• Title/Summary/Keyword: pitting

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Duplex Surface Modification with Micro-arc Discharge Oxidation and Magnetron Sputtering for Aluminum Alloys

  • Tong, Honghui;Jin, Fanya;He, Heng
    • Journal of the Korean Vacuum Society
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    • v.12 no.S1
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    • pp.21-27
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    • 2003
  • Micro-arc discharge oxidation (MDO) is a cost-effective plasma electrolytic process which can be used to improve the wear and corrosion resistance of Al-alloy parts by forming a alumina coating on the component surface. However, the MDO coated Al-alloy components often exhibit relatively high friction coefficients and low wear resistance fitted with many counterface materials, additionally, the pitting corrosion for the MDO coated AI-alloy components, especially for a thinner alumina coating, often occurs in atmosphere circumstance due to the porous alumina coats. Therefore, a duplex treatment, combining a MDO coated ahumina thin layer with a TiN coating, prepared by magnetron sputtering (MS), has been investigated. The Vicker's microhardness, pin-on-disc, electrochemical measurement, salt spray, XRD and SEM tests were used to characterize and analyze the treated samples. The work demonstrates that the MDO/MS coated samples have a combination of a very low friction coefficient and good wear resistance as well as corrosion since the micro-holes on alumina coating are partly or fully covered by TiN material.

An Evaluation of the Effect of Internal Thinning Defect on the Failure Pressure of Elbow (곡관의 손상압력에 미치는 내부 감육결함의 영향 평가)

  • Kim, Jin-Weon;Kim, Tae-Soon;Park, Chi-Yong
    • Journal of the Korean Society of Safety
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    • v.18 no.4
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    • pp.28-34
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    • 2003
  • In the present study, three-dimensional finite element analysis was performed to investigate the effects of internal wall thinning defect on the failure pressure of elbow in the piping system and to develop the failure pressure evaluation model. From the results of finite element analysis, the failure pressure was derived by employing local stress criteria, and the effects of thinning location, bend radius, and defect geometry on the failure pressure of internally wall thinned elbow were investigated. Also, based on these investigations and previous model developed to estimate the failure pressure of elbow with an external pitting defect, the failure pressure evaluation model to be applicable to the elbow containing an internal thinning defect was proposed and compared with the results of finite element analysis. The failure pressure calculated by the model agreed well with the results of finite element analysis.

Fabrication of Plasma Electrolytic Oxidation Coatings on Magnesium AZ91D Casting Alloys

  • Lee, Sung-Hyung;Yashiro, Hitoshi;Kure-Chu, Song-Zhu
    • Journal of Surface Science and Engineering
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    • v.50 no.6
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    • pp.432-438
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    • 2017
  • AZ91D casting alloy requires an advanced plasma anodizing processing because large amount of defects are liable to generate during anodization. In this study, plasma electrolytic oxidation (PEO) of AZ91D Mg alloy was conducted by the application of either constant voltage or current using a pulse mode and its effects on pore formation, surface roughness and corrosion resistance were investigated. The PEO films showed a three-layer structure. The PEO film thickness was found to increase linearly with voltage. The surface roughness, Ra, ranged between $0.2{\mu}m$ and $0.3{\mu}m$. The corrosion resistance increased from RN 3.5 to 9.5 by the PEO treatment when evaluated according to the 72 hour salt spray test. The PEO-treated surface exhibited higher pitting potential than the raw material.

Effect of ICCP Potential with Electrolyte on Corrosion and Discolor of Silver (은의 부식 및 변식에 미치는 전해질 용액에 따른 ICCP 전압의 영향)

  • Shin, Byung-Hyun;Kim, Do-Hyung;Chung, Won-Sub
    • Journal of Surface Science and Engineering
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    • v.53 no.5
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    • pp.207-212
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    • 2020
  • Silver is an inexpensive precious metal and is used in various jewelry in Asia. Although silver has high potential, it has corrosion resistance that is vulnerable to boiling sulfuric acid and nitric acid. So, silver research is needed to prevent the corrosion with environment. But silver corrosion is not studied. sulfuric acid make the uniform corrosion and chloride ion make the pitting corrosion. ICCP inhibits the corrosion because it offset electrons. This study used a potential from - 4 V to 4 V to check the effect of potential. Corrosion rate is lowet at -1 V.

Sintered Duplex Stainless Steels Corrosion Properties

  • Dobrzanski, L.A.;Brytan, Z.;Grande, M. Actis;Rossob, M.;Park, Woo-Young;Kim, Cheol-Su
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.583-584
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    • 2006
  • This work presents mechanical properties and corrosion resistance of duplex stainless steels obtained through powder metallurgy starting from austenitic, martensitic powders by controlled addition of alloying elements in the right quantity to obtain the chemical composition of the structure similar to biphasic one. In the mixes preparations the Schaffler's diagram was taken into consideration. Prepared mixes of powders have been sintered in a vacuum furnace with argon backfilling. After sintering rapid cooling was applied using nitrogen. Corrosion properties have been studied through electrochemical methods in 1M NaCl.

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Faults Detection of Industrial Gearbox using an Envelope Analysis (포락선 분석을 이용한 산업용 기어박스의 결함 검출)

  • Park, Y.J.;Lee, G.H.;Lee, J.J.
    • Journal of Biosystems Engineering
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    • v.34 no.2
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    • pp.82-88
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    • 2009
  • This study was conducted to detect faults in a gearbox comprised of gears, bearings and shafts. The envelope analysis was used as a method of detection, which could detect breakage and pitting of gears and bearings, and misalignment of shafts effectively. Vibration measured at the increaser was analyzed to characterize the faults. When the increaser has a defect, peaks with a constant period appear in the time history of vibration and its harmonic components also in the envelope spectrum. The envelope analysis showed that a crack in the stepped output shaft caused the increaser to generate the abnormal peaks.

Electrochemical Characteristics of Arc Thermal Sprayed Inconel 625 Coating on SS400 Steel in Seawater (Inconel 625로 아크 용사코팅된 SS400강의 해수 내 전기화학적 특성)

  • Park, Il-Cho;Kim, Seong-Jong
    • Journal of Surface Science and Engineering
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    • v.49 no.2
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    • pp.172-177
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    • 2016
  • In this paper, various electrochemical experiments were conducted in seawater solution to evaluate corrosion damage behavior of arc thermal sprayed Inconel 625 coating on SS400 steel in marine environment. As a result, corrosion damages of thermal sprayed Inconel 625 coating preferentially occurred at the defect area, and they were observed as a form of pitting corrosion in the galvanostatic experiments. In Tafel analysis, corrosion current density of Inconel 625 coating was relatively high due to influence of interconnected pores and Cr oxides in the thermal spray coating layer. On the other hand, the result of the potential measurement, thermal sprayed Inconel 625 coating should need the post-treatment which can compensate the defects like pores and cracks because Inconel 625 coating presented a higher potential of about 290 mV than that of the SS400 steel.

Mechanical Properties and Microstructure of Ni-0.9wt%P Electroformed Layer (Ni-0.9wt%P 전주층의 기계적 특성 및 미세조직)

  • 정현규;서무홍;김정수;천병선;김승호
    • Journal of Surface Science and Engineering
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    • v.34 no.4
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    • pp.289-296
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    • 2001
  • Ni-P electroformed layers were investigated for developing a steam generator tube repair technology in PWRs. The effects of an additive, RPP (Reagent over Pitting Protection) and agitation on mechanical properties and microstructure of the layer were evaluated. The addition of the RPP showed to inhibit the formation of pores, to refine the grain size, and to increase the residual stress in the layer. However, the agitation of the solution during electroforming was observed to increase pores in local regions of the electroformed layer, resulting in decreasing its mechanical properties. The heat treatment of the layer at $343^{\circ}C$ for 1 hr. precipitated the very fine particles of Ni3P in the layer, which inhibited grain growth and increased microhardness.

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Surface Characteristics of Stainless Steel Wire for Dental and Medical Use (치과 및 의료용 스테인리스강선의 표면특성)

  • 최한철;고영무
    • Journal of Surface Science and Engineering
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    • v.36 no.4
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    • pp.339-346
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    • 2003
  • Stainless steel wire has been used in industry, dental and medical parts. Especially, it has been used widely for the dental orthodontic materials. The orthodontic wire requires good mechanical properties, such as elastic strength, combined with a high resistance to corrosion. To increase elastic strength and good corrosion resistance, drawing methods(one-step and two-step drawing) have been used and the electrochemical characteristics of drawed wire have been researched using potentiodynamic method in 0.9%NaCl and field emission scanning electron microscope. The one-step drawed wire showed the formation of rough surface. The hardness and tensile strength of two-step drawed wire increased. For the case of two-step drawed wire, the corrosion resistance and pitting potential increased compared with one-step drawed wire due to the drawing induced small surface roughness, such as scratch. The passivation and active current density decreased as the reduction in area for drawing increased.

Effects of Plasma Nitriding on the Surface Charcteristice Of Stainless Steels (스테인스강의 표면특성에 미치는 플라즈마질화의 영향)

  • 최한철;김관휴
    • Journal of Surface Science and Engineering
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    • v.30 no.2
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    • pp.144-154
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    • 1997
  • Effects of plasma nitriding on the surface charcteristice of stainless steel(SS) were investjgated by utilizing wear tester, micro-hardness tester and potentiostat. The surface and corrosion morphology of plasma nitrided SS were analyzed by utilizing optical microscopy, SEM, XRD and WDX. It was found that plasma nitriding at $550^{\circ}C$, compared with $380^{\circ}C$, prodiced a good wear resistance and hardness as nitriding time increased, whereas Mo addition showd that were resistance and hardness decreased. Intergranular corrosion(IGC) resistance improved significantly in the case of plasma nirtrided SS containing 4.05wt% Mo at $380^{\circ}C$ because that nitrogen and Mo ast syner gidically to form a protective layer on surface which is responsible for the aggresive SCN-ion. Plasma nitrided at $550^{\circ}C$ decreased IGC as Mo content increased. Pitting improved in the plasma nitirided SS at Mo content incresased owing to retard a nucleation and growth of chromium carbide or nitirde in grain boundary.

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