• 제목/요약/키워드: particulate composite

검색결과 108건 처리시간 0.033초

골 생체조직공학을 위한 복합 세라믹 골 지지체의 제조와 생체역학적 특성 (Fabrication and Biomechanical Characteristics of Composite Ceramic Bone Scaffolds for Bone Tissue Engineering)

  • 김은석;정종훈
    • Journal of Biosystems Engineering
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    • 제29권5호
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    • pp.457-466
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    • 2004
  • Novel porous composite ceramic bone scaffolds composed of biodegradable PHBV(polyhydroxybutyrate-co-hydroxyvalerate) and TA(toothapatite) have been fabricated for bone tissue engineering by a modified solvent casting and particulate leach-ing method with salt-contained heat compression technique. The results of this study suggest that the PHBV-TA composite scaffold, especially the scaffold containing 30 weight$\%$ of TA may be a good candidate far bone tissue engineering of non-load bearing area in oral and maxillofacial region.

Hot Deformation Behavior of P/M Al6061-20% SiC Composite

  • Asgharzadeh, Hamed;Simchi, Abdolreza
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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    • pp.855-856
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    • 2006
  • In the present work, hot workability of particulate-reinforced Al6061-20%SiC composite produced by direct hot extrusion technique was studied. Uniaxial hot compression test at various temperatures and strain rates was used and the workability behavior was evaluated from the flow curves and the attendant microstructures. It was shown that the presence of SiC particles in the soft Al6061 matrix deteriorates the hot workability. Bulging of the specimens and flow lines were observed, which indicate the plastic instability during hot working. Microstructure of the composites after hot deformation was found to be heterogeneous, i.e. the reinforcement clusters were observed at the flow lines. The mechanism of deformation was found to be controlled primarily by dynamic recrystallization.

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(1-x) [0.5PZT-0.25PNN-0.25PZN]- x [Ni0.9Zn0.1Fe2O4] 세라믹스의 압전/자성 성질 및 자기전기적 효과 (Piezoelectric/magnetic Properties and Magnetoelectric Effects in (1-x) [0.5PZT-0.25PNN-0.25PZN] - x [Ni0.9Zn0.1Fe2O4] Particulate Ceramic Composites)

  • 박영권;손세모;류지구;정수태
    • 한국전기전자재료학회논문지
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    • 제23권11호
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    • pp.869-874
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    • 2010
  • Magnetoelectric composites with compositions (1-x)[0.5PZT-0.25PNN-0.25PZN](ferroelectric) - x[$(Ni_{0.9}Zn_{0.1})Fe_2O_4$](ferrite) in which x varies as 0, 0.1, 0.2, 0.4, 0.6, 0.8, 1.0 were prepared by conventional ceramic process. The presence of two phases (ferroelectric phase with large grain and ferrite phase with small grain) in the particulate ceramic composites was confirmed by XRD, SEM and EDX. The ferroelectric and magnetic properties of the composites were studied by measuring the P-E and M-H hysterisis loop on the composite composition (x=0, 0.1, 0.2, 1), they were strongly affects of the phase content in composite. The magnetoelectric votage was measured as a function of DC magnetic field and the maximum magnetoelectric voltage coefficient of 14 mV/cm Oe was observed in x=0.2(80 mol% ferroelectric and 20 mol% ferrite phase).

고에너지 밀링 및 합성반응에 의한 Fe-TiC 복합분말 제조 (Fabrication of Fe-TiC Composite Powder by High-Energy Milling and Subsequent Reaction Synthesis)

  • 안기봉;이병훈;이용희;;김지순
    • 한국분말재료학회지
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    • 제20권1호
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    • pp.53-59
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    • 2013
  • Fe-TiC composite powder was fabricated via two steps. The first step was a high-energy milling of FeO and carbon powders followed by heat treatment for reduction to obtain a (Fe+C) powder mixture. The optimal condition for high-energy milling was 500 rpm for 1h, which had been determined by a series of preliminary experiment. Reduction heat-treatment was carried out at $900^{\circ}C$ for 1h in flowing argon gas atmosphere. Reduced powder mixture was investigated by X-ray Diffraction (XRD), Field Emission-Scanning Electron Microscopy (FE-SEM) and Laser Particle Size Analyser (LPSA). The second step was a high-energy milling of (Fe+C) powder mixture and additional $TiH_2$ powder, and subsequent in-situ synthesis of TiC particulate in Fe matrix through a reaction of carbon and Ti. High-energy milling was carried out at 500 rpm for 1 h. Heat treatment for reaction synthesis was carried out at $1000{\sim}1200^{\circ}C$ for 1 h in flowing argon gas atmosphere. X-ray diffraction (XRD) results of the fabricated Fe-TiC composite powder showed that only TiC and Fe phases exist. Results from FE-SEM observation and Energy-Dispersive X-ray Spectros-copy (EDS) revealed that TiC phase exists uniformly dispersed in the Fe matrix in a form of particulate with a size of submicron.

Properties of Hot Pressed Alumina-Titanium Diboride Particulate Composites

  • Park, Dong-Soo;Han, Byung-Dong
    • The Korean Journal of Ceramics
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    • 제4권3호
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    • pp.227-230
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    • 1998
  • Alumina($Al_2O_3$)-Titanium Diboride($TiB_2) particulate composites were fabricated by hot pressing of the powder mixture that was prepared from Self-propagating High Temperature Synthesis (SHS) product and commercial powders. Their propeties were examined in order to find feasibility of using SHS for making the high performance ceramic composite. $TiB_2 particles obtained by grinding the SHS product were finer than the commercial powders. Hot pressed sample containing the SHS products exhibited higher strength than the one prepared from the commercial powders.

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EFFECTS OF PARTICLE RESONANCE ON DISPERSION OF ELASTIC WAVES IN PARTICULATE COMPOSITES

  • Kim, J.Y.;Ih, J.G.;Lee, B.H.
    • 한국음향학회:학술대회논문집
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    • 한국음향학회 1994년도 FIFTH WESTERN PACIFIC REGIONAL ACOUSTICS CONFERENCE SEOUL KOREA
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    • pp.734-739
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    • 1994
  • Elastic wave propagation in discrete random medium is studied to evaluate the effects of particle resonance on dispersion and attenuation of composite materials containing spherical inclusions. The frequency-dependent wave speed and attenuation coefficient can be obtained from proposed self-consistent method. It can be observed that the abrupt increase of effective wave speed and the concurrent peak of attenuation at low frequency is due to the lowest resonance of particles, whereas those in high frequency region are due to higher ones. The lowest resonance is mainly caused by the density mismatch and higher resonances by the stiffness mismatch between matrix and particles. The dispersion and attenuation of elastic waves in particulate composites are affected by the lowest resonance much than by higher ones.

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입자분산강화 알루미늄 복합재의 압출가공특성에 관한 연구 (A Study on Hot Extrusion Characteristics of Particulate Reinforced Aluminium Matrix Composite.)

  • 권혁천;윤의박
    • 한국재료학회지
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    • 제5권8호
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    • pp.953-959
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    • 1995
  • 분말야금법으로 제조된 A6061기 입자분산강화 복합재의 열간압술가공에 있어서 압출특성에 미치는 강화입자의 종류, 빌렛특성 및 암술조건의 영향에 대하여 조사하였다. A6061기 복합재료의 열간 압술 전단 변형저항에 미치는 강화입자종류의 영향은 Si $C_{w}$ > A1$_2$ $O_{3f}$ > A1$_2$ $O_{3f}$ > Si $C_{p}$의 순으로 되었으며, 모든 강화입자에서 부피분율이 증가함에 따라서 Kw값도 증가하였다. 압출조건, 강화입자의 첨가량 및 첨가입자의 평균입도에 관계없이 A1$_2$ $O_{3p}$가 첨가된 복합재의 열간압출가공에 필요한 소요압력은 Si $C_{p}$의 경우보다 컸다. 압출압력은 압출 다이스 반각이 커질수록 감소하는 경향은 나타났다. 이것은 다이스 반각에 의해 생성되는 빌렛과의 접촉면적이 증가하여 전단마찰응력(m $k_3$)이 상승하기 때문이다. 압출시 압출온도 상승은 저온에서 ~$50^{\circ}C$ 정도 증가하였으며, 압출온도가 50$0^{\circ}C$ 이상이 되면 압출재 표면에 극심한 tearing이 발생하였다. 강화입자의 첨가량이 증가할수록 이 현상은 더 심하게 되었다.게 되었다.

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고속 화염 용사법으로 제조된 WC계 Cr3C2 코팅과 WC계 YSZ 코팅의 마찰 및 마모 거동 연구 (Tribological Behavior Analysis of WC-Ni-Cr + Cr3C2 and WC-Ni-Cr + YSZ Coatings Sprayed by HVOF)

  • 박태준;이계원;오윤석
    • 한국분말재료학회지
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    • 제30권5호
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    • pp.415-423
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    • 2023
  • With the increasing attention to environmental pollution caused by particulate matter globally, the automotive industry has also become increasingly interested in particulate matter, especially particulate matter generated by automobile brake systems. Here, we designed a coating composition and analyzed its mechanical properties to reduce particulate matter generated by brake systems during braking of vehicles. We designed a composition to check the mechanical properties change by adding Cr3C2 and YSZ to the WC-Ni-Cr composite composition. Based on the designed composition, coating samples were manufactured, and the coating properties were analyzed by Vickers hardness and ball-on-disk tests. As a result of the experiments, we found that the hardness and friction coefficient of the coating increased as the amount of Cr3C2 added decreased. Furthermore, we found that the hardness of the coating layer decreased when YSZ was added at 20vol%, but the friction coefficient was higher than the composition with Cr3C2 addition.

Frictional Instabilities of Polymer Composite Containing Barite or Potassium Titanate for Brake Linings

  • Kim, Seong-Jin;Jang, Ho
    • KSTLE International Journal
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    • 제4권2호
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    • pp.60-65
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    • 2003
  • Tribological properties of novolac resin composites containing particulate barite (BaSO$_4$) or potassium titanate (K$_2$Oㆍ6(TiO$_2$))whiskers (two typical space fillers for commercial automotive brake linings) were investigated. The emphasis of the current investigation was given to the effect of the two fillers on the propensity of the stick-slip phenomena and formation of stable rubbing surface. A block-on-disk type tribometer was used for friction assessment. Results showed that the BaSO$_4$-filled composite produced large friction force oscillations at slow sliding speeds and created severe damage on the gray iron counter surface. On the other hand, the composite with $K_2$Oㆍ6(TiO$_2$) whiskers formed a stable rubbing surface and showed smooth sliding behavior without large friction force fluctuation. The microscopic observation of the rubbing surface revealed that the $K_2$Oㆍ6(TiO$_2$)whiskers played a key role in the formation of stable rubbing surface and smooth sliding behavior by effectively reinforcing the resin.

Synergistic effect of clay and polypropylene short fibers in epoxy based ternary composite hybrids

  • Prabhu, T. Niranjana;Demappa, T.;Harish, V.;Prashantha, K.
    • Advances in materials Research
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    • 제4권2호
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    • pp.97-111
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    • 2015
  • Polypropylene short fiber (PP)-clay particulate-epoxy ternary composites were prepared by reinforcing PP short fiber and clay particles in the range of 0.1 phr to 0.7 phr into epoxy resin. Prepared hybrid composites were characterized for their mechanical, thermal and flame retardant properties. The obtained results indicated an increase in impact resistance, tensile strength, flexural strength and Young's modulus to an extent (up to 0.5 phr clay and 0.5 phr PP short fiber) and then decreases as the reinforcing phases are further increased. The thermal stability of these materials are found to increase up to 0.2 phr clay and 0.2 phr PP addition, beyond which it is decreased. Addition of clay is found to have the negative effect on epoxy-PP short fiber composites, which is evident from the comparison of mechanical and thermal properties of epoxy-0.5 phr PP short fiber composite and epoxy-0.5 phr PP short fiber-0.5 phr clay composite hybrid. UL-94 tests conducted on the composite hybrids have showed a reduction in the burning rate. Morphological observations indicated a greater fiber pull with the addition of clay. The performed tests in the present study indicated that materials under investigation have promising applications in construction, agriculture and decorative purposes.