• 제목/요약/키워드: perpendicular to the grain

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$CoCr_{16.2}Pt_{10.8}Ta_4$ 합금박막의 Ti 우선증착에 따른 자기적 특성과 자구형상변화 (Magnetic properties and the shapes of magnetic domain for $CoCr_{16.2}Pt_{10.8}Ta_4$ alloy films with the prior deposition of Ti layer)

  • 이인선;김동원
    • 한국결정성장학회지
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    • 제10권1호
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    • pp.17-22
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    • 2000
  • 수직보자력이 크고 CoCrPt에 비하여 noise 저감 효과가 큰 것으로 알려진 CoCrPtTa계 합금박막의 수직이방성을 더욱 개선하기 위해 Ti를 우선 증착하였다. 본 연구에서는 Ti 두께 변화에 따른 비교적 높은 수직보자력치를 보였던 $CoCr_{16.2}Pt_{10.8}Ta_4$Ti/glass 시편에서 자기적 특성과 자구형상의 변화를 살펴보았다. 또한 VSM(Vibrating Sample Magnetometer)을 이용하여 M-H loop를 측정하였으며 자구형상은 MFM(Magnetic Force Microscopy)로 관찰하였다. 육방정 Ti가 하지층으로서 우선증착되면 bare glass 직접 증착되는 경우보다 CoCrPtTa 자성층의 수직이방성에 현저한 향상을 가져왔으며 Ti의 두께가 두꺼울수록 c-축 배향성도 개선되었다. MFM 결과에 의하면 Ti두레가 20 nm에서 90 nm로 증가함에 따라 자구형상이 연속적인 stripe type에서 mass type으로 분절된 형태로 변하였다. 이는 Ti의 증착이 비자성 Cr 편석 거동에 영향을 미쳐 자화반전시 인접 columnar grain의 자화벡터들간의 상호교환작용을 억제하는 자기적 분리 효과에 기여했음을 의미한다. 아울러 이와 같은 거동은 Ti가 CoCr계 자성층의 수직이방성을 개선하는데 있어서 형상자기이방성적인 측면에서의 기여가 현저함을 의미하기도 한다.

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Co-Cr(-Ta)/Si 이층막의 자기적 특성 (Magnetic Properties of Co-Cr(-Ta)/Si Bilayered Thin Film)

  • 김용진;박원효;금민종;최형욱;김경환;손인환
    • 한국전기전자재료학회논문지
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    • 제15권3호
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    • pp.281-286
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    • 2002
  • In odder to investigate the magnetic properties of CoCr-based bilayered thin films on kind of underlayer, we introduced amorphous Si layer to Co-Cr(-Ta) magnetic layer as underlayer. First, we prepared CoCr and CoCrTa single layer using the Facing Targets Sputtering system to investigate theirs properties. It was revealed that with increasing the film thickness of CoCr, CoCrTa single layer, crystalline orientation and perpendicular coercivity was improved. The CoCrTa thin film showed bettor crystalline and magnetic characteristics than CoCr thin film. As a result of investigating magnetic properties of CoCr and CoCrTa magnetic layer on introducing the Si underlayer, perpendicular coercivity and saturation magnetization of CoCr/Si and CoCrTa/Si bilayered thin film were decreased due to the increased grain size and diffusion of Si atoms to magnetic layer. And they showed constant with increasing the film thickness of Si thin film. However, in case of CoCrTa/Si bilayered thin film, in-plane coercivity was controlled low at about 250Oe. The c-axis orientations of CoCr/si and CoCrTa/Si bilayered thin film showed a good crystalline characteristics as about $2^{\circ}$.

분극방향에 따른 PZT 세라믹스의 압전특성 및 압축파괴강도의 변화 (Variations of Piezoelectric Properties and Compressive Strength of PZT Ceramics with Poling Directions)

  • 임진호;손준호;김정주;박병옥;조상희
    • 한국세라믹학회지
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    • 제32권10호
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    • pp.1131-1138
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    • 1995
  • Variations of piezoelectric properties and compressive strength of Sr-doped PZT ceramics were investigated with poling direction. The electro-mechanical coupling constants (k31 and k33) were increased linearly with increasing poling strength. The volume fraction of intergranular fracture also increased with incresing poling strength due to weakening of grain boundaries by domain rearrangement during poling process. The internal stresses induced from the poling at 2.5 kV/mm parallel and perpendicular to the poling direction poled were 405 MPa and 89 MPa, respectively. The compressive strength of the specimen poled parallel to the poling direction was higher than that perpendicular to the poling direction.

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LSI 공법으로 제작된 C/SiC 복합재의 압축거동 평가 (Compressive Fracture Behavior of C/SiC composite fabricated by Liquid Silicon Infiltration)

  • 윤동현;김재훈
    • 한국안전학회지
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    • 제33권1호
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    • pp.1-6
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    • 2018
  • The effects of the fiber direction, specimen size and temperature on the compressive strength of carbon fiber reinforced silicon carbide composite (C/SiC composite) manufactured by liquid silicon infiltration(LSI) is investigated. Tests were conducted in accordance with ASTM C 695 at room temperature and elevated temperatures. Experiments are conducted with two different specimens considering grain direction. With grain (W/G) specimens have a carbon fibers parallel to the load direction, but across grain (A/G) specimens have a perpendicular carbon fibers. To verify the specimen size effect of C/SiC composite, two types of specimens are manufactured. One has a one to two ratio of diameter to height and the other has a one to one ratio. The compressive strength of C/SiC composite increased as temperature rise. As specimens are larger, compressive strength of A/G specimens increased, however compressive strength of W/G decreased.

PZT의 파괴거동 및 압전 열화특성 (Fracture Behavior and Degradation of Piezoelectric Properties in PZT)

  • 태원필;김송희;조상희
    • 한국세라믹학회지
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    • 제29권10호
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    • pp.806-814
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    • 1992
  • The aim of this study was to investigate the change in compressive strength, freacture behavior and degradation of piezoelectric properties with compressive cyclic loading in Pb(Zr, Ti)O3 of tetragonal, morphotropic phase boundary and rhombohedral composition. The highest compressive strength was found in rhombohedral composition. After poling treatment the strength increased by 8.4% and 6.5% in tetragonal and morphotropic phase boundary compositions respectively while changed little in rhombohedral. The increase of compressive strength after poling treatment is believed to be due to the internal stress around grain boundary by domain alginment toward electric field direction in the microstructures having tetragonality and the occurrence of domain switching to the direction perpendicular to electrical field during fracture. Fracture mode relatively change from transgranular to intergranular was observed in the large grain sized tetragonal and morphotropic phase boundary compositions before and after poling but the transgranular fracture mode always remained in the rhombohedral composition. From the X-ray diffractometer analysis the domains parallel to the electric field direction is known to undergo rearrangement during the cyclic loading into random direction that is responsible for the degradation of piezoelectric property.

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고온초전도체 $Y_1Ba_2Cu_3O_{7-y}$의 자기이방성 (Magnetic Anisotropy in High $T_c\;Y_1Ba_2Cu_3O_{7-y}$ Superconductor)

  • 김문석;유성초;임우영;백종성
    • 한국자기학회지
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    • 제2권3호
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    • pp.228-232
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    • 1992
  • 고온초전도체 $Y_1Ba_2Cu_3O_{7-y}$의 grain을 높은 자기장에서 정렬시켜 여러가지 자기적 특성을 조사하였다. Grain이 정렬된 초전도체는 단결정과 같이 Cu-O layer에 수직, 수평 방향에 대해 자기이방성을 가진다. 2~77 K의 온도영역에서 측정한 lower critical field$(H_{c1})$은 온도가 증가하면서 선형적으로 감소하였는데, Cu-O layer에 대하여 외부 자기장이 수직인 경우가 더욱 급격히 감소하였다. 온도변화에 따른 자율화$(4{\pi}\;X)$의 측정으로부터 극저온의 자화율이 -1에 가까운 값을 가진다는 것을 알 수 있었다. 또한 이 자화 곡선을 London의 공식과 two-fluid model을 이용해 최소자승법으로 fitting하여 절대 영도에서 침투깊이$({\lambda}_0)$를 구하였다. 또한 2 K에서 외부 자기장에 따른 자화곡선을 측정하였으며, Bean의 critical state model을 이용한 임계전류밀도$(J_c)$의 계산으로부터 grain내부는 단결정 수준의 높은 $(J_c)$를 가지고 있음을 알 수 있었다.

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압연강판(壓延鋼板)의 피로균열(被虜龜裂) 전파거동(傳播擧動)에 대(對)한 연구(硏究) (A Study on the Propagation Behaviour of the Fatigue Cracks in Rolled Steel Plates)

  • 강창수
    • 대한조선학회지
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    • 제12권2호
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    • pp.43-58
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    • 1975
  • There are many reports on fatigue crack of metallic materials but most of them relate crack propagation rate to stress intensity factor. The problem of crack propagation is not yet clarified, especially the bridge between micro and macro phenomena In this experiment rotating bending fatigue tests have been carried out with smoothed specimen of rolled steel plates including 0.2% carbon under application of three stress conditions to investigate the slip band and the crack propagation behaviour. The results obtained are as follows; 1) The length of cracks which have grown at initial crack tips can be expressed as follows; $l=Ae^{BNr}$(A,B: constant, $N_r$: cycle ratio) $\frac{dl}{dN}=\frac{AB}{N_f}{\cdot}e^{BNr}$($N_f$:fatigue life) 2) The ratio of slipped grain number to total grain number is $S_f=7{\sigma}-5.6$-5.6{\sigma}_c$($\sigma$: stress amplitude) (${\sigma}_c$: fatigue limit) 3) When the fatigue process transfers from Stage I to Stage II, the crack which propagates into specimen changes its direction from that of the maximum shear stress to the direction of perpendicular to principal stress and this is same in the circumferential direction of specimen. the crack propagation behaviors of both sides of a crack are different each other when they approach to the grain boundary.

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Microstructural improvement in polycrystalline Si films by crystallizing with vapor transport of Al/Ni chlorides

  • Eom, Ji-Hye;Lee, Kye-Ung;Jun, Young-Kwon;Ahn, Byung-Tae
    • 한국정보디스플레이학회:학술대회논문집
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    • 한국정보디스플레이학회 2004년도 Asia Display / IMID 04
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    • pp.315-318
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    • 2004
  • We developed a vapor induced crystallization (VIC) process for the first time to obtain high quality polycrystalline Si films by sublimating the mixture of $AlCl_3$ and $NiCl_2$. The VIC process enhanced the crystallization of amorphous silicon thin films. The LPCVD amorphous silicon thin films were completely crystallized after 5 hours at 480 $^{\circ}C$. It is known that needle-like grains with very small width grow in the Ni-metal induced lateral crystallization. In our new method, the width of grains is larger because the grain can also grow perpendicular to the needle growth direction. Also the interface between the merging grain boundaries was coherent. As the results, a polycrystalline film with superior microstructure has been obtained.

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포천지역의 쥬라기 화강암에 발달된 결의 특성 (Characteristics of the Rock Cleavage in Jurassic Granite, Pocheon)

  • 박덕원;김형찬;이창범;장세원;이철우
    • 암석학회지
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    • 제13권3호
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    • pp.133-141
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    • 2004
  • 포천지역의 쥬라기 화강암내 결의 특성을 규명하였다 3가지 미세균열의 분포상은 박편의 확대사진(x6.7)에서 잘 나타난다. 우세균열 면은 1번 결의 면에 평행하며, 준 우세균열 면은 2번 결의 면에 평행하다. 이러한 1번 결 및 2번 결을 형성하는 미세균열은 3번 결의 면상에서 상호 거의 수직을 이룬다. 따라서, 연구지역의 화강암질암의 결은 미세균열의 선택적 배향성에 지배된다고 할 수가 있다. 결은 리프트, 그레인, 하드웨어 면의 순으로 발생빈도, 길이 및 밀도가 발달하고 있다.

Evaluation of Bearing Strength of Self-Tapping Screws according to the Grain Direction of Domestic Pinus densiflora

  • LEE, In-Hwan;KIM, Keonho;SHIM, Kug-bo
    • Journal of the Korean Wood Science and Technology
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    • 제50권1호
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    • pp.1-11
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    • 2022
  • To evaluate the bearing strength of red pine cross-laminated timber (CLT) with self-tapping screw (STS), which is widely used as a fastener for connection in CLT building, the bearing test was conducted. Accoring to the STS's diameters (8, 10, 12 mm), the bearing test specimens with half hole were manufactured. Bearing strength was compared and reviewed in consideration of the configuration in STS and the loading direction to the grain of red pine. As a result of the bearing test on the STS's diameter, the yield bearing load increases as the larger diameter of the STS in all directions of the red pine. The bearing strength of the thread part (thread + tip) was higher than the shank part (shank + shank cutter). In compared with the directions to the grain of red pine, the bearing strength of the cross section parallel to the loading direction was the highest, and the tangent section was the lowest bearing strength. The average bearing strength of the loading direction in parallel to the grain was 23.43 MPa, which was about 45% higher than the average 16.16 MPa in perpendicular to the grain. The predicted bearing strength calculated by Eurocode (EN) and Korean Building Code (KBC)'s equation was lower than the experimental value. It is nessesary to propose the new equations of bearing strength reflected the configuration information of STS.