• 제목/요약/키워드: physical and drying properties

검색결과 258건 처리시간 0.035초

A Study on Kaolin and Titanium dioxide affecting Physical Properties of Electrocoating

  • Yang, Wonseog;Hwang, Woonsuk
    • Corrosion Science and Technology
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    • 제12권5호
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    • pp.203-208
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    • 2013
  • The electrocoating for automotive bodies is pigmented with a mixture of titanium dioxide and kaolin. In this study, the effects of titanium dioxide and kaolin contents in coating on electrodeposition process, drying, and surface properties such as surface roughness, gloss, impact resistance and corrosion resistance were investigated. Titanium dioxide and kaolin in coating do not have a decisive effect on curing reaction during drying and corrosion resistance but on gloss, surface roughness, impact resistance and electrodeposition process of coating. According to its size and shape on coating surface, pigment contents increased during drying process. However, the contents of kaolin and $TiO_2$ in coating didn't affect the corrosion resistance on zinc phosphated substrate, and the curing properties.

화학적 박리법으로 제조된 산화그래핀 분말의 건조방법에 따른 물성 비교 (Effect of Drying Methods on the Production of Graphenes Oxide Powder Prepared by Chemical Exfoliation)

  • 노상균;노경훈;엄성훈;허승현;임형미
    • 한국재료학회지
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    • 제23권10호
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    • pp.592-598
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    • 2013
  • Graphene oxide powders prepared by two different drying processes, freeze drying and spray drying, were studied to compare the effect of the drying method on the physical properties of graphene oxide powder. The graphene oxide dispersion was prepared from graphite by chemical delamination with the aid of sulfuric acid and permanganic acid, and the dispersion was further washed and re-dispersed in a mixed solvent of water and isopropyl alcohol. A freeze drying method can feasibly minimize damage to the sample, but it requires a long process time. In contrast, spray drying is able to remove a solvent in a relatively short time, though this process requires exposure to a high temperature for a rapid evaporation of the solvent. The powders prepared by freeze drying and spray drying were characterized and compared by Raman spectroscopy, X-ray diffraction, field-emission scanning electron microscopy, transmission electron microscopy, and by an elemental analysis. The graphene oxide powders showed similar chemical compositions; however, the morphologies of the powders differed in that the graphene oxide prepared by spray drying had a winkled morphology and a higher apparent density compared to the powder prepared by freeze drying. The graphene oxide powders were reduced at $900^{\circ}C$ in an atmosphere of $N_2$. The effect of the drying process on the properties of the reduced graphene oxide was examined by SEM, TEM and Raman spectroscopy.

Fluidized Bed Drying Effect on the Aerogel Powder Synthesis

  • Hong, Seong-Hoon;Lee, Dong-Kyu;Oh, Chang-Sup;Kim, Yong-Ha
    • 에너지공학
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    • 제21권1호
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    • pp.43-46
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    • 2012
  • A fluidized bed drying approach was utilized to the synthesis of water glass based silica aerogel powders. The effects of the fluidized bed drying conditions such as the superficial velocity and temperature of hot air and bead size as well as bead/wet-gel ratio, on the physical properties such as tapping density and productivity of the aerogel powders were systematically investigated. The experimental results showed that the amount of beads mixed with wet-gels in the fluidized bed column has the most profound impact on the fluidization efficiency, greatly enhancing the yield of the aerogel powders up to 98% with a proper bead/wet-gel weight ratio as compared to 72% without using beads. No significant change was observed in the tapping density over a wide range of the fluidized drying condition. Consequently the fluidized bed drying approach shows a good promise as an alternative route for the large-scale production of the aerogel powders.

순환식 병류형 유채씨 건조 시뮬레이션 (Circulating Concurrent-flow Drying Simulation of Rapeseed)

  • 한재웅;금동혁;김웅;레안득;조성호;김훈
    • Journal of Biosystems Engineering
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    • 제35권6호
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    • pp.401-407
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    • 2010
  • In this study, computer simulations were conducted to assess the use of a circulating concurrent-flow dryer for rapeseed drying and to determined the effect of this drying method on the germination ratio of rapeseed after the drying process was complete. The simultaneous heat and mass transfer between air and rapeseed in a concurrent-flow dryer was examined by simulation. The drying simulation was based on several parameters with sequent time series. Equations concerning air psychrometrics, physical properties, thermal properties, equilibrium moisture content, thin layer drying of rapeseed, etc. were all combined to solve the simulation models. Based on energy and mass transfer in the concurrent-flow drying model, a simulation program for the circulating concurrent-flow rapeseed dryer was built along with a detailed description of the mathematical solution to the model. A pilot scale circulating concurrent-flow dryer(200 kg/batch) was used to verify the fitness of the simulation program. A comparison between the experimental data and the model predicted results was presented and discussed. The drying parameters and germination ratio were analyzed and the accuracy of the simulation program was evaluated. The simulation program proved to be reliable and was shown to be a convenient tool for predicting rapeseed drying and germination ratio of rapeseed in a concurrent-flow dryer.

Atomisation and vacuum drying studies on Malaysian honey encapsulation

  • Nurul Aisyah Rosli;Boon-Beng Lee;Khairul Farihan Kasim;Che Wan Sharifah Robiah Mohamad
    • 한국식품저장유통학회지
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    • 제30권4호
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    • pp.589-601
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    • 2023
  • Malaysian honey is rich in nutrients and bioactive compounds, which can be a healthy alternative to refined sugar in food production. However, liquid honey's viscous and sticky nature makes it unpreferable in industrial handling. This study, an atomization system coupled with vacuum drying to produce honey powders to overcome the problem. Three types of Malaysian honey, namely Acacia, Gelam, and Tualang, were encapsulated in Ca-alginate gel beads using the atomization system. The density viscosity, and surface tension of the honey-alginate solutions were measured, and the concentration of honey and alginate influenced the physical properties of the solutions. Honey-encapsulated gel beads in the size range of 2.16-2.92 mm were produced using the atomization system with the air-liquid mass flow rate ratios of 0.22-0.31, Weber number (We) of 112-545, and Ohnersorges number (Oh) of 0.35-10.46. Gel bead diameter can be predicted using a simple mathematical model. After vacuum drying, the honey gel powder produced was in the size range of 1.50-1.79 mm. Results showed that honey gel powders with good encapsulation efficiency and high honey loading could be produced using the atomization system and vacuum drying.

투석과 건조방법이 다시마(Laminaria japonica) 알긴산의 물성에 미치는 영향 (Effects of Dialysis and Various Drying Methods on Physical Properties of Alginates Prepared from Sea Tangle, Laminaria japonica)

  • 임영선;유병진
    • 한국수산과학회지
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    • 제38권4호
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    • pp.226-231
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    • 2005
  • To investigate the physical properties of sea tangle (Laminaria japonica) alginates, extracted by the Mexican process, the effects of extracting time and drying methods on intrinsic viscosities, MWs and DPs of alginates were examined. The MWs of alginates before and after dialysis decreased with increase of extracting time. The MW s before dialysis were lower than those after dialysis. The ash contents before dialysis decreased with increase of extracting time. After dialysis the ash contents of the alginates showed 10.4-10.9% of those, which were little affected by extracting time. In the ash composition after dialysis, the sodium content was 4.4 g/100 g, $90\%$ of total ash content. The ash contents, the intrinsic viscosities, the average molecular weight and the DPs of the alginates dried by AD before dialysis were higher than those by VF. The ash and uronic acid contents of alginates after dialysis showed $10.6-10.9\%\;and\l88.1-88.9\%$, respectively. But the intrinsic viscosities, the MWs and DPs of the alginates after dialysis gradually decreased by following dry methods. The decreased order was ADAD, ADVF, VFAD, VFVF. The coefficient of determination between MWs and DPs in the alginates having more than 300 kDa was 0.999.

로타리 킬른형 건조로 열유동 해석에 관한 연구 (Study on CFD Analysis of Dying Plant with Rotary Kiln Type for Eco-Industrial Park)

  • 강우정;황준
    • 한국기계가공학회지
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    • 제8권4호
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    • pp.61-68
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    • 2009
  • This paper presents the numerical analysis of process of sludge drying to know the characteristics of design parameters and develop the new process plant. Finite volume method and $k-{\varepsilon}$ turbulence model were used to analogy the sludge drying furnace. It has been attempted to perform the disposal of sewage sludge such as simple reclaiming and dumping in sea and incineration. Currently, these methods are restricted by national or international government regulations. The drying process is adopted as an effective method for sewage sludge treatment. However sewage sludge makes it difficult to treat with a large volume at the real drying process plant because of its own complicated physical, chemical, and thermal properties. The final design value of moisture content with 10% of the dried sludge can be obtained through the simulated outputs in this study.

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정제 제형 제조를 위한 포공영 추출물 함유 분말의 제조 및 평가 (Fabrication and Characterization of Taraxacum platycarpum Extract-loaded Particles for Tablet Dosage Form)

  • 진성규
    • 한국분말재료학회지
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    • 제26권3호
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    • pp.225-230
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    • 2019
  • To develop Taraxacum platycarpum extract (TP)-loaded particles for tablet dosage form, various TP-loaded particles composed of TP, dextrin, microcrystalline cellulose (MCC), silicon dioxide, ethanol, and water are prepared using a spray-drying method and fluid-bed-drying method. Their physical properties are evaluated using angle of repose, Hausner ratio, Carr's index, hardness, disintegrant time, and scanning electron microscopy. Optimal TP-loaded particles improve flowability and compressibility. Furthermore, 2% silicon dioxide gives increased flowability and compressibility. The formula of TP-loaded fluid-bed-drying particles at a TP/MCC/silicon-dioxide amount of 5/5/0.2 improves the angle of repose, Hausner ratio, Carr's index, hardness, and disintegrant time as compared with the TP-loaded spray-drying particles. The TP-loaded fluid-bed-drying particles considerably improve flowability and compressibility ($35.10^{\circ}$ vs. $40.3^{\circ}$, 0.97 vs. 1.17, and 18.97% vs. 28.97% for the angle of repose, Hausner ratio, and Carr's index, respectively), hardness (11.34 vs. 4.7 KP), and disintegrant time (7.4 vs. 10.4 min) as compared with the TP-loaded spray-drying particles. Thus, the results suggest that these fluid-bed-drying particles with MCC and silicon dioxide can be used as powerful particles to improve the flowability and compressibility of the TP.

혼화재료 혼입 콘크리트 강도 차에 따른 건조수축 및 크리프 특성 평가 (Evaluation of Drying Shrinkage and Creep Characteristics by Strength Differences of Concrete Mixed with Admixture)

  • 박동천;송화철
    • 한국건축시공학회:학술대회논문집
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    • 한국건축시공학회 2021년도 봄 학술논문 발표대회
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    • pp.199-200
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    • 2021
  • In the study, creep and dry shrinkage characteristics were evaluated to determine the material properties necessary for structural analysis such as column shortening and differential drying shrinkage. All the experiments were conducted in an constant temperature and humidity room. The mechanical properties as well as the specific creep and ultimate dry shrinkage values were derived. In addition the characteristics of the physical value of the high-strength fiber reinforced concrete were considered.

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식물성 지방산 비누의 물리적 특성에 대한 건조시간과 첨가물의 효과 (Effect of Drying Time and Additives regarding the Physical Properties of Vegetable Fatty Acid Soap)

  • 이성희;이기영
    • 한국산학기술학회논문지
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    • 제15권6호
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    • pp.4032-4038
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    • 2014
  • 식물성지방산 고형비누는 검화법 제조 후 수분증발 및 경도를 위한 건조과정이 필요하며, 주로 천연성분의 첨가물을 혼합하여 제조하고 있으나 그동안의 연구는 식물성고형비누의 사용성에 관한 연구가 대부분으로 천연성분이 혼합된 식물성 지방산 고형비누의 물리적 특성과 관련된 연구는 미비한 상태이다. 이에 본 연구는 고형비누가 건조되는 기간과 첨가물(tea tree E.O, $TiO_2$)에 따른 비누의 물성 변화(pH, 표면장력, 임계미셀농도, 세정력)를 pH paper, Du Nouy 측정법, 침전법과 초음파 세척기를 이용하여 비교 관찰하고자 하였다. 식물성지방산 고형비누는 첨가물의 혼합여부와 상관없이 pH가 동일하게 나타났으며, 건조 2주~12주까지 pH8로 변화가 없었다. 또한, 표면장력과 CMC 측정결과 $TiO_2$가 첨가된 비누만 건조기간과 상관없이 62.5mg/L로 일정한 값을 보였으며, 다른 비누시료는 건조 4주째만 CMC가 25mg/L로 낮아졌다. 세정력 측정 결과 4주간 건조한 Tea tree E.O, $TiO_2$를 혼합한 식물성지방산 고형비누의 제거효율은 4.50~4.65%로 첨가물이 없는 식물성지방산 고형비누의 제거효율 3.62~3.92%보다 세정력이 높게 나타났다.