• Title/Summary/Keyword: physical characterization

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Development and Characterization of High Temperature Filter (내열성여과포의 개발 및 기초성능 규명)

  • 박영옥;구철오;임정환;김홍룡;손재익;이영우
    • Journal of Energy Engineering
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    • v.7 no.1
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    • pp.103-112
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    • 1998
  • A high temperature fabric filter was developed and characterized in order to solve the various problems encountered in the operation of industrial fabric filters. Four kinds of dusts generated in the typical domestic industry were used for its characterization, coke dust from a steel manufacturing process, cement dust from a cement manufacturing process, fly ash from a fluidized-bed combustor, and incinerator ash from a waste plastics incinerator. The physical and chemical properties of the high temperature fabric filter were analyzed in terms of mean flow pore pressure, bubble point pore diameter, mean flow pore diameter, pore size distribution, and the changes in tensile strength and initial elastic modulus under $SO_2$ and $NO_2$ atmospheres. Pressure drop, dust penetration, and figure of merit for the fabric filter were also investigated in a bench-scale filter testing unit. The fabric filter developed in this study had good physical and chemical filter properties and showed a very applicability to typical industrial dusts treatments.

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DEEP-South: Round-the-Clock Physical Characterization and Survey of Small Solar System Bodies in the Southern Sky

  • Moon, Hong-Kyu;Kim, Myung-Jin;Roh, Dong-Goo;Park, Jintae;Yim, Hong-Suh;Choi, Young-Jun;Bae, Young-Ho;Lee, Hee-Jae;Oh, Young-Seok
    • The Bulletin of The Korean Astronomical Society
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    • v.41 no.1
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    • pp.54.2-54.2
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    • 2016
  • Korea Microlensing Telescope Network (KMTNet) is the first optical survey system of its kind in a way that three KMTNet observatories are longitudinally well-separated, and thus have the benefit of 24-hour continuous monitoring of the southern sky. The wide-field and round-the-clock operation capabilities of this network facility are ideal for survey and the physical characterization of small Solar System bodies. We obtain their orbits, absolute magnitudes (H), three dimensional shape models, spin periods and spin states, activity levels based on the time-series broadband photometry. Their approximate surface mineralogy is also identified using colors and band slopes. The automated observation scheduler, the data pipeline, the dedicated computing facility, related research activity and the team members are collectively called 'DEEP-South' (DEep Ecliptic Patrol of Southern sky). DEEP-South observation is being made during the off-season for exoplanet search, yet part of the telescope time is shared in the period between when the Galactic bulge rises early in the morning and sets early in the evening. We present here the observation mode, strategy, software, test runs, early results, and the future plan of DEEP-South.

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Characterization of Albino Tobaccos (Nicotiana tabacum L.) Derived from Leaf Blade-Segments Cultured in vitro

  • Bae, Chang-Hyu;Tomoko Abe;Lee, Hyo-Yeon;Kim, Dong-Cheol;Min, Kyung-Soo;Park, Kwan-Sam;Tomoki Matsuyama;Takeshi Nakano;Shigeo Yoshida
    • Journal of Plant Biotechnology
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    • v.1 no.2
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    • pp.101-107
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    • 1999
  • The leaf blade-segments of albino tobacco (Nicotiana tabacum L.) were cultured on MS media containing different concentrations of BAP (0, 0.4, 2.2, 4.4, 22.2 ${\mu}{\textrm}{m}$) with or without NAA (0, 0.5, 2.7 ${\mu}{\textrm}{m}$). Multiple shoots were induced on the media containing 0.4 to 2.2 ${\mu}{\textrm}{m}$ BAP. The best condition for multiple shoot induction with root formation was MS media containing 4.4 ${\mu}{\textrm}{m}$ BAP and 0.5 ${\mu}{\textrm}{m}$ NAA. The regenerated albino plants showed a significant reduction in accumulation of chlorophylls and carotenoids. The drastic reduction of the pigments content was associated with the distinct alterations in gene expression in the albino plants. firstly, the expression of plastid genes, such as rbcL, psbA, 165 rDNA and 235 rDNA, was reduced at the level of transcripts in the regenerated albino plants. Secondly, the alteration of structure of the plastid genes was not detected in the albino plants. However, the copy number of the plastid genes whose transcription level was reduced greatly was increased approximately two-fold, although the transcriptions of nuclear gene (255 rDNA) showed the wild-type level.

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Characterization of Physical Quality of Rice based on Reheating Process (재가열에 따른 벼 품종별 밥의 물리적 품질 특성)

  • Kim, Hyun-Joo;Woo, Koan Sik;Lee, Seuk Ki;Lee, Byong Won;Lee, Jihae;Lee, Yu-Young;Lee, Byoungkyu
    • The Korean Journal of Food And Nutrition
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    • v.31 no.5
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    • pp.760-765
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    • 2018
  • In order to observe physical properties of rice depending on reheating, the study cooked rice developed for high quality cooked rice and analyzed physical properties of rice depending on reheating following 24 hr refrigeration. As a result of palatability of cooked rice, Samgkwang had the lowest hardness, while Daebo and Haiami had the highest one. With respect to adhesiveness, toughness and stickiness, Sindongjin exhibited lowest properties. After cooking each rice by cultivars, the study observed their color, texture properties, and microstructure immediately after cooking, after 24 hr of refrigeration and further on. Lightness of cooked rice tended to drop because of refrigeration and reheating. Analysis of texture properties after cooking revealed that Haiami marked the highest points in all categories. When stored for 24 hr after cooking, hardness, viscosity and chewiness increased in cooked rice followed by a decrease after reheating. Observation of the microstructure of cooked rice using a scanning electron microscope revealed that Haiami had its particles in the center as closely condensed. It was apparent that all the cultivars formed stoma in an obvious manner because of refrigeration and reheating. The results of the present study show that physical properties of cooked rice varied according to reheating after cooking and storage depending on the inherent characteristics of rice cultivars.

Electrical/Optical Characterization of PZT Thin Films Deposited through Sol-Gel Processing

  • Hwang, Hee-Soo;Kwon, Kyoeng-Woo;Choi, Jeong-Wan;Do, Woo-Ri;Hwang, Jin-Ha
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.08a
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    • pp.361-361
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    • 2012
  • PZT (Pb(Zr,Ti)O3) thin films have been used widely in the MEMS application, due to their inherent ferroelectric and piezoelectric properties. Such ferroelectricity induces much higher dielectric constants compared to those of the nonperovskite materials. In this work, the PZT thin films were deposited onto Indium-Tin-oxide (ITO) substrates through the spin-coating of PZT sols. The deposited PZT thin films were characterized in terms of the electrical and optical properties with special emphases on conductivity and optical constants. The detailed analysis techniques incorporate the dc-based current-voltage characteristics for the electrical properties, spectroscopic ellipsometry for optical characterization, atomic force microscopy for surface morphology, X-ray Photoelectron Spectroscopy for chemical bonding, Energy-dispersive X-ray Spectrometry for chemical analyses and X-ray diffraction for crystallinity. The ferroelectric phenomena were confirmed using capacitance-voltage measurements. The integrated physical/chemical features are attempted towards energy-oriented applications applicable to next-generation high-efficiency power generation systems.

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Synthesis of Nanosized Titanium-Colloid by Sol-Gel Method and Characterization of Zinc Phosphating (졸-겔법에 의한 나노크기의 티탄-콜로이드 합성 및 인산염 피막 특성)

  • Lee Man Sig;Lee Sun-Do
    • Journal of the Korean institute of surface engineering
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    • v.38 no.1
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    • pp.37-43
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    • 2005
  • Nanosized titanium-colloid particles were prepared by sol-gel method. The physical properties, such as thermal stability, crystallite size and crystallinity according to synthesis condition have been investigated by TEM, XRD, SEM, TGA and DTA. In addition, Zinc phosphating has been studied in order to compare the phosphating characterization of prepared nanosized titanium-colloid particles. The major phase of all the prepared titanium-colloid particles was an amorphous structure regardless of synthesis temperature and the structure was composed of phoshate complex and titanium. The micrographs of HR- TEM showed that nanosized titanium-colloid particles possessed a spherical morphology with a narrow size distribution. The crystallite size of the titanium-colloid particles synthesized at 80℃ was 4-5 nm and increased to 8-10 nm with an increase of synthesis temperature (150℃). In addition, the coating weight increased with an increase of temperature of phosphating solution and when the concentration of titanium-colloid was 2.0 g/l, the coating weight was 1.0 g/㎡.

Characterization of Nafion/Pt/Polypyrrole Composite Membrane Prepared by Chemical In-situ Polymerization for DMFC (화학적 합성에 의해 제조된 직접 메탄올 연료전지용 나피온/백금/폴리피롤 복합 막의 특성 분석)

  • Park, Ho-Seok;Kim, Yo-Jin;Im, Hun-Suk;Choi, Bong-Gill;Hong, Won-Hi
    • 한국신재생에너지학회:학술대회논문집
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    • 2006.11a
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    • pp.421-424
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    • 2006
  • Nafion/Pt/Polypyrrole composite membranes were fabricated by chemical in-situ polymerization of pyrrole monomers with Pt precursors in Nafion matrix for DMFC. We demonstrated that positively charged pyrrolinum groups of polypyrrole particles were co-interacted with sulfonic groups of Nafion as verified by FT-IR results. Mutual interaction between $Nafion-SO_3^-$ (or negatively charged Pt precursors) and Polypyrrole$-NH_2^+$ influenced the physical properties of pristine Nafion. Thermal property proton conductivity, methanol permeability, and cell performance of pristine and modified Nafion were analyzed for an application of DMFC membrane. Thermal stabilities of sulfonic groups and side chains in Nafion/Pt/polypyrrole composite membranes were higher than those of Nafion due to mutual interaction between sulfonic groups of Nafion and pyrrolinum groups of polypyrrole. Methanol permeabilities of Nafion/Pt/Polypyrrole composite were reduced more proton conductivities with the increase in the content of Pt particles. As a result of that, the enhancement of cell performance by Nafion/Pt/Polypyrole O2 relative to Nafion was more pronounced under the specific experimental condition such as high temperature and more concentrated methanol solution.

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Characterization and Detection of Location Spoofing Attacks

  • Lee, Jeong-Heon;Buehrer, R. Michael
    • Journal of Communications and Networks
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    • v.14 no.4
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    • pp.396-409
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    • 2012
  • With the proliferation of diverse wireless devices, there is an increasing concern about the security of location information which can be spoofed or disrupted by adversaries. This paper investigates the characterization and detection of location spoofing attacks, specifically those which are attempting to falsify (degrade) the position estimate through signal strength based attacks. Since the physical-layer approach identifies and assesses the security risk of position information based solely on using received signal strength (RSS), it is applicable to nearly any practical wireless network. In this paper, we characterize the impact of signal strength and beamforming attacks on range estimates and the resulting position estimate. It is shown that such attacks can be characterized by a scaling factor that biases the individual range estimators either uniformly or selectively. We then identify the more severe types of attacks, and develop an attack detection approach which does not rely on a priori knowledge (either statistical or environmental). The resulting approach, which exploits the dissimilar behavior of two RSS-based estimators when under attack, is shown to be effective at detecting both types of attacks with the detection rate increasing with the severity of the induced location error.

Electrochemical Oxidation of Amoxicillin in Its Commercial Formulation on Thermally Prepared RuO2/Ti

  • Auguste, Appia Foffie Thiery;Quand-Meme, Gnamba Corneil;Ollo, Kambire;Mohamed, Berte;Sahi placide, Sadia;Ibrahima, Sanogo;Lassine, Ouattara
    • Journal of Electrochemical Science and Technology
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    • v.7 no.1
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    • pp.82-89
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    • 2016
  • In this work, a ruthenium dioxide electrode has been prepared by thermal decomposition at 400 ℃ then used for the oxidation of commercial amoxicillin. The physical characterization showed that RuO2 electrode presents a mud cracked structure. Its electrochemical characterization has revealed an increase of the voltammetric charge in acid electrolyte compared to neutral electrolyte indicating the importance of protons in its surface redox processes. The voltammetric study of the oxidation of amoxicillin has been investigated. It has been obtained that the oxidation of amoxicillin is controlled by both adsorption and diffusion processes. Moreover, the oxidation of amoxicillin occurs via direct and indirect processes in free or electrolyte containing chlorides. Through preparative electrolysis, enhancement of amoxicillin oxidation was observed in the presence of chloride where the amoxicillin degradation yield reached more than 50 % compared to less than 5% in the absence of chlorides. Spectrophotometric investigations have revealed the degradation of intermediates absorbing at 350 nm.

Characterization and Early Age Physical Properties of Ambient Cured Geopolymer Mortar Based on Class C Fly Ash

  • Kotwal, Ashley Russell;Kim, Yoo Jae;Hu, Jiong;Sriraman, Vedaraman
    • International Journal of Concrete Structures and Materials
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    • v.9 no.1
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    • pp.35-43
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    • 2015
  • The critical element for sustainable growth in the construction industry is the development of alternative cements. A new technological process called geopolymerization provides an innovative solution, and the presence of aluminum and silicon oxides in fly ash has encouraged its use as a source material. Many previous investigations have involved curing the binder in a heated environment. To reduce energy consumption during the synthesis of geopolymers, the present study investigated the properties of ambient cured geopolymer mortar at early ages. An experimental program was executed to establish a relationship between the activator composition and the properties of geopolymer mortar in fresh and hardened states. Concentrations of sodium hydroxide and sodium silicate were ascertained that are advantageous for constructability and mechanical behavior. Scanning electron microscopy, energy dispersive X-ray spectroscopy and X-ray diffraction techniques were also used to characterize the material. Test results indicate that there is potential for the concrete industry to use fly ash based geopolymer as an alternative to portland cement.