• 제목/요약/키워드: paramagnetic material

검색결과 40건 처리시간 0.022초

집중유도형 교류전위차법에 의한 강자성체 및 상자성체의 2차원 표면결함의 비파괴평가 (Nondestructive Evaluation of 2-Dimensional Surface Crack in Ferromagnetic Metal and Paramagnetic Metal by ICFPD Technique)

  • 김훈;장자철웅;정세희
    • 대한기계학회논문집
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    • 제19권5호
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    • pp.1202-1210
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    • 1995
  • Aiming at nondestructive evaluation of defect with high accuracy and resolution, ICFPD(Induced Current Focusing Potential Drop) technique was newly developed. This technique can be applied for locating and sizing of defects in components with not only simple shape such as plain surface but also more complex shape and geometry such as curved surface and dissimilar joing. This paper describes the principle of ICFPD technique and also the results of 2-dimensional surface crack in ferromagnetic metal(A508 Cl. III steel) and paramagnetic metal (pure aluminum and stainless 304 steel) measured by this technique. Results are that surface defects in each specimen are detected with the difference of potential drop, and potential drops are distributed a similar shape for each metal and each depth. The normalized potential drop ( $V_{\delta}$2/$^{t}$ / $V_{{\delta} 2}$$^{-1}$) max. in the vicinity of defect is varied with the depth of defect. Therefore, ICFPD technique can be used for the evaluation of defect not only in ferromagnetic metal but also in paramagnetic steel..

X-선에 조사된 설탕의 전자 상자성 공명 연구 (A Study of Electron Paramagnetic Resonance of Sugar Irradiated X-ray)

  • 옥치일;손필국;허경찬;손종기;이인;김장환
    • 대한방사선기술학회지:방사선기술과학
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    • 제23권2호
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    • pp.39-42
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    • 2000
  • When ordinary sugar is exposed to ionizing radiation, a number of free radical are created in sugar, and Electron Paramagnetic Resonance (EPR) signal appears from the sugar because of the paramagnetic property of free radical. In this paper, EPR signal intensity has been measured in x-ray irradiated sugar for various absorbed doses, irradiated dose up to 50 Gy. The EPR intensity signals are increased as the x-ray irradiation increases. Also, the fading value decreased to about 3% in 30day after the irradiation. Therefore, the sugar is a useful material for emergency dosimeter as the free radical dosimetry with the EPR equipment.

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The Low-Radiation Dosimetry Application of "tris" Lyoluminescence using Electron Paramagnetic Resonance at Low Temperature

  • Son, Phil-Kook;Choi, Suk-Won;Kim, Sung-Soo;Gwag, Jin-Seog
    • Journal of Magnetics
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    • 제17권3호
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    • pp.172-175
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    • 2012
  • We present a method for detecting very weak radiation by analyzing the inner structure of irradiated tris (lyoluminescence) materials using electron paramagnetic resonance (EPR) at low temperature. Organic materials have been looked into for use in emergency dosimetry of inhabitants around radiation accidents. However, this technology has never been applied to imperceptible radiation doses (< 0.5 Gy) because there is no proper method for detecting the change of inner structure of the subject bombed by very weak radiation at room temperature. Our results show that tris materials can be applied as a radiation detectors of very small radiation doses below 0.05 Gray, if EPR is used at low temperature (130 K ${\leq}$ T ${\leq}$ 270 K). The EPR signal intensity from the irradiated-tris sample had barely faded at all after 1 year.

제1원리 분자궤도계산법에 의한 초기 spin 조건에 따른 $MnO_2$ 반도체의 전자상태 변화 계산 (Calculation on Electronic State of $MnO_2$ Oxide Semiconductor with other initial spin conditions by First Principle Molecular Orbital Method)

  • 이동윤;김봉서;송재성;김현식
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2003년도 추계학술대회 논문집 Vol.16
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    • pp.148-151
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    • 2003
  • The spin density of ${\beta}-MnO_2$ structure was theoretically investigated by $DV-X_{\alpha}$ (the discrete variation $X{\alpha}$) method, which is a sort of the first principle molecular orbital method using Hatre-Fock-Slater approximation. The used cluster model was $[Mn_{14}O_{56}]^{-52}$. The ${\beta}-MnO_2$ is a paramagnetic oxide semiconductor material having the energy band gap of 0.18 eV and an 3 loan-pair electrons in the 3d orbital of an cation. This material exhibits spin-only magnetism and has the magnetic ordering temperature of 94 K. Below this temperature its magnetism appears as antiferromagnetism. The calculations of electronic state showed that if the initial spin condition of input parameters changed, the magnetic state changed from paramagnetic to antiferromagnetic. When d orbital of all Mn atoms in cluster had same initial spin state as only up spin, paramagnetic spin density distribution appeared by the calculation. On the other way, d orbital had alternately changed spin state along special direction the resulted spin distribution showed antiferromagnetism.

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균열을 가진 상자성체의 교류전위차에 미치는 하중의 영향 (Loading Effect on ACPD of a Crack in Paramagnetic Material)

  • 이정희
    • 비파괴검사학회지
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    • 제19권1호
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    • pp.1-7
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    • 1999
  • 교류전위차법 (alternating current potential drop : ACPD)을 이용하여 이차원 표면균열을 갖고 있는 상자성체 (paramagnetic material)의 모드 I (opening mode) 응력확대계수($K_I$)를 실험적으로 평가하기 위하여 하중에 따른 교류전위차 변화(change in ACPD)를 연구하였다. 아울러 하중에 의한 전위차 변화의 원인 그리고 전위차 변화에 미치는 자속(magnetic flux) 탈자(demagnetization) 및 균열길이의 영향을 연구하였다. 상자성체의 교류전위차는 인장하중을 증가시킬수록 선형적으로 감소하였다. 전위차 감소의 원인은 균열선단 주위의 도전율(conductivity)이 인장하중의 증가에 따라 증가하고 이는 시험편의 저항과 내부 인덕턴스를 감소시키기 때문이다. 도전율의 변화는 균열선단 주변의 응력상태에 의존하기 때문에 일정 $K_I$ 변화에 따른 전위차 변화량은 균열길이에 의존하지 않는다. 하중에 의한 전위차변화량은 시험편 주위의 자속의 유무에 영향을 받지만 탈자의 유무에는 영향을 받지 않는다.

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복합 유도전류-누설자속법과 고밀도 홀센서배열에 의한 니켈 코팅 인코넬 시험편의 비파괴검사 (NDT of a Nickel Coated Inconel Specimen Using by the Complex Induced Current - Magnetic Flux Leakage Method and Linearly Integrated Hall Sensor Array)

  • 전종우;이진이;박덕근
    • 비파괴검사학회지
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    • 제27권5호
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    • pp.375-382
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    • 2007
  • 전자기적인 방법을 이용한 비파괴검사는 금속의 표면 및 표면 근방의 균열을 탐상하는데 매우 유용하다. 그러나, 강자성체, 상자성체 또는 강자성체와 상자성체 조직이 혼재되는 경우가 발생하여 기존의 비파괴검사법에 의하면 탐상신호의 해석에 어려움이 많다. 또한, 경우에 따라서는 국부적인 자성체의 존재를 유사결함으로 오해 또는 큰 결함을 국부적인 자성체의 존재로 오해할 수 있다. 한편, 원자력 발전소의 구조물 소재로 중요하게 사용되고 있는 Inconel은 결함 발생시 Nickel로 피막 처리한 후 연장 사용하게 된다. 이때, 상자성체인 Inconel과 강자성체인 Nickel의 혼재에 의하여 결함을 탐상하기 곤란하다. 본 연구에서는 Inconel 부재, Nickel 코팅부위 및 경계면에 존재하는 결함을 탐상하기 위한 방법으로써, 복합 유도전류-누설자속법과 고밀도 홀센서 배열을 이용한 라인스캔형 자기카메라를 제안하고, 탐상 가능 결함의 깊이 및 정량 평가 가능성에 대하여 보고한다.

FEF 탐상법을 이용한 상자성체 표면결함 평가 (The Evaluation of Surface Crack in Paramagnetic Material by FEF Technique)

  • 김훈
    • 비파괴검사학회지
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    • 제24권5호
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    • pp.532-537
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    • 2004
  • 전자기장을 유도하는 원리를 기초로 한 새로운 비파괴탐상법인 FEF법을 개발하였다. 이 탐상법은 전자기장을 유도하는 유도선과 이를 감지하는 감지부로 구성되어 있고, 비접촉 방식으로 탐상을 실시한다. 본 연구는 알루미늄합금, 스테인레스강과 인코넬 합금강의 재료에 방전 가공한 결함에 대하여 결함 검출 및 결함 깊이에 대한 평가를 실시하였다. 결함이 없는 영역에서의 측정전압은 lift-off에 의존한다. 결함영역에서 탐촉자가 결함에 가까이 접근할수록 전압은 증가하고, 결함위치에서 최고전압으로 측정되며, 이 최고치는 결함의 깊이에 따라 변화한다. 각 재료에 대한 전압분포 같은 경향으로 측정된다.

재료의 선택적 사용에 의한 금형의 국부적 유도가열기법 (Localized Induction-Heating Method by the Use of Selective Mold Material)

  • 박근;도범석;박정민;이상익
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2009년도 춘계학술대회 논문집
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    • pp.168-171
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    • 2009
  • High-frequency induction is an efficient way to heat mold surface by electromagnetic induction in a non-contact procedure. Though the induction heating has an advantage in terms of its rapid-heating capacity on the mold surface, it still has a restriction on mold temperature control due to geometric restriction of an induction coil according to the mold shape. It has been recently applied to the injection molding of thin-walled parts or micro/nano structures. For localized induction heating, an injection mold composed of ferromagnetic material and paramagnetic material is used. The electromagnetic induction concentrates on the ferromagnetic material, from which we can selectively heat for the local mold elements. The present study proposed a localized induction heating method by means of selective use of mold material. The feasibility of the proposed heating method is investigated through the comparison of experimental observations according to the mold material.

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Paramagnetic Zn(1-x)MnxO (0.00≤x≤0.06) Nanoparticles Prepared by The Coprecipitation Method

  • Harsono, Heru;Wardana, I Nyoman Gede;Sonief, Achmad As'ad;Darminto, Darminto
    • Transactions on Electrical and Electronic Materials
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    • 제18권1호
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    • pp.46-50
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    • 2017
  • The Zn1-xMnxO ($0.00{\leq}x{\leq}0.06$) samples have been synthesized in the form of powder by the coprecipitation method at low temperature using $Zn(CH_3COO)_2$. $2H_2O$ and $Mn(CH_3COO)_2$. $4H_2O$ powders, as well as HCl and $NH_4OH$ solutions as starting materials. Characterization was conducted using XRD, TEM, XRF, FTIR and VSM. The result shows that the $Zn_{(1-x)}Mn_xO$ ($0.00{\leq}x{\leq}0.06$) nanoparticles have the wurtzite phase with a hexagonal structure and particle sizes ranging from 17.48 to 118.83 nm. In a qualitative analysis of XRF, the peaks that confirm the existence of the manganese element in Mn-doped ZnO samples were observed. Meanwhile, FTIR test result shows that there are peaks at around $500cm^{-1}$ and $400cm^{-1}$ in the FTIR spectra for Mn doped ZnO samples which clearly reveal the existence of the (Zn, Mn)-O strain mode. The (Zn, Mn)-O absorption peak positions have shifted to a lower wave number with increasing Mn doping content. The peak intensity is also lower if compared to that of the ZnO sample without doping. From the VSM test, it is shown that $Zn_{(1-x)}Mn_xO$ ($0.00{\leq}x{\leq}0.06$) nanoparticles are all paramagnetic having monotonically increased susceptibility as increasing Mn content.