• 제목/요약/키워드: plasma spray

검색결과 336건 처리시간 0.029초

고체산화물 연료전지를 위한 플라즈마 용사코팅 Ni/YSZ 음극 복합체의 특성평가 (Characterization of Ni/YSZ Anode Coating for Solid Oxide Fuel Cells by Atmospheric Plasma Spray Method)

  • 박수동;윤상훈;강기철;이창희
    • Journal of Welding and Joining
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    • 제26권4호
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    • pp.50-54
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    • 2008
  • In this research, anode for SOFC has been manufactured from two different kinds of feedstock materials through thermal spraying process and the properties of the coatings were characterized and compared. One kind of feedstock was manufactured from spray drying method which includes nano-components of NiO, YSZ (300 nm) and graphite. And the other is manufactured by blending the micron size NiO coated graphite, YSZ and graphite powders as feedstock materials. Microstructure, mechanical properties and electrical conductivity of the coatings as-sprayed, after oxidation and after hydrogen reduction containing nano composite which is prepared from spray-dried powders were evaluated and compared with the same properties of the coatings prepared from blended powder feedstock. The coatings prepared from the spray dried powders has better properties as they provide larger triple phase boundaries for hydrogen oxidation reaction and is expected to have lower polarization loss for SOFC anode applications than that of the coatings prepared from blended feedstock. A maximum electrical conductivity of 651 S/cm at $800^{\circ}C$ was achieved for the coatings from spray dried powders which much more than that of the average value.

Spray-ICP technique에 의한 $SnO_2$미분말 합성 및 박막 제조 (Synthesis of ultrafine particles and thin films of $SnO_2$ by the spray-ICP technique)

  • 김정환;박종현;김영도;신건철
    • 한국결정성장학회지
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    • 제8권3호
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    • pp.487-492
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    • 1998
  • ICP(Inductively Coupled Plasma)를 열원으로 출발용액의 농도변화 및 $TiO_2$ 첨가로 $SnO_2$$(Sn,Ti)O_2$미분말을 합성하였으며 SnO2 박막을 제조하였다. 각각 합성된 $SnO_2$ 미분말은 모두 tetragonal의 rutile형으로서 입자들의 평균입경은 30nm로 매우 미세하였으며, 좁은 입도분포를 나타내었다. $TiO_2$를 첨가하였을 경우 $SnO_2-TiO_2$ 미분말은 고용체를 이루었으며, 첨가량이 증가함에 따라 결정성은 감소하였다. ICP tail flame으로 fused quartz 기판을 가열하여 (101)면을 주 peak로 하는 $SnO_2$ 박막을 얻었다.

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정전기 분무 열분해법에 의한 MgO 박막 증착과 AC-PDP로의 용용에 대한 연구 (Deposition of MgO Thin Films by Electrostatic Spray Pyrolysis(ESP) method and Application to AC-PDP)

  • 김수길;은재환;김형준;김영기;박정후
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2000년도 춘계학술대회 논문집 디스플레이 광소자 분야
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    • pp.133-138
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    • 2000
  • MgO thin films were deposited using $Mg(tmhd)_2$ as a precursor dissolved in a solvent by electrostatic spray pyrolysis. When a pure tetra hydro furan was used as a solvent, a large number of particles appeared on the MgO thin film surface due to homogeneous nucleation. However, by adding 1-butyl alcohol or 1-octyl alcohol to THF, homogeneous nucleation was restricted and the number density of the large particles was also drastically reduced. X-ray diffraction analysis showed that the MgO films had a (100) preferred orientation regardless of the type of solvents used. Characterization using Fourier Transformed-Infrared and spectroscopic photometer revealed that the crystallized MgO thin films on the glass substrate had a high optical transmittance (> 85 %) in the visible range. Discharge characteristics of MgO thin films deposited by ESP method on an alternating-current plasma display panel were compared with a MgO thin film prepared by reactive radio-frequency planar magnetron sputtering.

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Value of spray-dried egg in pig nursery diets

  • Song, Minho;Kim, Sheena;Kim, Younghwa;Park, Juncheol;Kim, Younghoon
    • 농업과학연구
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    • 제42권3호
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    • pp.207-213
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    • 2015
  • High-quality protein ingredients have been used in nursery diets, in spite of expensive ingredients, to minimize nutritional deficiency and disease problems. Recent dramatic increases in prices of protein products for nursery diets have exacerbated the challenge. Spray-dried egg may be a part of the solutions. Therefore, this review describes the value of spray-dried egg in nursery diets as a high-quality protein source. Spray-dried egg is egg by-product and is produced by only eggs without shell that are below the USDA Grade B standards. Spray-dried egg is an excellent nutrient source: 1) highly digestible, 2) excellent balance of amino acids, 3) rich content of fat, and 4) high metabolizable energy. These can be attributed to growth of nursery pigs. Beyond the provision of bioavailable nutrients, spray-dried egg also may provide specific physiological benefits. Spray-dried egg contains 1) immunoglobulin antibodies (IgY: IgG in egg yolk) that may attach to intestinal pathogens and excrete them and 2) lysozymes antimicrobial protein that can damage bacteria cell wall. Thereby feeding spray-dried egg may reduce concentration of intestinal pathogen and thus improve potential gut health or enteric disease resistance in nursery pigs. This is important for physiologically immature weaned pigs. Based on these benefits, spray-dried egg is believed to have the same benefits as spray-dried plasma protein and milk products in diets for nursery pigs. Therefore, it is suggested that spray-dried egg has a great potential as a valuable protein source in nursery diets.

용사법에 의한 주철제 표면개질부의 내마모성 연구 (A study on the anti-wear properties of surface modified cast iron by metal spray method)

  • 이광렬;최영국;김영식
    • 한국해양공학회:학술대회논문집
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    • 한국해양공학회 2002년도 추계학술대회 논문집
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    • pp.312-317
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    • 2002
  • A experimental try was conducted for the purpose of establishment of the cast iron modification by the metal spray method. The friction and wear resistance properties of the metal sprayed cast iron surface were evaluated. The application experiment for the cast iron modification by the metal spray method was conducted in order to develope the restoring method of the scrapped cast iron cylinder liner of the marine engine.

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Particle Deposition, PD Process - New Potential in Material Processing -

  • Fukumoto, Masahiro
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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    • pp.47-48
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    • 2006
  • Oridinal thermal spray process has developed into two ways, namely, temperature dominated represented by plasma spraying, and velocity dominated represented by HVOF. It is common for both that the particle materials sprayed are basically in melted or half melted condition. New process has developed recently, that is, Cold Spray and Aerosol Deposition. Particle's heating is limited in CS lower than half of the material's melting point. Moreover, exactly no heating is loaded in AD process. Through the investigation on common feature for these three spraying processes, potential of new material process - Particle Deposition, PD - is considered and proposed.

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대기 플라즈마 용사공정을 이용한 Fe계 벌크 비정질 금속 코팅의 초기 분말의 화학조성과 크기에 대한 미세 조직 및 마모 특성 (Microstructure and Tribological Properties along with Chemical Composition and Size of Initial Powder in Fe-based BMG Coating through APS)

  • 김정환;윤상훈;나현택;이창희
    • 한국표면공학회지
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    • 제41권5호
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    • pp.220-225
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    • 2008
  • In this study, two kinds of Fe-based bulk metallic glasses (BMG) powder were built-up through atmospheric plasma spray (APS) technique. The microstructure of two coatings was analyzed through X-ray diffraction, scanning electron microscopy and transmission electron microscopy. Crystallization and oxidation in coatings were affected by chemical composition and initial powder size. Then, both of them influenced the tribological property.

가스터빈 블레이드 열차폐 코팅의 접착강도 평가 (Evaluation of a Bond Strength of Thermal Barrier Coating for Gas Turbine Blade)

  • 김대진;이동훈;김형익;김문영;양성호;박상열;구재민;석창성
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2007년도 춘계학술대회A
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    • pp.195-199
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    • 2007
  • In this study, bond strength tests were performed for the thermal barrier coating applied to the 1st stage turbine blade. After the tests, the specimens were cut and the locations of failure were observed by using optical microscope. The influence of heat treatment on bond strength of a bond coating and the difference among the three types of bond coatings are treated.

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유압실린더 세라믹코팅 기공률 최소화 방안 (Minimization of Porosity in Ceramic Coating on a Hydraulic Cylinder)

  • 정영호;문승재;유호선
    • 플랜트 저널
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    • 제6권4호
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    • pp.63-71
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    • 2010
  • The best way to prevent the corrosion of piston rod is a selection of quality of the material and method of construction which minimize the porosity. The high velocity oxy fuel(HVOF) method, which generates lower porosity than existing plasma spray, was applied to ceramic laminated bond layer. Porosity percentage fell to bellow 2%, lower than that of plasma spray at 7%. Coating material of ceramic-coated main layer was selected as the $Cr_2O_3$ affiliation material, which is more dense than $Al_2O_3$ affiliation. To fill up the pores formed after the coating process, we sealed the bond layer and main layer. Sealing process was performed twice, once after the coating and once after the grinding. Upon the anti-corrosion test on the sealed sample and on the non-sealed sample, it is confirmed that the sealed sample was not corroded for 1,000 hours while the non-sealed sample was corroded within 48 hours.

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Characterion of Calcium Phosphate Films Grown on Surgicl Ti-6AI-4V By Ion Beam Assisted Deposition

  • Lee, I-S.;Song, J-S.;Choi, J-M;Kim, H-E.
    • 한국진공학회지
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    • 제7권s1호
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    • pp.30-36
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    • 1998
  • The plasma-spray technique is currently the most frequently used method to produce calcium phosphate coatings. Hydroxyapatite(HAp), one form of calcium phosphate, is preferred by its ability to form a direct bond with living bone, resulting in improvements of implant fixation and faster bone healing. Recently, concerns have been raised regarding the viable use and long-term stability of plasma-spray HAp coatings due to its nature of comparatively thick, porous, and poor bonding strength to metal implants. Thin layers (maximum of few microns) of calcium phosphate were formed by an e-beam evaporation with and without ion bombardments. The Ca/P ration of film was controlled by either using the evaporants having the different ration of Ca/P with addition of CaO, or adjusting the ion beam assist current. The Ca/P ration had great effects on the structure formation after heat treatment and the dissolution bahavior. The calcium phosphate films produced by IBAD exhibited high adhesion strength.

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