• 한국식품영양학회지
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• 제11권5호
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• pp.506-512
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• 1998

In order to replance systhetic colors by natural colors as food additive, properties of Gardenia yellow color and Gardenia blue color were compared with Food yellow No. 4 and Food blue No. 1. Color differeance between Food yellow No. 4 and Gardenia yellow color was 7.55. Thermal stability of Food yellow No. 4 was above 99%. On the other hand, in case of Gardenia yellow color, showed adove 90% of residual color units in 8$0^{\circ}C$$\times$30min and 10$0^{\circ}C$$\times$30min at pH 7.0 but 75% in 121$^{\circ}C$$\times$15min. Difference of light stability between Food yellow No. 4 and gardenia yellow color was about 18%. Addition of ascorbic acid was increased about 6% in light stability. Color difference between Food blue No. 2 and Gardenia blue color was 107. Thermal stability of Food blue No. 2 was above 99%. But Gardenia blue color showed 92% of residual color units in 8$0^{\circ}C$$\times$30min and 10$0^{\circ}C$$\times$30min at pH 7.0 but 90% in 121$^{\circ}C$$\times$15min. Difference of light stability between Food blue No. 4 and Gardenia blue color was about 8%. Addition of -tocopherol was increased about 4% in light stability of Gardenia blue color.

• Molecular & Cellular Toxicology
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• 제5권3호
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• pp.257-264
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• 2009

Gardenia yellow, extracted from gardenia fruit, has been widely used as a coloring agent for foods, and thus, safety of its usage is of prime importance. In the current study, short-term genotoxicity assays were conducted to evaluate the potential genotoxic effects of gardenia yellow. The gardenia yellow used was found to contain 0.057 mg/g of genipin, a known biologically active compound of the gardenia fruit extract. Ames test did not reveal any positive results. No clastogenicity was detected by a chromosomal aberration test, even on evaluation at the highest feasible concentration of gardenia yellow. Gardenia yellow was also shown to be non-genotoxic using an in vitro comet assay and a micronucleus test with L5178Y cells, although a marginal increase in DNA damage and micronuclei frequency was reported in the respective assays. Additionally, in vivo micronucleus test results clearly demonstrated that oral administration of gardenia yellow did not induce micronuclei formation in the bone marrow cells of male ICR mice. Taken together, our results indicate that gardenia yellow is not mutagenic to bacterial cells, and that it does not cause chromosomal damage in mammalian cells, either in vitro or in vivo.

• Journal of the Korean Wood Science and Technology
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• 제48권2호
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• pp.154-165
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• 2020

To assign the functionality of the regenerated fiber from waste MDF(wMDF) made of pitch pine, we examined the dyeing characteristics of natural dyes, sappan wood as a polychromatic natural red series, monochromatic gardenia as a yellow series, and indigo blue series. For nonemordanting dye, the colors of regenerated fiber dyed by sappan wood and gardenia were reddish yellow (YR) and yellow (Y) series, respectively, and dyeing conditions were appropriate a 30 ~ 50 g/L of dyeing materials at 60 ℃ for 60minutes of dyeing time. We obtained regenerated woody dyed fibers (Re-WDF), YR to the red (R) series by premordanting with Al and Cu mordant for sappan wood and the purplish red (RP) series by Fe premordanting. In the case of gardenia, only Y series colors were developed in nonemordanting dye or all three mordants. Indigo dye produced Re-WDF with greenish yellow (GY) tone at 1%, green (G) tone at 3%, and blue (B) tone at 5% concentration or more. Re-WDF with indigo showed the best light fastness followed by sappan wood and gardenia. In particular, the light fastness of Re-WDF with gardenia was very poor. The light fastness was somewhat improved by premordanting(Fe>Cu>Al) both sappan wood and gardenia dyes.

• 한국식품영양학회지
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• 제11권1호
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• pp.68-71
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• 1998

현재 사용중인 합성색소 중에서 사용빈도가 가장 높은 합성색소 중의 하나인 황색 4호의 대체용 천연색소를 치자에서 추출하였으며 추출조건은 추출온도 7$0^{\circ}C$, 추출시간 48시간, 추출 pH 7.0 및 기질농도는 10%였으며 이때의 추출수율은 61%였다. 추출한 조색소를 정제하기 위하여 활성백토를 사용하여 정제를 실시하였으며, 조색소액에서 배당체 성분과 색소성분을 각각 단일 peak로 분리하였다. 조색소액을 정제한 후 정제도는 약 27배 증가하였고, 수율은 96%로 높게 나타났다.

• 한국의류산업학회지
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• 제4권2호
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• pp.192-197
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• 2002

On the whole the various medium colors were developed by repeat dyeing with different colorants after dyeing with one colorant in case of natural dyeing. In this study, however in order to obtain various colors on silk fabrics with natural dyes, pre-mordanting and combination dyeing were carried out. Metal compounds containing alum, copper and iron were used for pre-mordants. Gardenia and Sappan wood were used as colorants for combination dyeing. In combination dyeing of Gardenia and Sappan wood, these two natural colorants showed good miscibility in dye bath. The various colors were obtained according to various metal compounds for pre-mordants and various mixing portion of Gardenia and Sappan wood.

• 복식문화연구
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• 제10권4호
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• pp.433-440
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• 2002

Natural gardenia and Japanese pagoda tree have been known as them of the most widely used yellow vegetable dyes. Cotton and silk fabrics(KS K 0905) were chosen as specimens. Those were dyed with natural gardenia and Japanese pagoda tree. The conditions of dyeing were varied according to the kinds of mordants, using mordants or not and the concentrations of the natural dyes. Sn, Al, Fe and Cu were chosen for the mordants. 5%(owf), 10%(owf), 15%(owf) and 20%(owf) were used as for the concentration of the natural dyes. The color differences were measured by the Spectrometer(UV-VIS-NIR) before and after dyeing. The results are as follows: 1. Deeper colors were proportionately shown up to the concentration of the natural dye. 2. Silk was shown the higher dye affinity than the cotton at the same concentration of the dye. 3. The color difference between the Sn-mordanted specimens and the Al-mordanted specimens were significant. When the concentration of the dye increased, the colors got darker, specially in b* value. 4. The color difference between the Fe-mordanted specimens and the Cu-mordanted specimens were significant in L* value and b* value. 5. The deeper or lighter yellow were controllable under the concentration of the natural dye and the mordants. 6. The most effective and the economic concentration of the natural dye was 10% owf through the experiments.

• 한국의류산업학회지
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• 제5권1호
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• pp.82-88
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• 2003

This study was carried out to investigate combination dyeing of the cationized cotton with natural colorants extracted from Gardenia and Sappan wood extract using methanol. To improve dyeing properties of cotton with natural dye, cotton fabric was preheated with cationizing agent containing chlorohydrine group in aqueous solution of sodium hydroxide. On the whole the various medium colors were developed by repeat dyeing with different colorants after dyeing with one colorant in case of natural dyeing, In this study, however in order to obtain various colors on cationized cotton fabrics with natural dyes, pre-mordanting and combination dyeing were carried out. The various colors were obtained according to various metal compounds for pre-mordants and various mixing portion of Gardenia and Sappan wood. Metal compounds containing alum, copper and iron were used for pre-mordants.

• 한국의류학회지
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• 제29권6호
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• pp.868-876
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• 2005

Silk fabrics were dyed with yellow natural materials. Gardenia, turmeric, amur cork tree, safflower, Japanese pagoda tree, and onion were used as natural materials. Color image of natural dyed silk fabrics was classified by 4 factors(Cheerfulness, Comfortness, Pastrol, Revealation). Cheerfulness factor affected significantly with color image. Amur cork tree or turmeric dyed fabrics were shown as light and cute, safflower or gardenia dyed fabric shown as comfort, and onion dyed fabrics shown as mature and simple. Color image with specialty was significant difference in Preference and Revelation factor. Preference was appeared as amur cork tree>turmeric>gardenia>safflower>Japanese pagoda tree>onion.

• 한국의류산업학회지
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• 제6권6호
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• pp.778-784
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• 2004

The natural dyeing of silk fabric with natural gardenia blue powder was investigated. The sum of K/S values was increased with increasing the amount of gardenia powder up to 20%,(o.w.b.). The proper time, temperature and pH for the dyeing of silk fabric with gardenia blue powder were 60~80 minutes, $80^{\circ}C$ and pH 4, respectively. The B and BG colors were obtained according to various mordanting methods, mordants and mordant concentrations. The various colorfastness were not improved by mordanting. The colorfastness to light was poor, but the colorfastness to dry cleaning and washing were good.

• 펄프종이기술
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• 제43권1호
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• pp.1-10
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• 2011

To investigate the combination dyeing properties of natural dyes, the combination dyeing using gallnut,-Al, Cu, Fe-sappan wood, and gallnut-Al, Cu, Fe-gardenia was performed on bast fiber of mulberry, cotton, silk, and their K/S values, colors, and sunlight fastness were measured. The gallnut-Al, Cu, Fe-gardenia dyeing showed the highest K/S values when the dyeing concentration of gallnut is 3%. It tended to show the higher K/S values than gallnut-Al, Cu, Fe-sappan wood. The silk showed the highest values of in K/S, and then followed by cotton, and bast fiber of mulberry. The mordants developed different colors on the bast fiber and the cotton treated with gallnut-Al, Cu, Fe-sappan wood. However, the silk showed a series of YR, showing no effect of the mordants on the development of color. The combination dyeing of gallnut-Al, Cu, Fe-gardenia showed a series of Y. The results showed that sappan wood could develop various colors but gardenia could develop a series of Y. No distinct improvement on sunlight fastness of the combination dyeing was observed.