• 제목/요약/키워드: photometric method

검색결과 149건 처리시간 0.033초

가스크로마토그라피-염광광도 검출기에 의한 혈장중 카르복실기 함유 약물의 정량 (Determination of Carboxyl Drugs by Gas Chromatography-Flame Photometric Detector)

  • 박만기;조영현;유무영;강탁림
    • 약학회지
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    • 제30권4호
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    • pp.180-184
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    • 1986
  • Such carboxyl drugs as mefenamic acid, alclofenac, ketoprofen, cicloxilic acid and tolfenainic acid in rat plasma were determined by the gas chromatography flame photometric detector (GC-FPD). After methylthiomethyl (MTM) esterification with MTM-chloride in 1, 8-diazabicyclo [5.4.0] undec-7-ene (DBU) catalyst, determination of these drugs by this method was tried and compared with that by the GC-flame ionization detector (FID) method in respect to sensitivity and effect of inteferences. The results showed it was possible to analyze with accuracy by this method because of specificity of the FPD, although these drugs were not separated from interferences in plasma on GC column. The GC-FPD method was more sensitive than GC-FID method and the minimum detectable amount of monocarboxylic drugs on 3%, QF-1 column was about 15fmol/injection.

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가스크로마토그라피-염광광도검출기를 이용한 지방산의 신속간편한 정량 (A Rapid and Convenient Method for the Determination of Fatty Acid by Gas Chromatography-Flame Photometric Detector)

  • 조영현;박만기;이숙연
    • 약학회지
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    • 제29권5호
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    • pp.227-233
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    • 1985
  • A new method of determination of fatty acid using gas chromatography-flame photometric detector (GC-FPD) is described. Fatty acid was methylthiomethyl-esterified with methylthiomethy chloride in 1,8-diazabicyclo [5,4,0]-undec-7-ene catalyst and its concentration measured by GC-FPD with 3%OV-1 or 3% FS-1 column. The FPD responses of thirteen fatty acid methylthiomethyl esters were examined and were proportional to the concentration of the esters without regard to their chemical structures. Consequently it was possible to determine various fatty acid using one standard calibration curve by GC-FPD. We could rapidly and conveniently determine varous fatty acids using one standard calibration curve by GC-FPD. We could rapidly and conveniently determine 13 fatty acids in Ginseng Radix alba by this method.

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Non-Lambertian면의 형상복원 (3D Shape Reconstruction of Non-Lambertian Surface)

  • 김태은;이말례
    • 한국멀티미디어학회논문지
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    • 제1권1호
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    • pp.26-36
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    • 1998
  • 2차원 밝기 영상에서 3차원 정보를 얻는 문제는 컴퓨터 시각 연구에서 매우 중요한 분야를 차지하고 있다. 이러한 목적을 위해 먼저 2차원 영상을 취득할 때 카메라의 위치, 광원의 방향, 영상내 물체의 반사특성 등 본질적인 정보를 이용한다. 이중에서 물체의 표면 반사특성은 매우 중요한 단서가 된다. 과거에는 물체의 반사특성을 Lambertian 반사만을 전제하여 연구를 진행했지만 실세계의 물체는 대부분 Non-Lambertian 반사특성을 갖는다. 본 논문에서는 2차원 밝기 영상에서 물체의 반사특성을 해석하고, 반사특성 파라미터를 추정하여 물체의 형상을 복구하는 새로운 방법과 반사특성을 모르는 상황에서 신경회로망 학습에 의해 형상을 복구하는 방법을 제안한다. 물체의 반사특성은 전반사 성분과 난반사 성분을 함께 갖는 Non-Lambertian 면을 그 대상으로 하며, 이러한 반사특성은 전반사(Torrance-Sparrow) 모델과 난반사(Lambertian) 모델의 선형적인 합으로 설명될 수 있다. 본 논문에서 제안한 Photometric Matching은 주변 화소의 밝기 분포를 고려하여 참조영상과의 매칭을 통한 형상복구 알고리듬으로써 기존의 Photometric Stereo에 근본을 두고 있지만, 잡음 및 오차의 누적 정도가 향상되었다. 또한 물체의 반사특성을 모르는 상황에서 신경회로망 학습에 의한 형상복구방법을 제안한다. 이 방법은 역전파 학습알고리듬을 이용해 광원 방향에 따른 밝기값에 대해 면법선을 교사하여 형상을 결정한다.

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스티칭 영상의 객관적 영상화질의 평가 방법 (Objective Quality Assessment for Stitched Image and Video)

  • 미어 사데크 빌라흐;타이 탄 투안;안희준
    • 한국방송∙미디어공학회:학술대회논문집
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    • 한국방송∙미디어공학회 2017년도 추계학술대회
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    • pp.218-220
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    • 2017
  • Recently, stitching techniques are used for obtaining wide FOV, e.g., panorama contents, from normal cameras. Despite many proposed algorithms, the no objective quality evaluation method is developed, so the comparison of algorithms are performed only in subjective way. The paper proposes a 'Delaunay-triangulation based objective assessment method' for evaluating the geometric and photometric distortions of stitched or warped images. The reference and target images are segmented by Delaunay-triangulation based on matched points between two images, the average Euclidian distance is used for geometric distortion measure, and the average or histogram of PSNR for photometric measure. We shows preliminary results with several test images and stitching methods for demonstrate the benefits and application.

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비냉각형 선농축 방식에 의한 대기 중 휘발성 황화합물의 분석방법 개발 (Development of an Analytical Approach to Measure Volatile Sulfur Compounds Using a Non-Cryogenic Preconcentration Method)

  • 김기현;이강웅
    • 한국대기환경학회지
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    • 제13권5호
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    • pp.355-360
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    • 1997
  • The atmospheric concentration of dimethylsulfide (DMS), known as the predominant volatile organic. sulfur compound, is determined at subnanogram level by a combined application of non-cryogenic preconcentration method and gas chromatography with flame photometric detection (GC/FPD). The volatile DMS in air is preconcentrated using a trapping tube containing adsorbent like Molecular Sieve 5A (or gold-coated sands). The tube is then connected to the GC/FPD system via a six-way rotary valve, thermally desorbed at 40$0^{\circ}C$, separated on OV101 column, and detected by a flame photometric detector. The DMS peak elutes at about 2.5 mins and is integrated electronically. The analytical precision, if expressed in terms of relative standard error, is around 5%. The detection limit of our GC/FPD system is ca 1 ng of DMS. Details of our analytical system are presented.

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물체의 면 반사특성 추정과 측광정합을 이용한 3차원 형상복구 (Estimation of surface reflectance properties and 3D shape recovery using photometric matching)

  • 김태은;류석현;송호근;최종수
    • 한국통신학회논문지
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    • 제21권7호
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    • pp.1633-1641
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    • 1996
  • In this paper we propose a new method for anlayzing the properties of surface reflectance and reconstructing the shape of object using estimated reflectance parameters. We have investigated the hybrid reflectance surface which has specularreflection and diffuse reflection, which can be explained by Torrance-Sparrow model. Sample sphere made on one maerial is used to estimate the reflectance properties by using LMS algorithm. We can make the reference image which consists of surface normal and brightness value using estimated reflectance parameters, and thenarbitrary shape object made of the same material as sample can be reconstructed by matching with reference image. Photometric matching method proposed in this paper is robust because it mateches object image with the reference imageconsidering its neighbor brightness distribution. Also, in this paper plate diffuse illumination is used to remove intensity disparity with simple scheme. It is expected that the proposed algorithm can be applied to 3D recognition, vision inspection system and other fields.

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배광데이터를 이용한 3차원 평면프리즘의 설계 알고리즘 개발 (Development of 3 Dimensional Planar Prism Design Algorithm Using Photometric Data)

  • 김유신;최안섭
    • 한국조명전기설비학회:학술대회논문집
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    • 한국조명전기설비학회 2006년도 춘계학술대회 논문집
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    • pp.3-7
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    • 2006
  • Development of light sources has been constantly grown for a high efficacy and long life. And, the design of luminaires has ben developed for the reflection and refraction of light mechanism. But it has been not enough to study for the refraction of light mechanism. Therefore, this study aims to study for the refraction of light mechanism to using Monte-Carlo method and Ray-tracing method. In addition, the purpose of this study is to shu calculation process for development of 3 dimensional planar prism design algorithm in orer to use the results of photometric data that is able to obtain various luminous intensity distribution.

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Detection of Variable Stars in the Open Cluster M11 Using Difference Image Analysis Pipeline

  • Lee, Chung-Uk;Koo, Jae-Rim;Kim, Seung-Lee;Lee, Jae-Woo;Park, Byeong-Gon;Han, Cheong-Ho
    • Journal of Astronomy and Space Sciences
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    • 제27권4호
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    • pp.289-307
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    • 2010
  • We developed a photometric pipeline to be used for a wide field survey. This pipeline employs the difference image analysis (DIA) method appropriate for the photometry of star dense field such as the Galactic bulge. To verify the performance of pipeline, the observed dataset of the open cluster M11 was re-processed. One hundred seventy eight variable stars were newly discovered by analyzing the light curves of which photometric accuracy was improved through the DIA. The total number of variable stars in the M11 observation region is 335, including 157 variable stars discovered by previous studies. We present the catalogue and light curves for the 178 variable stars. This study shows that the photometric pipeline using the DIA is very useful in the detection of variable stars in a cluster.

PULSATIONAL CHARACTERISTICS OF V1719 CYGNI WITH PECULIAR LIGHT CURVE

  • KIM CHULHEE;KIM SEUNG-LI;SADAKANE KOZO
    • 천문학회지
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    • 제26권2호
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    • pp.115-134
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    • 1993
  • The light curve and radial velocity curve of multiperiodic dwarf cepheid VI719 Cyg (HD200925) with peculiar light curve have been reanalyzed in order to identify the oscillation modes to confirm the helium settling within the envelope. To do these, through the period search for the photometric and radial velocity data from the literature, two different periods were determined and the oscillation modes corresponding to the first and second periods were identified as the fundamental and first radial overtones. Hence the helium settling within the envelope was confirmed from the period ratio. The color excess, metallicity, effective temperature, and surface gravity corresponding to two different modes were determined and it was found that these parameters almost do not depend upon different oscillation mode. By utilizing the surface brightness method, we investigated the variation of angular diameter and radial displacement and it was found that the angular variation is very peculiar. Also by referring to the stellar models, mass and age were determined as $2.7M_{\bigodot}$ and 0.42 Gyr respectively which make this variable star heavier and younger than other multimode dwarf cepheids. Preliminary spectroscopic CCD observations were carried out and it was found that Mg in VI719 Cygni is nearly solar abundent according to the analysis of $5172.68{\AA}MgI$ line which is inconsistent with the photometric result. It was suggested that VI719 Cyg may be classified as a $\rho$ Pup stars according to the photometric characteristics.

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근접쌍성 RZ Cas의 측광학적 연구 (A PHOTOMETRIC STUDY FOR A CLOSE BINARY RZ Cas)

  • 이용삼;권수진;정장해
    • Journal of Astronomy and Space Sciences
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    • 제14권2호
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    • pp.233-241
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    • 1997
  • 충북대학교 천문대에서 1991년 10월부터 1993년 3월까지 총 42일간 근접쌍성 RZ Cas의 광전 측광 관측을 수행하여 UBV 광도곡선을 완성하였다. 제 1식심 의 광도곡선으로부터 8개의 제 1식심 시각 및 새로운 광도요소를 결정하였다. 우리의 광도곡선에서 제 1식심이 개기 식임을 확인하였고, 개기 식 지속시간이 평균 18.1분으로서 이 값은 약 $0.^{p}01$에 해당하는 값임을 알았다. Wilson Devinney 분석법을 사용하여 우리의 광도곡선과 Duerbeck & Hanel(1979)의 시선속도 곡선을 동시에 만족하는 RZ Cas 의 측광 및 분광학적 해를 구하고 이 값으로부터 이 쌍성 계의 절대량을 산출하였다.

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