• Title/Summary/Keyword: pellet form

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CaO Manufacture for $CO_2$ Adsorption at a High Temperature (고온에서의 이산화탄소 흡착을 위한 흡착제 CaO 제조)

  • Lee Tae-Jong;Kim Gil-Soo;Baek Il-Hyun;Kim Bu-Ung
    • Journal of the Korean Institute of Gas
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    • v.5 no.4 s.16
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    • pp.27-32
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    • 2001
  • It is desired that carbon dioxide causing a greenhouse effect be removed at a high temperature and high pressure in a steam reforming reaction. In this research, a pellet form of adsorbent CaO is employed to capture $CO_2$. The adsorbent was manufactured using a high pressure molding on powdered $CaCO_3$ followed by calcination. Then its properties were analyzed and the adsorption experiments were carried out in a batch adsorption chamber. The pore area was found to be dependent on a molding pressure and the pore distribution showed two peaks. It is examined that $CO_2$ binds to CaO by means of chemisorption and its maximum conversion is nearly $80\%$ at $700^{\circ}C$.

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Optimazation of Submerged Culture Conditions for Exo-Biopolymer Production by Paecilomyces japonica

  • Bae, Jun-Tae;Sinha, Jayanta;Park, Jong-Pil;Song, Chi-Hyun;Yun, Jong-Won
    • Journal of Microbiology and Biotechnology
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    • v.10 no.4
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    • pp.482-487
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    • 2000
  • Optimization of submerged culture conditions for the production of exo-biopolymer from Paecilomyces japonica ws studied. Maltose, yeast extract, and potassium phosphate were the most suitable sources of carbon, nitrogen, and inorganic salt, respectively, for both production of the exo-biopolymer and mycelial growth. The optimal culture conditions in a flask culture were pH 5.0, $25^{\circ}C$, and 150 rpm in a medium containing (as in g/l) 30 maltose, 6 yeast extruct, 2 polypeptone, $0.5{\;}K_3HPO_4,{\;}0.2{\;}KH_2PO_4,{\;}0.2{\;}MnSO_4{\cdot}5H_2O,{\;}0.2{\;}MgSO_4{\cdot}7H_2O$. Exo-biopolymer production and mycelial growth in the above suggested medium were significantly increased in a 2.5-1 jar fermentor, where the maximum biopolymer concentration was 8 g/l. The morphological changes of the mycelium in the submerged culture were observed within pH ranges from 4.0 to 9.0; i.e., growth of the filamentous form was optimal at culture pHs of 5.0 and 6.0, whereas pellet was formed at other pHs.

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Preparation, Characterization and Low Frequency a.c. Conduction of Polypyrrole-Lead Titanate Composites

  • Basavaraja, C.;Choi, Young-Min;Park, Hyun-Tae;Huh, Do-Sung;Lee, Jae-Wook;Revanasiddappa, M.;Raghavendra, S.C.;Khasim, S.;Vishnuvardhan, T.K.
    • Bulletin of the Korean Chemical Society
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    • v.28 no.7
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    • pp.1104-1108
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    • 2007
  • Conducting Polypyrrole-lead titanate (PPy/PbTiO3) composites have been prepared by in situ deposition technique by placing different wt.% of fine grade powder of PbTiO3 (10, 20, 30, 40, and 50%) during polymerization of pyrrole. The composites formed were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), and thermogravimetric analysis (TGA), and these data indicate that PbTiO3 particles are dominating with an increase in crystallinity as well as thermal stability of the composites. The results on the low frequency dielectric studies which are obtained in the form of pressed pellet state are interpreted in terms of Maxwell Wagner polarization, which are responsible for the dielectric relaxation mechanism and frequency dependence of conductivity.

Characterization of Water Vapor Transmission & Dielectric Breakdown in Insulation Materials for Jacket Compound (자켓 컴파운드용 절연재의 수증기투과 및 절연파괴 특성)

  • Song, Jae-Joo;Han, Jae-Hong;Song, IL-Keun;Han, Yong-Hee;Han, Byung-Sung
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.11b
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    • pp.52-56
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    • 2001
  • Experiments of 2 type on insulating compounds accomplished to change PVC using in URD(Underground) power cable jacketing. one was DB (Dielectric Breakdown) test on the pure base resins and the others were WVT(Water Vapor Transmission) test on the compounds which contained C/B(Carbon Black), anti-oxidant to base resin. a kind of specimens made by pressing to resin of pellet or lump form was HDPE(High Density Polyethylene), MDPE(Medium Density Polyehylene), LDPE(Low Density Polyethylene), LLDPE(Linear Low Density Polyethylene), PVC (Polyvinyl Chloride). As a results of AC DB and WVT test, we saw that strength of Insulation was HDPE > LLDPE ≒ MDPE > LDPE and WVT ratio was HDPE < LLDPE < MDPE < LLDPE ≒ LDPE${\ll}$PVC. WVT of PVC using for jacket showed characteristic 15 times more than MDPE or LLDPE. Therefore, to development of watertightness cable, our works present need of Changing in insulating materials

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A Study on the Dynamic Viscoelasticity of EVA/Acetylene Black Composites (EVA/Acetylene Black 복합체의 동역학적 점탄성 분석)

  • Lee, Kyoung-Yong;Yang, Jong-Seok;Choi, Yong-Sung;Nam, Jong-Chul;Sung, Baek-Ryong;Park, Dong-Ha;Park, Dae-Hee
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2005.11a
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    • pp.140-141
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    • 2005
  • To measure elastic properties of semiconducting materials in power cable, we have investigated modulus of EVA/acetylene black composite showed by changing the content of acetylene black. The specimen was primarily kneaded in material samples of pellet form for 5 minutes on rollers ranging between 70[$^{\circ}C$] and 100[$^{\circ}C$]. Then this was produced as sheets after pressing for 20 minutes at 180[$^{\circ}C$] with a pressure of 200[kg/cm]. The contents of conductive acetylene black were 20, 30 and 40[wt%], respectively. The modulus experiment was measured by DMA 2980. The ranges of measurement temperature were from -50[$^{\circ}C$] to 100[$^{\circ}C$] and measurement frequency is 1[Hz]. The modulus of specimens was increased according to an increment of acetylene black content. And modulus was rapidly decreased at the glass transition temperature. The tan$\delta$ of specimens was decreased according to an increment of acetylene black content.

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Study on the viscoelasticity properties of EBA/Carbon Black composites by temperature changes (온도 변화에 따른 EBA/카본블랙 복합체의 점탄성 특성에 관한 연구)

  • Yang, Jong-Seok;Lee, Kyoung-Yong;Choi, Yong-Sung;Nam, Jong-Chul;Park, Dong-Ha;Park, Dae-Hee
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2005.11a
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    • pp.136-137
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    • 2005
  • To measure elastic properties of semiconducting materials in power cable, we have investigated modulus of EBA/carbon black composite showed by changing the content of carbon black. The specimen was primarily kneaded in material samples of pellet form for 5 minutes on rollers ranging between 70[$^{\circ}C$] and 100[$^{\circ}C$]. Then this was produced as sheets after pressing for 20 minutes at 180[$^{\circ}C$] with a pressure of 200[kg/cm]. The contents of conductive carbon black were 20, 30 and 40[wt%], respectively. The modulus experiment was measured by DMA 2980. The ranges of measurement temperature were from -50[$^{\circ}C$] to 100[$^{\circ}C$] and measurement frequency is 1 [Hz]. The modulus of specimens was increased according to an increment of carbon black content And modulus was rapidly decreased at the glass transition temperature. The tan$\delta$ of specimens was decreased according to an increment of carbon black content.

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A Study on the Dielectric Properties of EVA/Carbon Black Composites (EVA/카본블랙 복합체의 유전특성에 관한 연구)

  • Lee, K.Y.;Yang, J.S.;Lee, K.W.;Choi, Y.S.;Park, D.H.
    • Proceedings of the KIEE Conference
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    • 2005.07c
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    • pp.1893-1895
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    • 2005
  • To measure electrical properties of semiconducting materials in power cable, we have investigated dielectric properties of EVA showed by changing the content of carbon black. The specimen was primarily kneaded in material samples of pellet form for 5 minutes on rollers ringing between $70[^{\circ}C]$ and $100[^{\circ}C]$. Then that was produced as sheets after pressing for 20 minutes at $180[^{\circ}C]$ with a pressure of 200[kg/cm]. The contents of conductive carbon black were 20, 30 and 40(wt%), respectively The dielectric properties of specimens were measured by dielectric thermal analyzer (CONCEPT 40, NOVOCONTROL). Measuring frequencies were 10, 60, 100, 1000, 10000, 100000, 1000000(Hz) and measuring temperatures were -40, -20, 20, $90[^{\circ}C]$. From above experimental result, permittivity was increased, while $tan{\delta}$ was decreased according to an increment of the content of carbon black.

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Formation and Dispersion Measurement in Semiconducting Materials Using the SEM and AFM (SEM과 AFM을 사용한 반도전 재료 내 카본블랙의 형태 및 분산성 측정)

  • Lee, Kyoung-Yong;Yang, Jong-Seok;Nam, Jong-Chul;Choi, Yong-Sung;Park, Dong-Ha;Park, Dae-Hee
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2005.07a
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    • pp.236-237
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    • 2005
  • To measure surface roughness and smoothness of semiconducting materials in power cable, we have investigated the formation and growth process of carbon black showed by changing the content of carbon black. The specimens were primarily kneaded in material samples of pellet form for 5 minutes on rollers ranging between 70[$^{\circ}C$] and 100[$^{\circ}C$]. Then they were produced as sheets after pressing for 20 minutes at 180[$^{\circ}C$] with a pressure of 200[kg/cm]. The contents of conductive carbon black were the variable, and their contents were 20, 30 and 40[wt%], respectively. The surface roughness and smoothness of specimens were measured by SEM and AFM. From SEM experimental result, carbon black in specimens formed matrix as a particles. Also we showed growth process of carbon black according to an increment of the content of carbon black. From AFM experimental result, surface roughness of specimens decreased according to an increment of the content of carbon black.

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Practical resolution of angle dependency of multigroup resonance cross sections using parametrized spectral superhomogenization factors

  • Park, Hansol;Joo, Han Gyu
    • Nuclear Engineering and Technology
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    • v.49 no.6
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    • pp.1287-1300
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    • 2017
  • Based on the observation that ignoring the angle dependency of multigroup resonance cross sections within a fuel pellet would result in nontrivial underestimation of the spatial self-shielding of flux, a parametrized spectral superhomogenization (SPH) factor library (PSSL) method is developed as a practical means of resolving the problem. Region-wise spectral SPH factors are calculated by the normal and transport corrected SPH iterations after ultrafine group slowing down calculations over various light water reactor pin-cell configurations. The parametrization is done with fuel temperature, U-238 number density, fuel radius, moderator source represented by ${\Sigma}_{mod}V_{mod}$, and the number density ratio of resonance nuclides to that of U-238 in a form of resonance interference correction factors. The parametrization is successful in that the root mean square errors of the interpolated SPH factors over the fuel regions of various pin-cells are within 0.1%. The improvement in reactivity error of the PSSL method is shown to be superior to that by the original SPH method in that the reactivity bias of -200 pcm to -300 pcm vanishes almost completely. It is demonstrated that the environment effect takes only about 4% in the reactivity improvement so that the pin-cell based PSSL method is effective in the assembly problems.

Formulation of Omeprazole Preparations using Omeprazole-Ethylendiamine Complex (오메프라졸-에칠렌디아민 복합체를 이용한 제제설계)

  • Oh, Sea-Jong;Park, Seong-Bae;Park, Sun-Hee;Hwang, Sung-Joo;Rhee, Gye-Ju
    • Journal of Pharmaceutical Investigation
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    • v.25 no.1
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    • pp.19-29
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    • 1995
  • The study was carried out to develop useful formulation for omeprazole(OMP) through OMP-ethylendiamine complex(OMPED), and the pharmaceutical properties of formula were tested to find out the difference in vivo behaviors of formulations between the free and complexed OMP. Oral and suppository dosage forms were also formulated and the dissolution profiles and pharmacokinetic parameters were measured to observe the difference in bioavailability between the free and complex form, and the correlation between dissolution rate and bioavailability was evaluated. The results are summarized as follows; In the case of formulation for oral administration, the release of OMP from enteric OMPED pellets was found satisfactory to the requirement standard and no decomposition of OMP in the pellets was found in acidic solution. Therefore the enteric OMPED pellets are anticipated to be a stable formulation. The release of OMP from OMPED tablet with chitosan as excipient and coated with cellulose acetate phthalate was found to be significantly retarded. The results of bioavailability test for OMP and OMPED tablets with lactose-excipient showed that the AUC value of OMP tablet was $116.89\;{\mu}g\;{\cdot}\;min/ml$, that of OMPED tablet was $161.10\;{\mu}g\;{\cdot}\;min/ml$, respectively. The reason why was thought that OMP decomposes more readily in body than OMPED, and the AUC of the tablet with chitosan-excipient and coated with cellulose acetate phthalate was most enhanced. In the case of bioavailability for suppositories with OMP, $OMP-{\beta}\;-cyclodextrin$ complex and OMPED, the AUC of OMPED suppository was most increased. From the above results, it is thought that the more stable and bioavailable oral or rectal dosage forms could be developed by using the OMPED as a potential OMP complex.

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