• Title/Summary/Keyword: photometric method

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Determination of Carboxyl Drugs by Gas Chromatography-Flame Photometric Detector (가스크로마토그라피-염광광도 검출기에 의한 혈장중 카르복실기 함유 약물의 정량)

  • 박만기;조영현;유무영;강탁림
    • YAKHAK HOEJI
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    • v.30 no.4
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    • pp.180-184
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    • 1986
  • Such carboxyl drugs as mefenamic acid, alclofenac, ketoprofen, cicloxilic acid and tolfenainic acid in rat plasma were determined by the gas chromatography flame photometric detector (GC-FPD). After methylthiomethyl (MTM) esterification with MTM-chloride in 1, 8-diazabicyclo [5.4.0] undec-7-ene (DBU) catalyst, determination of these drugs by this method was tried and compared with that by the GC-flame ionization detector (FID) method in respect to sensitivity and effect of inteferences. The results showed it was possible to analyze with accuracy by this method because of specificity of the FPD, although these drugs were not separated from interferences in plasma on GC column. The GC-FPD method was more sensitive than GC-FID method and the minimum detectable amount of monocarboxylic drugs on 3%, QF-1 column was about 15fmol/injection.

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A Rapid and Convenient Method for the Determination of Fatty Acid by Gas Chromatography-Flame Photometric Detector (가스크로마토그라피-염광광도검출기를 이용한 지방산의 신속간편한 정량)

  • 조영현;박만기;이숙연
    • YAKHAK HOEJI
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    • v.29 no.5
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    • pp.227-233
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    • 1985
  • A new method of determination of fatty acid using gas chromatography-flame photometric detector (GC-FPD) is described. Fatty acid was methylthiomethyl-esterified with methylthiomethy chloride in 1,8-diazabicyclo [5,4,0]-undec-7-ene catalyst and its concentration measured by GC-FPD with 3%OV-1 or 3% FS-1 column. The FPD responses of thirteen fatty acid methylthiomethyl esters were examined and were proportional to the concentration of the esters without regard to their chemical structures. Consequently it was possible to determine various fatty acid using one standard calibration curve by GC-FPD. We could rapidly and conveniently determine varous fatty acids using one standard calibration curve by GC-FPD. We could rapidly and conveniently determine 13 fatty acids in Ginseng Radix alba by this method.

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3D Shape Reconstruction of Non-Lambertian Surface (Non-Lambertian면의 형상복원)

  • 김태은;이말례
    • Journal of Korea Multimedia Society
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    • v.1 no.1
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    • pp.26-36
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    • 1998
  • It is very important study field in computer vision 'How we obtain 3D information from 2D image'. For this purpose, we must know position of camera, direction of light source, and surface reflectance property before we take the image, which are intrinsic information of the object in the scene. Among them, surface reflectance property presents very important clues. Most previous researches assume that objects have only Lambertian reflectance, but many real world objects have Non-Lambertian reflectance property. In this paper the new method for analyzing the properties of surface reflectance and reconstructing the shape of object through estimation of reflectance parameters is proposed. We have interest in Non-Lambertian reflectance surface that has specular reflection and diffuse reflection which can be explained by Torrance-Sparrow model. Photometric matching method proposed in this paper is robust method because it match reference image and object image considering the neighbor brightness distribution. Also in this thesis, the neural network based shaped reconstruction method is proposed, which can be performed in the absence of reflectance information. When brightness obtained by each light is inputted, neural network is trained by surface normal and can determine the surface shape of object.

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Objective Quality Assessment for Stitched Image and Video (스티칭 영상의 객관적 영상화질의 평가 방법)

  • Billah, Meer Sadeq;Tuan, Thai Thanh;Ahn, Heejune
    • Proceedings of the Korean Society of Broadcast Engineers Conference
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    • 2017.11a
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    • pp.218-220
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    • 2017
  • Recently, stitching techniques are used for obtaining wide FOV, e.g., panorama contents, from normal cameras. Despite many proposed algorithms, the no objective quality evaluation method is developed, so the comparison of algorithms are performed only in subjective way. The paper proposes a 'Delaunay-triangulation based objective assessment method' for evaluating the geometric and photometric distortions of stitched or warped images. The reference and target images are segmented by Delaunay-triangulation based on matched points between two images, the average Euclidian distance is used for geometric distortion measure, and the average or histogram of PSNR for photometric measure. We shows preliminary results with several test images and stitching methods for demonstrate the benefits and application.

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Development of an Analytical Approach to Measure Volatile Sulfur Compounds Using a Non-Cryogenic Preconcentration Method (비냉각형 선농축 방식에 의한 대기 중 휘발성 황화합물의 분석방법 개발)

  • 김기현;이강웅
    • Journal of Korean Society for Atmospheric Environment
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    • v.13 no.5
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    • pp.355-360
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    • 1997
  • The atmospheric concentration of dimethylsulfide (DMS), known as the predominant volatile organic. sulfur compound, is determined at subnanogram level by a combined application of non-cryogenic preconcentration method and gas chromatography with flame photometric detection (GC/FPD). The volatile DMS in air is preconcentrated using a trapping tube containing adsorbent like Molecular Sieve 5A (or gold-coated sands). The tube is then connected to the GC/FPD system via a six-way rotary valve, thermally desorbed at 40$0^{\circ}C$, separated on OV101 column, and detected by a flame photometric detector. The DMS peak elutes at about 2.5 mins and is integrated electronically. The analytical precision, if expressed in terms of relative standard error, is around 5%. The detection limit of our GC/FPD system is ca 1 ng of DMS. Details of our analytical system are presented.

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Estimation of surface reflectance properties and 3D shape recovery using photometric matching (물체의 면 반사특성 추정과 측광정합을 이용한 3차원 형상복구)

  • 김태은;류석현;송호근;최종수
    • The Journal of Korean Institute of Communications and Information Sciences
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    • v.21 no.7
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    • pp.1633-1641
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    • 1996
  • In this paper we propose a new method for anlayzing the properties of surface reflectance and reconstructing the shape of object using estimated reflectance parameters. We have investigated the hybrid reflectance surface which has specularreflection and diffuse reflection, which can be explained by Torrance-Sparrow model. Sample sphere made on one maerial is used to estimate the reflectance properties by using LMS algorithm. We can make the reference image which consists of surface normal and brightness value using estimated reflectance parameters, and thenarbitrary shape object made of the same material as sample can be reconstructed by matching with reference image. Photometric matching method proposed in this paper is robust because it mateches object image with the reference imageconsidering its neighbor brightness distribution. Also, in this paper plate diffuse illumination is used to remove intensity disparity with simple scheme. It is expected that the proposed algorithm can be applied to 3D recognition, vision inspection system and other fields.

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Development of 3 Dimensional Planar Prism Design Algorithm Using Photometric Data (배광데이터를 이용한 3차원 평면프리즘의 설계 알고리즘 개발)

  • Kim, Yu-Sin;Choi, An-Seop
    • Proceedings of the Korean Institute of IIIuminating and Electrical Installation Engineers Conference
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    • 2006.05a
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    • pp.3-7
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    • 2006
  • Development of light sources has been constantly grown for a high efficacy and long life. And, the design of luminaires has ben developed for the reflection and refraction of light mechanism. But it has been not enough to study for the refraction of light mechanism. Therefore, this study aims to study for the refraction of light mechanism to using Monte-Carlo method and Ray-tracing method. In addition, the purpose of this study is to shu calculation process for development of 3 dimensional planar prism design algorithm in orer to use the results of photometric data that is able to obtain various luminous intensity distribution.

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Detection of Variable Stars in the Open Cluster M11 Using Difference Image Analysis Pipeline

  • Lee, Chung-Uk;Koo, Jae-Rim;Kim, Seung-Lee;Lee, Jae-Woo;Park, Byeong-Gon;Han, Cheong-Ho
    • Journal of Astronomy and Space Sciences
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    • v.27 no.4
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    • pp.289-307
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    • 2010
  • We developed a photometric pipeline to be used for a wide field survey. This pipeline employs the difference image analysis (DIA) method appropriate for the photometry of star dense field such as the Galactic bulge. To verify the performance of pipeline, the observed dataset of the open cluster M11 was re-processed. One hundred seventy eight variable stars were newly discovered by analyzing the light curves of which photometric accuracy was improved through the DIA. The total number of variable stars in the M11 observation region is 335, including 157 variable stars discovered by previous studies. We present the catalogue and light curves for the 178 variable stars. This study shows that the photometric pipeline using the DIA is very useful in the detection of variable stars in a cluster.

PULSATIONAL CHARACTERISTICS OF V1719 CYGNI WITH PECULIAR LIGHT CURVE

  • KIM CHULHEE;KIM SEUNG-LI;SADAKANE KOZO
    • Journal of The Korean Astronomical Society
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    • v.26 no.2
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    • pp.115-134
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    • 1993
  • The light curve and radial velocity curve of multiperiodic dwarf cepheid VI719 Cyg (HD200925) with peculiar light curve have been reanalyzed in order to identify the oscillation modes to confirm the helium settling within the envelope. To do these, through the period search for the photometric and radial velocity data from the literature, two different periods were determined and the oscillation modes corresponding to the first and second periods were identified as the fundamental and first radial overtones. Hence the helium settling within the envelope was confirmed from the period ratio. The color excess, metallicity, effective temperature, and surface gravity corresponding to two different modes were determined and it was found that these parameters almost do not depend upon different oscillation mode. By utilizing the surface brightness method, we investigated the variation of angular diameter and radial displacement and it was found that the angular variation is very peculiar. Also by referring to the stellar models, mass and age were determined as $2.7M_{\bigodot}$ and 0.42 Gyr respectively which make this variable star heavier and younger than other multimode dwarf cepheids. Preliminary spectroscopic CCD observations were carried out and it was found that Mg in VI719 Cygni is nearly solar abundent according to the analysis of $5172.68{\AA}MgI$ line which is inconsistent with the photometric result. It was suggested that VI719 Cyg may be classified as a $\rho$ Pup stars according to the photometric characteristics.

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A PHOTOMETRIC STUDY FOR A CLOSE BINARY RZ Cas (근접쌍성 RZ Cas의 측광학적 연구)

  • 이용삼;권수진;정장해
    • Journal of Astronomy and Space Sciences
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    • v.14 no.2
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    • pp.233-241
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    • 1997
  • New UBV Photometric observations for a close binary RZ Cas were obtained at the Chungbuk National University Observatory for 42 nights from October 1991 to March 1993, and standardized UBV light curves were constructed. From the primary light curves, the eight minimum times were determined by using a new light element. We confirmed the primary minimum was totality and derived the average duration was 18.1 minutes corresponding to $0.^{p}01$. The photometric and spectroscopic solutions were calculated with the obtained light curves and the radial velocity curves of Duerbeck & Hanel(1979) by using Wilson-Devinney method. From these values, the absolute dimensions of this binary system were estimated.

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