• 제목/요약/키워드: pectin analysis

검색결과 77건 처리시간 0.023초

Low-ester Pectin Gel의 단단함과 강도(强度)의 예측 (Prediction of Firmness and Strength of Low-ester Pectin Gel from Chemical Composition)

  • 김우정
    • 한국식품과학회지
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    • 제18권5호
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    • pp.364-371
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    • 1986
  • High-ester pectin을 HCI 단독 또는 HCI 과 $NH_4OH$를 병용하여 demethylation 시킨뒤 얻어진 low-ester pectin(LM pectin)으로 gel을 제조하였다. LM pectin gel의 단단함과 강도(强度)를 측정한 결과 HCI로 처리된 LM pectin gel은 일반적으로 강도(强度)가 약하고 거칠며 탄력이 없었다. 반면 $HCl-NH_4OH$로 처리한 LM pectin gel은 텍스쳐가 부드럽고 탄력이 좋았다. 물리적 성질에 대한 LM pectin의 화학적 조성의 상관 관계에서 단단함(Sag값)에 대한 ester함량 및 분자량, 그리고 강도(强度)(puncture stress)에 대한 amide 및 ester함량 EH는 분자량 간에는 유의성 있는 관계가 밝혀졌다. 상관성이 높은 화학적 인자에서 LM pectin gel의 물리적 성질을 예측할 수 있는 관계식을 산출하였다.

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녹두전분과 감자전분 복숭아편의 질감과 관능적 특성 (The Effect of Addition of Mungbean Starch and Potato Starch on the Textural and Sensory Characteristics of Peach Pyun)

  • 조재욱
    • 한국식품영양학회지
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    • 제12권2호
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    • pp.156-163
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    • 1999
  • This study was evaluate of chemical properties. textural charact6eristics and sensory properties prod-uced peach pyuns through the change of gelling agents such as mungbean starch potato starchy and pec-tin and of sugar density with 10%, 20%, and 30%. Sensory evaluation was that peach pyun added mun-gbean starch was more preferable in appearance and texture than peach pyun added potato starch. Peac-h pyun added 0% pectin was more preferable than peach pyun with 1% pectin. As a result of texture analysis the texture of peach pyun added mungbean starch was denser than that added potato starch. Adding 1% pectin to peach pyun increased mechanical properties such as hardness and chewiness. Mun-gbeaan starch pyun with pectin on lightness Potato starch pyun with pectin on redness and potato star-ch pyun with pectin on yellowness were significant(p<001). Lightness has a tendency to decrease with increasing sugar density. Adding 1% pectin has the effect to increase lightness redness and yellowness. The subject parameters that effect overall quality on sensory evaluation were found taste quality tex-ture quality hardness adhesiveness and taste by using regression analysis.

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식이섬유 첨가에 의한 백설기의 특성변화에 관한 연구 (Effect of Addition of Dietary Fibers on Quality of Backsulgies)

  • 최인자;김영아
    • 한국식품조리과학회지
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    • 제8권3호
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    • pp.281-289
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    • 1992
  • The physicochemical, rheological and sensory characteristics of Backsulgies added with dietary fibers-cellulose, pectin and wheat bran-were investigated. The maximum acceptable ratio of fibers was 10% for wheat bran or cellulose, 3% for pectin. As me results of physicochemical analysis, cellulose and pectin had larger water-binding capacity man wheat bran. Swelling power was increased with temperature increment. But the type of added dietary fiber did not make significant differences. The degree of gelatinization was measured by maltose content. The retrogradation of backsulgies was significantly delayed by the addition of dietary fibers. The retardation effect of dietary fibers for retrogradation of backsulgies was also proved by textural analysis and time constant determination of Avrami equation. Pectin had especially excellent delaying effect while me storage time extended. There were no significant differences in sensory characteristics between me backsulgi with no dietary fibers and backsulgies added with cellulose 3%, pectin 1% and wheat bran 3%. Therefore, we concluded mat cellulose 3%, pectin 1% and wheat bran 3% were me optimum addition ratios, which have the delaying effect of retrogradation, and which could be accepted as same as conventional backsulgies organoreptically.

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Pectin from Passion Fruit Fiber and Its Modification by Pectinmethylesterase

  • Contreras-Esquivel, Juan Carlos;Aguilar, Cristobal N.;Montanez, Julio C.;Brandelli, Adriano;Espinoza-Perez, Judith D.;Renard, Catherine M.G.C.
    • Preventive Nutrition and Food Science
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    • 제15권1호
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    • pp.57-66
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    • 2010
  • Passion fruit fiber pectin gels represent a new alternative pectin source with potential for food and non-food applications on a commercial scale. Pectic polysaccharides were extracted from passion fruit (Passiflora edulis) fiber using citric acid as a clean catalyst and autoclaved for 20 to 60 min at $121^{\circ}C$. The best condition of pectin yield with the highest molecular weight was obtained with 1.0% of citric acid (250 mg/g dry passion fruit fiber pectin) for 20 min of autoclaving. Spectroscopic analyses by Fourier transform infrared, enzymatic degradation reactions, and ion-exchange chromatography assays showed that passion fruit pectin extracted for 20 min was homogeneous high methoxylated pectin (70%). Gel permeation analysis confirmed that the pectin extract obtained by autoclaving by 20 min showed higher molecular weights than those autoclaved for 40 and 60 min. Passion fruit pectin extracted for 20 min was enzymatically modified with fungal pectinmethylesterase to create restructured gels. Short autoclave treatment (20 min) with citric acid as extractant resulted in a significant increase of gel strength, improving pectin extraction in terms of functionality. The treatment of solubilized material (pectic polysaccharides) in the presence of insoluble material (cellulose and hemicellulose) with pectinmethylesterase and calcium led to the creation of a stiffer passion fruit fiber pectin gel, while syneresis was not observed.

펙틴의 정제 및 분석 (Purification and Analysis of Pectins)

  • 황재관
    • 한국식품영양과학회지
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    • 제22권4호
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    • pp.500-509
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    • 1993
  • Pectins present in the primary cell walls and middle lamellae of plant cell walls are extracted by water, cheating agents, acid or alkali solutions. However, some neutral contaminating components are extracted in conjunction with pectins during the extraction process. Thus, the accurate characterization of physi-cochemical properties of pectins necessitates to get rid of the impurities. In this review, dialysis, alcohol precipitation, ion exchange chromatography and metal precipitation were compared as procedures to purify the pectin extracts. In addition, the chemical methods to analyze pectins are discussed in terms of three major chemical constituents, i.e., anhydrogalacturonic acid, methoxyl groups and neutral sugars.

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여러가지 첨가제에 의한 옥수수전분 겔(Gel)의 특성변화 (The Characteristic Changes of Corn Starch Gels by Various Types of Additives)

  • 주난영;이혜수
    • 한국식품조리과학회지
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    • 제7권2호
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    • pp.19-23
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    • 1991
  • 본 연구에서는 gel화를 유도할 수 있는 첨가제를 첨가하여 만든 5가지 옥수수 전분 gels와 아무것도 첨가하지 않은 control옥수수 전분 gel의 관능적 물성적 특성을 조사 비교하였다. 1. 관능검사를 실시한 결과 \circled1 Agar의 hardness는 control보다 유의하게 높았고, pectin은 control 보다 유리하게 낮았다. \circled2 CMC와 pectin의 adhesiveness는 control 보다 유의하게 높았고 agar는 control보다 유의하게 낮았다. \circled3 전체적인 acceptability는 CMC와 Pectin은 control보다 유의하게 선호도가 낮았고 나머지 시료들은 control과 유의차가 없었다. 2. Instron을 이용한 물성검사 결과 \circled1 Agar의 hardness는 control보다 유의하게 높았고, 나머지 시료들의 hardness는 control보다 유의적으로 낮았다. \circled2 Agar와 casein의 cohesiveness는 control보다 유의하게 높았으며 gelatin은 control보다 유의하게 낮았다. 3. 관능검사나 Instron에 의한 기계적 검사에 있어서 시료의 차이를 가장 잘 구분해 주는 특성치는 hardness라고 생각되어진다

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한국산 사과의 품종별 펙틴물질들에 관한 연구 (A Study on Pectic Substances of Korean Apple Varieties)

  • 임화재;이혜수
    • 한국식품조리과학회지
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    • 제2권1호
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    • pp.65-70
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    • 1986
  • 수확적기의 한국산 사과품종별 총펙틴함량과 각 펙틴 fraction 함량을 알아보고 2% Sodium hexa metaphosphate (SHMP)로 추출한 펙틴의 품종간 그리고 시판 펙틴과의 성분을 비교하였다. Nitta 방법에 의해 정량한 사과의 품종별 펙틴함량은 건조중량으로 1.76∼4.0%로 품종간에 차이를 보여 국광이 4.0%로 가장 높았으며 스퍼 얼리 브래이스 골덴 딜리셔스, 후지, 홍옥의 순이었다. 각 펙틴 fraction을 보면 용해성 펙틴함량은 국광이 가장 낮았고 스퍼 얼리 브레이스와 골덴 딜리셔스가 가장 높았다. 한편 스퍼 얼리 브레이스와 골덴 딜리셔스의 불용성 펙틴함량이 낮은 것으로 보아 이 두 사과는 숙성초기에 펙틴물질이 많이 변하는 것 같다. 2% SHMP로 추출한 총펙틴질의 성분 분석에서 회분함량은 사과품종간에 차이를 보이며 시판 펙틴보다 높았다. Anhydrogalacturonic acid (AUA) 함량은 시판 펙틴보다 낮으며 품종간에 범위가 다양했다. 메톡실함량은 시판펙틴보다 높으며 모든 사과품종이 70% 이상의 에스터화정도를 가졌다.

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반응표면 분석법을 이용한 오미자편의 물성특성 (Optimization of Rheological Properties for the Processing of Omija-pyun(Omija jelly) by Response Surface Methodology)

  • 정희선;주나미
    • 한국식품조리과학회지
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    • 제19권4호
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    • pp.429-438
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    • 2003
  • The optimization of Omija-pyun as a traditional dessert, with the most European taste and year round availability, was studied with regard to its texture. The response surface methodology was used to determine the optimal composition of Omija-pyun as a European style dessert. The texture, including the springiness, gumminess, cohesiveness, adhesiveness, hardness and chewiness, was measured using TPA parameters (TA-HD Texture Analyser, stable micro system, UK). The texture of Omija-pyun was influenced by pectin and sucrose to the first linear order. The properties of springiness and adhesiveness were influenced by pectin x pectin to the second quadratic order. No cross product effects between ingredients were found from the analysis. The maximum springiness was obtained with 42g of pectin, 450g of sucrose, 110g of glucose syrup and 4.8g of tartaric acid. The maximum chewiness was with 55g of pectin, 330g of sucrose, 140g of glucose syrup and 5.7g of tartaric acid. The maximum adhesiveness was achieved using 17g of pectin and 400g of sucrose. The gumminess and hardness increased with increasing pectin content, and a cross product effect was observed(Eds note: you said earlier that no cross product effects between the ingredients was found\ulcorner) between sucrose and glucose syrup.

유자 착즙액을 이용한 유자젤리의 제조 (Manufacture of Citron Jelly Using the Citron-extract)

  • 김인철
    • 한국식품영양과학회지
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    • 제28권2호
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    • pp.396-402
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    • 1999
  • To increase the utilization of citron(Citrus junos), manufacturing conditions of citron jelly were studied. Citron extract was diluted 7 fold for jelly processing and it's pH was 2.64. Due to the low pH of citron extract, 2.5∼3.0% of pectin was added which was slightly higher than the amount for ordinary jelly process. To reduce the loss of citron flavor and vitamin C, it was heated for 10 min. and found to be enough for proper hardness of jelly. Agar and gelatin was used as jellying agents to improve the physical properties of pectin jelly. From the result of compression curve analysis, addition of 5% and 7% of gelatin were more effective in jelly texture than agar in 1.5% and 2.5% pectin jelly, respectively. Sucrose was replaced by glucose and oligosaccharide; galactooligosaccharide, fructooligosaccharide and isomaltooligosaccharide. From the sensory evaluation analysis, 30% of sucrose and 30% of isomaltooligosaccharide in jelly was evaluated as superior to other sugars.

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대체 감미료와 low methoxyl pectin을 이용한 저열량 pectin gel의 제조 (Replacement of sucrose with other sweeteners and low methoxyl pectin in low caloric pectin gels)

  • 오혜숙;이명희;문수재
    • 한국식품조리과학회지
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    • 제9권4호
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    • pp.289-292
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    • 1993
  • 당알코올의 대체 감미료로서의 유용성을 검토하기 위한 목적으로 LMP jelly들을 제조하여 품질 특성을 비교하였다. 관능검사 결과 LMP jelly의 감미도는 설탕의 50%를 maltitol로 대치하였을때 현저하게 감소하였고, 반면 같은 50%를 3종류의 당알코올로 혼합 사용한 경우에는 제조시 당알코올의 대체 가능성을 높음을 시사하였다.

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