• 제목/요약/키워드: neutron diffraction

검색결과 125건 처리시간 0.033초

Residual Stress Measurement on T-type Welded Specimen by Neutron Diffraction

  • Jang, D.Y.;Park, M.J.;Choi, H.D.;Kim, J.P.
    • International Journal of Korean Welding Society
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    • 제1권2호
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    • pp.45-50
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    • 2001
  • This paper presents application of neutron diffraction technique to the measurement of residual stresses in the T-type 20 m thick welded stainless steel plates(100$\times$50 $mm^2$ and 50$\times$50 $mm^2$). The High Resolution Powder Diffractormeter of the Korea Atomic Research Institute was utilized in the measurement. The power of nuclear reactor was 24 MWt and the measured reflection in the 220 plane (2$\theta$)was $92.66^{\circ}$. Poisson ratio of 0.265 and elastic constant of 211 GPa were applied to the calculation of stresses and strains. Three directional components such as normal, transverse, and longitudinal stresses were measured. The results showed that three components were tensile and became compressive along the y axis in the zone away from the welded center. The compressive stresses became tensile in the zone away from the center line of x axis. This may be due to the balance effect caused by the net stress to keep the specimen shape flat.

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Determination of Non-stoichiometry of Tubular Titanium Carbide Formed by Self-Propagating High Temperature Synthesis

  • Choi, Y.;Cho, N.I.
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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    • pp.782-783
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    • 2006
  • Titinium carbide $(TiC_x)$ was produced by self-propagating high temperature synthesis (SHS) method. The morphology and non-stoichiometric number of the SHS product were observed by scanning electron microscopy and neutron diffractometry, respectively. Tubular titanium carbide with hole inside was formed with different non-stoichiometric number (x), which value increased with combustion temperature.

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중성자회절법을 이용한 이트리아 저코니아의 결정구조 연구 (Neutron Diffraction Study on the Crystal Structure of Yttria-Stabilized Zirconium Oxide)

  • Jin-Ho Lee;Chang-Hee Lee;Won-Sa Kim
    • 한국광물학회지
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    • 제13권3호
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    • pp.164-170
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    • 2000
  • 중성자 단결정 및 분말회절실험을 이용하여 이트리아를 첨가한 저코니아 (yttria-stabilized airconia, Zr0.73Y0.27O1.87) 결정의 구조 분석을 수행하였다 시료는 입방정계로써, 공간군 Fm/equation omitted/ a=5.155(2)$\AA$, V=136.99(5), Z=4로 결정화되었고, 중성자 단결정 회절실험의 결과로 얻어진 70개의 브라그 회절반점을 이용한 최종신뢰도 R(F) 및 $\omega$R(I) 값은 각각 0.0576, 0.1057 이었다. Zr과 Y 원자 들은 이상적인 형석 (CaF2) 구조의 cation 위치에 불규칙하게 배열되어 있었으며, 산소 원자들의 대부분 (95%)은 (1/4,1/4,1/4) 위치에서 <110> 방향으로 $\Delta$/a~0.033의 크기만큼 이동하였고, 나머지 산소 원자들은 <100> 방향으로 $\Delta$/a~0.033의 변위가 존재하였다. Rietveld 분석법을 이용한 중성자 분말회절실험의 결과는 단결정 회절실험에서 보여주었던 결정학적 정보와 모든 면에서 잘 일치하고 있었으며, 정방정계의 구조에서 기인되는 몇 개의 불순상의 존재가 최종 분석된 분말 회절상에서 확인되었다.

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Fabrication of Prototype vuv Spectrometer & Liquid Target System Containing Hydrogen

  • 이윤만;김재훈;김진곤;안병남
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2012년도 제42회 동계 정기 학술대회 초록집
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    • pp.586-586
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    • 2012
  • The vuv spectrometer for ITER main plasma measurement is designed as a five-channel spectral system. To develop and verify the design, a two-channel prototype system was fabricated with No. 3 (14.4-31.8 nm) and No. 4 (29.0-60.0 nm) among the five channels. For test of the prototype system, a hollow cathode lamp is used as a light source. The system is composed of a collimating mirror to collect the light from source to slit, and two holographic diffraction gratings with toroidal geometry to diffract and also to collimate the light from the common slit to detectors. The overall system performance was verified by comparing the measured spectral resolutions with the calculated spectral resolutions. And we also have developed liquid jet target system. This study is about a neutron generator, which is designed to overcome many of the limitations of traditional beam-target neutron generators by utilizing a liquid target. One of the most critical aspects of the beam-target neutron generator is the target integrity under the beam exposure. A liquid target can be a good solution to overcome damage to the target such as target erosion and depletion of hydrogen isotopes in the active layer, especially for the ones operating at high neutron fluxes and maintained relatively thin with no need for water cooling. In this study, liquid target containing hydrogen has been developed and tested.

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