• Proceedings of the Korean Society of Precision Engineering Conference
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• 2005.10a
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• pp.100-104
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• 2005

The injection molding is very effective process for various plastic products due to its high productivity. It is also good fur precise products like optical parts. Various thermoplastic materials are also available with this injection molding process. In recent, however, as the overall size of the product increases and micro or nano scale of patterns are applied to the products, we now have some problems such as low fidelity of the replication of the pattern, high molding pressure, or warpage from the in-mold stress. Injection/compression molding is studied to overcome those problems in molding large thin plate with micro pattern array on its surface. An injection compression mold is designed to 3 pieces mold for side gate. We install 4 pressure transducers and 9 thermocouples to measure the melt pressure and surface temperature in the cavity during the process. As a result, the maximum molding pressure for injection compression molding is reduced to 1/3 compared to injection molding and the uniformity of the pressure in the cavity is enhanced by about 15%.

• Advances in nano research
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• v.10 no.2
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• pp.101-114
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• 2021

An analytical investigation has been performed on the mechanical performance of waves propagated in a Single-Layered Graphene Sheet (SLGS) when an In-plane Varying Bending (IVB) load is interacted. It has been supposed that the Graphene Sheet (GS) is located on an elastic medium. Employing a two-parameter elastic foundation, the effects of elastic substrate on the GS behavior are modeled. Besides, the kinematic equations are derived by the means of a trigonometric two-variable refined plate theory. Moreover, in order to indicate the size-dependency of the SLGS, a Nonlocal Strain Gradient Theory (NSGT) was considered. The nonlocal governing differential equations are achieved in the framework of Hamilton's Principle (HP). Also, an analytical approach was used to detect the unknowns of the final eigenvalue equation. Finally, the effects of each parameters using some dispersion charts were determined.

• Advances in nano research
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• v.17 no.3
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• pp.257-274
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• 2024

This work aims to study and analyse the dynamic size dependent behvior of functionally graded carbon nanotubes (FGCNTs) nanoplates embedded in elastic media and subjected to moving point load. The non-classical effect is incorporated into the governing equations using the nonlocal strain gradient theory (NSGT). Four different reinforcement configurations of the carbon nanotubes (CNTs) are considered to show the effect of reinforcement configuration on the dynamic behvior of the FGCNTs nanoplates. The material characteristics of the functionally graded materials are assumed to be continuously distributed throughout the thickness direction according to the power law. The Hamiltonian principle is exploited to derive the dynamic governing equations of motion and the associated boundary conditions in the framework of the first order shear deformation plate theory. The Navier analytical approach is adopted to solve the governing equations of motion. The obtained solution is checked by comparing the obtained results with the available results in the literature and the comparison shows good agreement. Numerical results are obtained and discussed. Obtained results showed the significant impact of the elastic foundation parameters, the non-classical material parameters, the CNT configurations, and the volume fractions on the free and forced vibration behaviors of the FGCNT nanoplate embedded in two parameters elastic foundation and subjected to moving load.

• Journal of Environmental Health Sciences
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• v.29 no.1
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• pp.51-61
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• 2003

Pollution purification using titanium dioxide (TiO$_2$) photocatalyst has attracted a great deal of attention with increasing number of relent environmental problems. Currently, the application of TiO$_2$ photocatalyst has been focused on purification and treatment of waste water. However. the use of conventional TiO$_2$ powder photocatalyst results in disadvantage of stirring during the reaction and of separation after the reaction. And the usage of artificial UV lamp has made the cost of photocatalyst treatment system high. Consequently, we herein studied the pilot-scale design to aid in optimization of the energy-saving process for more through development and reactor design by solar light/UV lamp/ TiO$_2$system. In this study, we manufactured the TiO$_2$sol by sol-gel method. According to analysis by XRD, SEM and TEM, characterization of TiO$_2$ sol were nano-size (5-6 nm) and anatase type. Inorganic binder (SiO$_2$) was added to TiO$_2$ lot to be coated for support strongly, and support of ceramic bead was used to lower separation rate that of glass bead The influences were studied of various experimental parameters such as TiO$_2$ quantity, pH, flow rate. additives, pollutants concentration, climate condition and reflection plate by means of reaction time of the main chararteristics of the obtained materials. In water treatment system, variable realtor as solar light/ or UV lamp according to climate condition such as sunny and cloudy days treated the phenol and E-coli(Escherichia coli) effectively.

• Advances in nano research
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• v.10 no.5
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• pp.449-460
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• 2021

Flexoelectricity is an interesting materials' property that is more touchable in small scales. This property beside the sandwich structures placed in the center of scientists' attention due to their extraordinary effects on the mechanical properties. Furthermore, in the passage of decades, more elaborated sandwich structures took into consideration results from using honeycomb core. This kind of structure, inspiring from honeycomb core, provides more stiffness to weight ratio, which plays a crucial role in different industries. In this paper, based on the Love-Kirchhoff's hypothesis, Hamilton's principle, modified couple stress theory and Fourier series analytical method, equations of motion for a sandwich plate containing a honeycomb core integrated by two face-sheets have derived and solved analytically. The equations of both face sheets have derived by flexoelectricity consideration. Moreover, it should be noticed that the whole structure rests on the visco-Pasternak foundation. Conducting current research provided an acceptable and throughout study based on flexoelectricity to address the effect of materials' characteristics, length-scale parameter, aspect, and thickness ratios and boundary conditions on the natural frequency of honeycomb sandwich plates. Also, based on the presented figures and tables, there is a close agreement between previous studies and recent work. Due to the high ratio of strength to weight, current model analyzing is capable of taking into account for different vehicles' manufacturing in a high range of industries.

• Journal of the Microelectronics and Packaging Society
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• v.30 no.2
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• pp.65-70
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• 2023

Nanoimprint lithography (NIL) has attracted much attention due to its process simplicity, excellent patternability, process scalability, high productivity, and low processing cost for pattern formation. However, the pattern size that can be implemented on metal materials through conventional NIL technologies is generally limited to the micro level. Here, we introduce a novel hard imprint lithography method, extreme-pressure imprint lithography (EPIL), for the direct nano-to-microscale pattern formation on the surfaces of metal substrates with various thicknesses. The EPIL process allows reliable nanoscopic patterning on diverse surfaces, such as polymers, metals, and ceramics, without the use of ultraviolet (UV) light, laser, imprint resist, or electrical pulse. Micro/nano molds fabricated by laser micromachining and conventional photolithography are utilized for the nanopatterning of Al substrates through precise plastic deformation by applying high load or pressure at room temperature. We demonstrate micro/nanoscale pattern formation on the Al substrates with various thicknesses from 20 ㎛ to 100 mm. Moreover, we also show how to obtain controllable pattern structures on the surface of metallic materials via the versatile EPIL technique. We expect that this imprint lithography-based new approach will be applied to other emerging nanofabrication methods for various device applications with complex geometries on the surface of metallic materials.

• Bulletin of the Korean Chemical Society
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• v.18 no.8
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• pp.831-840
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• 1997

Core/shell structured composite metal oxides of Fe2O3/MgO were prepared by thermal decomposition of Fe(acac)3 adsorbed on the surface of MgO cores. The morphology of the composites conformed to that of the MgO used as the cores. Broad powder X-ray diffraction peaks shifted toward larger d, large BET surface area (∼350 m2/g), and the size of crystalline domains in nano range (4 nm), all corroborate to the nanocrystallinity of the Fe2O3/MgO composite which was prepared by using nanocrystalline MgO as the core. By use of microcrystalline MgO as the core, microcrystalline Fe2O3/MgO composite was prepared, and it had small BET surface area of less than 35 m2/g. AFM measurements on nanocrystalline Fe2O3/MgO showed a collection of spherical aggregates (∼80 nm dia) with a very rough surface. On the contrary, microcrystalline Fe2O3/MgO was a collection of plate-like flat crystallites with a smooth surface. The nitrogen adsorption-desorption behavior indicated that microcrystalline Fe2O3/MgO was nonporous, whereas nanocrystalline Fe2O3/MgO was mesoporous. Bimodal distribution of the pore size became unimodal as the layer of Fe2O3 was applied to nanocrystalline MgO. The macropores in a wide distribution which the nanocrystalline MgO had were absent in the nanocrystalline Fe2O3/MgO. The decomposition of CCl4 was largily enhanced by the overlayer of Fe2O3 on nanocrystalline MgO making the reaction between nanocrystalline Fe2O3/MgO and CCl4 be nearly stoichiometric. The reaction products were environmentally benign MgCl2 and CO2. Such an enhancement was not attainable with the microcrystalline samples. Even for the nanocrystalline MgO, the enhancement was not attained, if not with the Fe2O3 layer. Without the layer of Fe2O3, it was observed that the nanocrystalline domain of the MgO transformed into microcrystalline one as the decomposition of CCl4 proceeded on its surface. It appeared that the layer of Fe2O3 on the particles of nanocrystalline Fe2O3/MgO blocked the transformation of the nanocrystalline domain into microcrystalline one. Therefore, in order to attain stoichiometric reaction between CCl4 and Fe2O3/MgO core/shell structured composite metal oxide, the morphology of the core MgO has to be nanocrystalline, and also the nanocrystalline domains has to be sustained until the core was exhausted into MgCl2.

• Korean Chemical Engineering Research
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• v.48 no.1
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• pp.75-79
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• 2010

The precursor powders with thin wall structure were prepared by spray pyrolysis from the spray solution with ethylenediaminetetraacetic acid, citric acid and $NH_4Cl$ flux. The $BaMgAl_{10}O_{17}:Eu$ phosphor powders formed from the spray solution without organic additives and flux material had sizes of $1{\sim}5{\mu}m$ and hollow structure with high thickness at post-treatment temperature of $1,200^{\circ}C$. However, $BaMgAl_{10}O_{17}:Eu$ phosphor powders formed from the spray solution with ethylenediaminetetraacetic acid, citric acid and $NH_4Cl$ flux had fine size and plate-like shape. The mean crystallite sizes of the phosphor powders with fine sizes were 23, 35, and 33 nm when the content of $NH_4Cl$ flux were 0, 6, 35 wt% of phosphor. The photoluminescence intensity of the phosphor powders formed from the spray solution with the optimum amount of $NH_4Cl$ flux as 35 wt% was 215% of that of the phosphor powders formed from the spray solution without flux material.