Properties between Anthropogenic and Natural Paddy Field Soils From Computed Tomographic Images

  • Chun, Hyen Chung;Jung, Ki-Yuol;Choi, Young Dae;Jo, Su-min;Lee, Sanghun;Hyun, Byung-Keun;Shin, Kooksik;Sonn, Yeonkyu;Kang, Hang-Won
    • 한국토양비료학회지
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    • 제48권5호
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    • pp.351-360
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    • 2015
  • Human influence on soil formation has dramatically increased with human civilization and industry development. Increase of anthropogenic soils induced researches on the anthropogenic soils; classification, chemical and physical characteristics of anthropogenic soils and plant growth from anthropogenic soils. However there have been no comprehensive analyses on soil pore or physical properties of anthropogenic soils from 3 dimensional images in Korea. The objectives of this study were to characterize physical properties of anthropogenic paddy field soils by depth and to find differences between natural and anthropogenic paddy field soils. Soil samples were taken from two anthropogenic and natural paddy field soils; anthropogenic (A_c) and natural (N_c) paddy soils with topsoil of coarse texture and anthropogenic (A_f) and natural (N_f) paddy soils with topsoil of fine texture. The anthropogenic paddy fields were reestablished during the Arable Land Remodeling Project from 2011 to 2012 and continued rice farming after the project. Natural paddy fields had no artificial changes or disturbance in soil layers up to 1m depth. Samples were taken at three different depths and analyzed for routine physical properties (texture, bulk density, etc.) and pore properties with computer tomography (CT) scans. The CT scan provided 3 dimensional images at resolution of 0.01 mm to calculate pore radius size, length, and tortuosity of soil pores. Fractal and configuration entropy analyses were applied to quantify pore structure and analyze spatial distribution of pores within soil images. The results of measured physical properties showed no clear trend or significant differences across depths or sites from all samples, except the properties from topsoils. The results of pore morphology and spatial distribution analyses provided detailed information of pores affected by human influences. Pore length and size showed significant decrease in anthropogenic soils. Especially, pores of A_c had great decrease in length compared to N_c. Fractal and entropy analyses showed clear changes of pore distributions across sites. The topsoil layer of A_c showed more degradation of pore structure than that of N_c, while pores of A_f topsoil did not show significant degradation compared with those of N_f. These results concluded that anthropogenic soils with coarse texture may have more effects on pore properties than ones with fine texture. The reestablished paddy fields may need more fundamental remediation to improve physical conditions.

양극 산화 조건 변화에 따른 AAO Template Morphology 제어 (AAO Template Morphology Controlled by Variation of Anodizing Condition)

  • 조예원;이성갑;김경민
    • 한국전기전자재료학회논문지
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    • 제28권4호
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    • pp.249-251
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    • 2015
  • In this study, the application of biosensor having a large surface area for more effective and AAO (anomic aluminium oxide) template in order to gain concentration and voltage of anodizing process morphology changes to the control of experiments were conducted. The biosensor surface may increase the response characteristics by having a large surface area. So the entrance to a little more efficient wide depth sensing experiment was carried out to obtain a structure body with a branch shape with a large surface area with increasing. Experimental results from the FE-SEM observation was obtained template morphology. As a result, depending on the anodizing time, the depth of the layer of aluminum oxide was found that it was confirmed that the deepening of the pore size changes according to anodizing condition. And measuring the detection performance according to the conditions in the electrolyte and the reaction because of blood using a biosensor measuring sensing property according to the depth of the pore depth is considered that does not have a significant impact.

지피상태(地被狀態)에 따른 임지(林地)의 수저유(水貯留) 특성(特性)(II) (Water Storage Characteristics of Surface Soil by the Different Forest Floor Conditions(II))

  • 이헌호;이창우
    • 한국산림과학회지
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    • 제83권4호
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    • pp.473-479
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    • 1994
  • 본 연구는 임지의 수저류능력을 토양공극 구분에 의한 실제 이용가능수량으로 평가하여 지속적인 수자원의 확보를 위한 기초자료를 제공할 목적으로 수행하였으며, 그 결과는 다음과 같다. 1. 조공극은 임지>임간나지>초지의 순으로 높았고, 토심이 깊을수록 전공극, 조공극, 이용가능수량은 감소하는 반면, 세공극은 점차 증가하는 것으로 나타났다. 2. 토양의 공극과 이학적 특성은 지피상태별로 표층(0~20cm)에서 고도의 유의차를 보이는 반면, 토심 20~40cm와 토심 40~60cm에서는 큰 차이가 없었다. 한편, 동일 시험구에서 표층(0~20cm)과 토심 20~40cm와는 큰 차이를 보이나 토심 20~40cm와 토심 40~60cm와는 큰 차이가 없었다. 3. 전 시험구에서 이용가능수량은 조공극과 고도의 상관관계를 나타냈다. 4. 조공극량과 토심을 이용하여 나타낸 이용가능수량으로 각 지피상태별 수저류량 추정모델을 산출할 수 있었다.

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지오텍스타일로 보강된 농업용 저수지 제체의 붕괴거동 (Behavior of Failure of Agricultural Reservoirs Embankment Reinforced by Geotextile under Overtopping Condition)

  • 이달원;노재진
    • 한국농공학회논문집
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    • 제56권2호
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    • pp.59-64
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    • 2014
  • In this study, the large scale test was performed to investigate the behavior of failure for the embankment and spillway transitional zone by overtopping. The pore water pressure, earth pressure, settlement and failure pattern of covering embankment with geotextile were compared and analyzed. The pore water pressure showed a small change in the spillway transition zone and core, indicating that the geotextile efficiently reinforced the embankment. The earth pressure decreased the infiltration of the pore water only in inclined cores type to secure local stability. The behavior of failure started from the bottom and gradually progressed upwards. After the intermediate overtopping period (100 min), width and depth of the seepage erosion were very small due to the effect of geotextile which delayed failure. Therefore, the reinforced method by geotxtile was a very effective method to respond to the emergency due to overtopping.

급속열처리를 통한 알루미나 나노 템플레이트의 기공 균일도 개선에 관한 연구 (A Study on Improved Pore Uniformity of Nano Template using the Rapid Thermal Anneal)

  • 김동희;김진광;권오대;양계준;이재형;임동건
    • 한국전기전자재료학회논문지
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    • 제19권2호
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    • pp.189-194
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    • 2006
  • Ordered nanostructure materials have received attention due to their unique physical properties and potential applications in electronics, mechanics and optical devices. To actualize most of the proposed applications, it is quite important to obtain highly ordered nanostructure arrays. The well-aligned nanostructure can be achieved by synthesizing nanostructure material in the highly ordered template. To get well-aligned pore array and reduce process time, rapid thermal anneal by an IR lamp was employed in vacuum state at $500^{\circ}C$ for 2 hour. The pore array is comparable to a template annealed in vacuum furnace at $500^{\circ}C$ for 30 hours. The well-fabricated AAO template has the mean pore diameter of 70 nm, the barrier layer thickness of 25 nm, the pore depth of $9{\mu}m$, and the pore density of higher than $1.2{\times}10^{10}cm^{-2}$.

급속열처리를 통한 알루미나 나노템플릿의 기공 균일도 개선에 관한 연구 (A Study on Improved Pore Uniformity of Nano Template Using the Rapid Thermal Processor)

  • 김동희;김진광;권오대;양계준;이재형;임동건
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2005년도 하계학술대회 논문집 Vol.6
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    • pp.637-638
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    • 2005
  • AAO templates were fabricated using a two-step anodization process with pretreatment such as electro polishing and annealing. To reduce process time and get well-aligned pore array, rapid thermal processor by an halogen lamp was employed in vacuum state at $500^{\circ}C$ for various time. The pore array of AAO template annealed at $500^{\circ}C$ for 2 h is comparable to a template annealed in conventional furnace at $500^{\circ}C$ for 30 h. The well-fabricated AAO template has the mean pore diameter of 70 nm, the barrierlayer thickness of 25 nm, and the pore depth of $9{\mu}m$. And the pore density can be as high as $2.0\times10^{10}cm^{-2}$.

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사면안정을 위한 지중 흡수관의 설계 (Design of Absorption Pipe for Slope Stability)

  • 조홍제;문종규;이광제
    • 한국지반공학회논문집
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    • 제26권11호
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    • pp.75-87
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    • 2010
  • 불포화토에 강우가 지속되면 토체내 간극수압이 상승하게 된다. 따라서 토층의 포화로 인해 강도가 저하되고, Suction압이 균형을 이루는 임계 깊이까지 Wetting Front가 하강하여 사면붕괴가 발생한다. 지중 간극수압을 제어할 수 있다면 강도저감을 방지함으로써 사면안정을 유지할 수 있을 것이다. 본고는 지중 간극수를 흡수하여 배출할 수 있는 흡수관 설계를 시도하여 실험성과로 그 가능성을 제시하였다. 흡수관은 사면안정을 위한 보조공법으로 활용하는 것이 효과적일 것이다.

산화에 의한 산림환경변화가 토양의 특성에 미치는 영향 (Effects of Forest Environmental Changes on Soil Characteristics by Forest Fire)

  • 남이;민일식;장관순;박관수;이윤원
    • 한국토양환경학회지
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    • 제3권2호
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    • pp.61-70
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    • 1998
  • 본 연구는 충남 금산군에 위치한 산화적지에서 산화후 개벌지역과 비개벌지역을 대상으로 산림식생의 존재여부가 산림토양의 이화학적 성질 변화로 인한 수저유능력에 미치는 영향을 파악하기 위해 가비중, 공극율(조공극 및 세공극), 투수성, 통기성 및 유기물 함량을 비교 분석하였다. 주요 측정인자들에 의해 얻어진 결과는 다음과 같다. 산화지역의 비개벌지 및 개벌지에서 토양 통기성과 투수성을 측정한 결과 비개벌지가 개벌지 보다 양호하였으며, 특히 산정보다는 산록부근에서 가장 큰 차이를 보였다. 또한 산화 뒤 2년이 경과된 후 가장 큰 변화가 나타난 부분은 표토 5∼15cm층이었다. 토양공극 분포는 비개벌지가 개벌지 보다 전공극, 조공극, 세공극이 높게 나타났으며, 토심이 증가함에 따라 전공극량과 조공극량은 감소하였다. 토양가비중은 비개벌지가 개벌지 보다 낮게 나타났으며, 토심이 증가할수록 높게 나타났다. 또한 산록>산복>산정 순으로 통기성, 투수성, 전공극 등이 동일하게 나타났다. 유기물함량은 비개벌지가 개벌지 보다 높았으며 토심이 증가할수록 감소하였다. 토심의 증가에 따라 토양가비중은 정의 상관관계를 나타냈고, 전공극량, 조공극, 통기성, 투수성 및 유기물함량은 부의 상관관계를 나타내었다. 산화적지에서 개벌에 따른 산림환경 변화는 토양의 물리성 및 화학성을 악화시키는 것으로 나타났다.

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Computer Tomography as a Tool for Physical Analysis in an Anthropogenic Soil

  • Chun, Hyen Chung;Park, Chan Won;Sonn, Yeon Kyu;Cho, Hyun Joon;Hyun, Byung Keun;Song, Kwan Cheol;Zhang, Yong Seon
    • 한국토양비료학회지
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    • 제46권6호
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    • pp.549-555
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    • 2013
  • Human influence on soil formation has dramatically increased as the development of human civilization and industry. Increase of anthropogenic soils induced research of those soils; classification, chemical and physical characteristics and plant growth of anthropogenic soils. However there have been no reports on soil pore properties from the anthropogenic soils so far. Therefore the objectives of this study were to test computer tomography (CT) to characterize physical properties of an anthropogenic paddy field soil and to find differences between natural and anthropogenic paddy field soils. Soil samples of a natural paddy field were taken from Ansung, Gyeonggi-do (Ansung site), and samples of an anthropogenic paddy field were from Gumi in Gyeongsangnam-do (Gasan) where paddy fields were remodeled in 2011-2012. Samples were taken at three different depths and analyzed for routine physical properties and CT scans. CT scan provided 3 dimensional images to calculate pore size, length and tortuosity of soil pores. Fractal analysis was applied to quantify pore structure within soil images. The results of measured physical properties (bulk density, porosity) did not show differences across depths and sites, but hardness and water content had differences. These differences repeated within the results of pore morphology. Top soil samples from both sites had greater pore numbers and sizes than others. Fractal analyses showed that top soils had more heterogeneous pore structures than others. The bottom layer of the Gasan site showed more degradation of pore properties than ploughpan and bottom layers from the Ansung site. These results concluded that anthropogenic soils may have more degraded pore properties as depth increases. The remodeled paddy fields may need more fundamental remediation to improve physical conditions. This study suggests that pore analyses using CT can provide important information of physical conditions from anthropogenic soils.