• Title/Summary/Keyword: phase evolution

검색결과 651건 처리시간 0.025초

액상량이 탄화규소 소결체의 미세구조 및 상변태에 미치는 영향 (Influence of Liquid-Phase Amount on the Microstructure and Phase Transformation of Liquid-phase Sintered Silicon Carbide)

  • 이종국;강현희;박종곤;이은구
    • 한국세라믹학회지
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    • 제35권4호
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    • pp.413-419
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    • 1998
  • ${\beta}$-silicon carbides with yttrium aluminum garnet of 2,5,10 mol% were prepared by a liquid--phase sint-ering and the microstructural evolution and phase transformation were investigated during sintering as functions of liquid-phase amount and sintering time. The rate of grain growth decreases with the addition of the amount of yttrium aluminum garnet (YAG) in the SiC starting powder however the apparent density and the aspect ratio of grains in sintered body increase. The phase transformation from ${\beta}$-SiC to ${\alpha}$-SiC were dependent on the liquid-phase amount and sintering time.

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TMA Study on Phase Evolution During Hydrogen-assisted Disproportionation of Nd-Fe-B Alloy

  • Kwon, H.W.;Yu, J.H.
    • Journal of Magnetics
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    • 제16권3호
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    • pp.229-233
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    • 2011
  • Phase evolution during the hydrogen-assisted disproportionation of $Nd_{12.5}Fe_{80.6}B_{6.4}Ga_{0.3}Nb_{0.2}$ alloy was investigated mainly by using a magnetic balance-type thermomagnetic analyser (TMA). In order to avoid any undesirable phase change in the course of heating for TMA, a swift TMA technique with very high heating rate (around 2 min to reach $800^{\circ}C$ from room temperature) was adopted. The hydrided $Nd_{12.5}Fe_{80.6}B_{6.4}Ga_{0.3}Nb_{0.2}$ alloy started to be disproportionated in hydrogen from around $600^{\circ}C$, and the alloy after the early disproportionation (from 600 to $660^{\circ}C$) has been partially disproportionated. The partially disproportionated alloy consisted of a mixture of $NdH_x$, $Fe_3B$, ${\alpha}$-Fe, and the remaining undisproportionated $Nd_2Fe_{14}BH_x$-phase. During the subsequent heating to $800^{\circ}C$ in hydrogen, two additional phases of $Fe_{23}B_6$ and $Fe_2B$ were formed, and the material consisted of a mixture of $NdH_x$, $Fe_{23}B_6$, $Fe_3B$, $Fe_2B$, and ${\alpha}$-Fe phases. During the subsequent isothermal holding at $800^{\circ}C$ for 1 hour, the phase constitution was further changed, and one additional unknown magnetic phase was formed. Eventually, the fully disproportionated $Nd_{12.5}Fe_{80.6}B_{6.4}Ga_{0.3}Nb_{0.2}$ alloy consisted of $NdH_x$, $Fe_{23}B_6$, $Fe_3B$, $Fe_2B$, ${\alpha}$-Fe, and one additional unknown magnetic phase.

$\alpha$'-Sialon 세라믹스에서의 주상형 입자성장 (Growth of Elongated Grains in $\alpha$'-Sialon Ceramics)

  • 신익현
    • 한국분말재료학회지
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    • 제6권3호
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    • pp.246-250
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    • 1999
  • The effects of the ${\beta}-Si_3N_4$ starting particle size and $\alpha$/$\beta$ phase transformation during sintering process on the microstructure evolution of Yttrium $\alpha$-Sialon ceramics were investigated. As-received ${\beta}-Si_3N_4$ powder (mean particle size: 0.54$\mu$m) and classified ${\beta}-Si_3N_4$ powder(mean particle size: $0.26\mu{m}$) were used as starting powders. With decreasing the starting particle size, the growth of elongated grains was enhanced, which resulted in the whisker -like microstructure with elongated grains. These results were discussed in relation to the two-dimensional nucleation and growth theory. In the specimen heat treated at $1600^{\circ}C$ for 10h before sintering at $1950^{\circ}C$for 1h under 40atm(2-step sintering), the grain size was smaller than of the 1-step sintering at 195$0^{\circ}C$ for 1h. However, bimodal microstructure evolution were not not remarkable in both sample, which is ascribed to the $\alpha$-phase contents existing in ${\beta}-Si_3N_4$ starting powder.

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적응진화연산을 이용한 퍼지-전력계통안정화장치 설계 (A Design of Fuzzy Power System Stabilizer using Adaptive Evolutionary Computation)

  • 황기현;박준호
    • 대한전기학회논문지:전력기술부문A
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    • 제48권6호
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    • pp.704-711
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    • 1999
  • This paper presents a design of fuzzy power system stabilizer (FPSS) using adaptive evolutionary computation (AEC). We have proposed an adaptive evolutionary algorithm which uses a genetic algorithm (GA) and an evolution strategy (ES) in an adaptive manner in order to take merits of two different evolutionary computations. FPSS shows better control performances than conventional power system stabilizer (CPSS) in three-phase fault with heavy load which is used when tuning FPSS. To show the robustness of the proposed FPSS, it is appliedto damp the low frequency oscillations caused by disturbances such as three-phase fault with normal and light load, the angle deviation of generator with normal and light load and the angle deviation of generator with heavy load. Proposed FPSS shows better robustness than CPSS.

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TWO-FLUID CLOSURE PARAMETERS FOR DIFFUSIVE ACCELERATION OF COSMIC RAYS

  • KANG HYESUNG
    • 천문학회지
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    • 제26권1호
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    • pp.1-12
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    • 1993
  • In order to explore the time dependence of the closure parameters of the two-fluid calculations for supernova remnants and the terminal shocks of stellar winds, we have considered a simple model in which the time evolution of the cosmic-ray distribution function was followed in the test-particle limit using the Bohm diffusion model. The particles are mostly accelerated to relativistic energy either in the free expansion phase of the SNRs or in the early phase of the stellar winds, so the evolution of the closure parameters during these early stages is substantial and should be followed correctly. We have also calculated the maximum momentum which is limited by either the age or the curvature of these spherical shocks. We found that SNRs expanding into the medium where the gas density decreases with the distance from the explosion center might be necessary to explain the observed power-law distribution of the galactic cosmic rays. The energy loss due to the escaping energetic particles has been estimated for the terminal shocks of the stellar winds.

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TIME-DEPENDENT INITIAL MASS FUNCTION AND PRESENT DAY MASS FUNCTION OF OPEN CLUSTERS

  • Lee, See-Woo;Kim, Yong-Ha
    • 천문학회지
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    • 제16권2호
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    • pp.43-54
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    • 1983
  • The present day mass functions of main sequence stars in the well observed open clusters, Hyades, Praesepe, Pleiades, NGC 654 and NGC 6530 arc derived and compared with those computed from the model of time-dependent initial mass function and star formation rate. The agreements between the observed and computed present day mass functions suggest the importance of fragmentation process at the early phase and fragment interaction at the later phase of cluster evolution. This process of star formation is different from that related to the evolution of the solar neighborhood, and also could explain the lack of low mass stars observed in some open clusters.

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Elaboration of (Steel/Cemented Carbide) Multimaterial by Powder Metallurgy

  • Pascal, Celine;Chaix, Jean-Marc;Dutt, Ankur;Lay, Sabine;Allibert, Colette H.
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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    • pp.291-292
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    • 2006
  • A steel/cemented carbide couple is selected to generate a tough/hard two layers material. Sintering temperature and composition are deduced from phase equilibria, and experimental studies are used to determine optimal conditions. Liquid migration from the hard layer to the tough one is observed. Microstructure evolution during sintering of the tough material (TEM, SEM, image analysis) evidences coupled mechanisms of pore reduction and WC dissolution. Liquid migration, as well as interface crack formation due to differential densification are limited by suitable temperature and time conditions.

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