• Title/Summary/Keyword: paramagnetic material

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Nondestructive Evaluation of 2-Dimensional Surface Crack in Ferromagnetic Metal and Paramagnetic Metal by ICFPD Technique (집중유도형 교류전위차법에 의한 강자성체 및 상자성체의 2차원 표면결함의 비파괴평가)

  • 김훈;장자철웅;정세희
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.19 no.5
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    • pp.1202-1210
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    • 1995
  • Aiming at nondestructive evaluation of defect with high accuracy and resolution, ICFPD(Induced Current Focusing Potential Drop) technique was newly developed. This technique can be applied for locating and sizing of defects in components with not only simple shape such as plain surface but also more complex shape and geometry such as curved surface and dissimilar joing. This paper describes the principle of ICFPD technique and also the results of 2-dimensional surface crack in ferromagnetic metal(A508 Cl. III steel) and paramagnetic metal (pure aluminum and stainless 304 steel) measured by this technique. Results are that surface defects in each specimen are detected with the difference of potential drop, and potential drops are distributed a similar shape for each metal and each depth. The normalized potential drop ( $V_{\delta}$2/$^{t}$ / $V_{{\delta} 2}$$^{-1}$) max. in the vicinity of defect is varied with the depth of defect. Therefore, ICFPD technique can be used for the evaluation of defect not only in ferromagnetic metal but also in paramagnetic steel..

A Study of Electron Paramagnetic Resonance of Sugar Irradiated X-ray (X-선에 조사된 설탕의 전자 상자성 공명 연구)

  • Ok, Chi-Il;Son, Phil-Kook;Heo, Kyoung-Chan;Shon, Jong-Gi;Lee, In;Kim, Jang-Whan
    • Journal of radiological science and technology
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    • v.23 no.2
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    • pp.39-42
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    • 2000
  • When ordinary sugar is exposed to ionizing radiation, a number of free radical are created in sugar, and Electron Paramagnetic Resonance (EPR) signal appears from the sugar because of the paramagnetic property of free radical. In this paper, EPR signal intensity has been measured in x-ray irradiated sugar for various absorbed doses, irradiated dose up to 50 Gy. The EPR intensity signals are increased as the x-ray irradiation increases. Also, the fading value decreased to about 3% in 30day after the irradiation. Therefore, the sugar is a useful material for emergency dosimeter as the free radical dosimetry with the EPR equipment.

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The Low-Radiation Dosimetry Application of "tris" Lyoluminescence using Electron Paramagnetic Resonance at Low Temperature

  • Son, Phil-Kook;Choi, Suk-Won;Kim, Sung-Soo;Gwag, Jin-Seog
    • Journal of Magnetics
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    • v.17 no.3
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    • pp.172-175
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    • 2012
  • We present a method for detecting very weak radiation by analyzing the inner structure of irradiated tris (lyoluminescence) materials using electron paramagnetic resonance (EPR) at low temperature. Organic materials have been looked into for use in emergency dosimetry of inhabitants around radiation accidents. However, this technology has never been applied to imperceptible radiation doses (< 0.5 Gy) because there is no proper method for detecting the change of inner structure of the subject bombed by very weak radiation at room temperature. Our results show that tris materials can be applied as a radiation detectors of very small radiation doses below 0.05 Gray, if EPR is used at low temperature (130 K ${\leq}$ T ${\leq}$ 270 K). The EPR signal intensity from the irradiated-tris sample had barely faded at all after 1 year.

Calculation on Electronic State of $MnO_2$ Oxide Semiconductor with other initial spin conditions by First Principle Molecular Orbital Method (제1원리 분자궤도계산법에 의한 초기 spin 조건에 따른 $MnO_2$ 반도체의 전자상태 변화 계산)

  • Lee, Dong-Yoon;Kim, Bong-Seo;Song, Jae-Sung;Kim, Hyun-Sik
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2003.11a
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    • pp.148-151
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    • 2003
  • The spin density of ${\beta}-MnO_2$ structure was theoretically investigated by $DV-X_{\alpha}$ (the discrete variation $X{\alpha}$) method, which is a sort of the first principle molecular orbital method using Hatre-Fock-Slater approximation. The used cluster model was $[Mn_{14}O_{56}]^{-52}$. The ${\beta}-MnO_2$ is a paramagnetic oxide semiconductor material having the energy band gap of 0.18 eV and an 3 loan-pair electrons in the 3d orbital of an cation. This material exhibits spin-only magnetism and has the magnetic ordering temperature of 94 K. Below this temperature its magnetism appears as antiferromagnetism. The calculations of electronic state showed that if the initial spin condition of input parameters changed, the magnetic state changed from paramagnetic to antiferromagnetic. When d orbital of all Mn atoms in cluster had same initial spin state as only up spin, paramagnetic spin density distribution appeared by the calculation. On the other way, d orbital had alternately changed spin state along special direction the resulted spin distribution showed antiferromagnetism.

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Loading Effect on ACPD of a Crack in Paramagnetic Material (균열을 가진 상자성체의 교류전위차에 미치는 하중의 영향)

  • Lee, Jeong-Hee
    • Journal of the Korean Society for Nondestructive Testing
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    • v.19 no.1
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    • pp.1-7
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    • 1999
  • In order to determine the mode I stress intensity factor ($K_I$) by means of the alternating current potential drop(ACPD) technique, the change in potential drop due to load for a paramagnetic material containing a two-dimensional surface crack was examined. The cause of the change in potential drop and the effects of the magnetic flux and the demagnetization on the change in potential drop were clarified by using the measuring systems with and without removing the magnetic flux from the circumference of the specimen. The change in potential drop was linearly decreased with increasing the tensile load and was caused by the change in conductivity near the crack tip. The reason of decreasing the change in potential drop with increasing the tensile load was that the increase of the conductivity near the crack tip due to the tensile load caused the decreases of the resistance and internal inductance of the specimen The relationship between the change in potential drop and the change in $K_I$ was not affected by demagnetization and was independent of the crack length.

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NDT of a Nickel Coated Inconel Specimen Using by the Complex Induced Current - Magnetic Flux Leakage Method and Linearly Integrated Hall Sensor Array (복합 유도전류-누설자속법과 고밀도 홀센서배열에 의한 니켈 코팅 인코넬 시험편의 비파괴검사)

  • Jun, Jong-Woo;Lee, Jin-Yi;Park, Duk-Keun
    • Journal of the Korean Society for Nondestructive Testing
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    • v.27 no.5
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    • pp.375-382
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    • 2007
  • Nondestructive testing (NDT) by using the electromagnetic methods are useful for detecting cracks on the surface and subsurface of the metal. However, when the material contains both ferromagnetic and paramagnetic materials, it is difficult for NDT to detect and analyze cracks using this method. In addition the existence of a partial ferromagnetic material can be incorrectly characterized as a crack in the several cases. On the other hand a large crack has sometimes been misunderstood as a partially magnetized region. Inconel 600 is an important material in atomic energy plant. A nickel film is coated when a crack a appears on an Inconel substrate. Cracks are difficult to detect on the combined material of an Inconel substrate with a nickel film, which are paramagnetic and ferromagnetic material respectively. In this paper, a scan type magnetic camera, which uses a complex induced current-magnetic flux leakage (CIC-MFL) method as a magnetic source and a linearly integrated Hall sensor array (LIHaS) on a wafer as the magnetic sensors, was examined for its ability to detect cracks on the combined material. The evaluation probability of a crack is discussed. In addition the detection probability of the minimum depth was reported.

The Evaluation of Surface Crack in Paramagnetic Material by FEF Technique (FEF 탐상법을 이용한 상자성체 표면결함 평가)

  • Kim, Hoon
    • Journal of the Korean Society for Nondestructive Testing
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    • v.24 no.5
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    • pp.532-537
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    • 2004
  • FEF(Focused Electromagnetic Field) technique was newly developed that is based on the induction principle exciting electromagnetic field. The technique consists of an induction wire and a sensor for detecting electromagnetic field, and is applied in a non-contact mode. In this study, the technique was applied to the evaluation of EDM slits in some conductive materials - aluminum alloy, stainless steel and Inconel alloy. The voltage in the non-defect region is depended upon the measurement lift-off. The voltage signals on defects are measured with peak values, and the peak values changed with the depth of defects. The voltage distributions for all conductive materials are the same trend.

Localized Induction-Heating Method by the Use of Selective Mold Material (재료의 선택적 사용에 의한 금형의 국부적 유도가열기법)

  • Park, Keun;Do, Bum-Suk;Park, Jung-Min;Lee, Sang-Ik
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2009.05a
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    • pp.168-171
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    • 2009
  • High-frequency induction is an efficient way to heat mold surface by electromagnetic induction in a non-contact procedure. Though the induction heating has an advantage in terms of its rapid-heating capacity on the mold surface, it still has a restriction on mold temperature control due to geometric restriction of an induction coil according to the mold shape. It has been recently applied to the injection molding of thin-walled parts or micro/nano structures. For localized induction heating, an injection mold composed of ferromagnetic material and paramagnetic material is used. The electromagnetic induction concentrates on the ferromagnetic material, from which we can selectively heat for the local mold elements. The present study proposed a localized induction heating method by means of selective use of mold material. The feasibility of the proposed heating method is investigated through the comparison of experimental observations according to the mold material.

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Paramagnetic Zn(1-x)MnxO (0.00≤x≤0.06) Nanoparticles Prepared by The Coprecipitation Method

  • Harsono, Heru;Wardana, I Nyoman Gede;Sonief, Achmad As'ad;Darminto, Darminto
    • Transactions on Electrical and Electronic Materials
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    • v.18 no.1
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    • pp.46-50
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    • 2017
  • The Zn1-xMnxO ($0.00{\leq}x{\leq}0.06$) samples have been synthesized in the form of powder by the coprecipitation method at low temperature using $Zn(CH_3COO)_2$. $2H_2O$ and $Mn(CH_3COO)_2$. $4H_2O$ powders, as well as HCl and $NH_4OH$ solutions as starting materials. Characterization was conducted using XRD, TEM, XRF, FTIR and VSM. The result shows that the $Zn_{(1-x)}Mn_xO$ ($0.00{\leq}x{\leq}0.06$) nanoparticles have the wurtzite phase with a hexagonal structure and particle sizes ranging from 17.48 to 118.83 nm. In a qualitative analysis of XRF, the peaks that confirm the existence of the manganese element in Mn-doped ZnO samples were observed. Meanwhile, FTIR test result shows that there are peaks at around $500cm^{-1}$ and $400cm^{-1}$ in the FTIR spectra for Mn doped ZnO samples which clearly reveal the existence of the (Zn, Mn)-O strain mode. The (Zn, Mn)-O absorption peak positions have shifted to a lower wave number with increasing Mn doping content. The peak intensity is also lower if compared to that of the ZnO sample without doping. From the VSM test, it is shown that $Zn_{(1-x)}Mn_xO$ ($0.00{\leq}x{\leq}0.06$) nanoparticles are all paramagnetic having monotonically increased susceptibility as increasing Mn content.