• Journal of the Korea Fashion and Costume Design Association
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• v.9 no.3
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• pp.47-57
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• 2007

This study focused on the properties natural dyeing and natural material and on the development of functional material for well-being in apparel industry. Comus officinalis Siebold et Zuccarini is used as natural dyeing material which had been reported that have curable effect for unbalanced immunity, geriatric diseases like urinary tract system, diabetes, hypertension, arthritis, tinnitus, hyperhidrosis and women's diseases like hypermenorrhea. And this material also has anti-cancer effect so that can restraint cancer cells. 3 kinds tester of cotton, wool and silk are dyed by boiled with each dye (flower, fruits, bark of tree) as first dyeing and dried in the shade. These testers are done by post-mordanting method. Aluminium Potassium(Alk(SO4)2), Cuprie Sulfate($CuSO4{\cdot}5H2O$), Stannous Chloride($SnCl2{\cdot}2H2O$), Ferrous Sulfate($FeCl2{\cdot}4H2O$), Titanium Sulfate 24% aqueous solution(Ti(SO4)2) are used as mordants. Dyeing results of Comus officinalis Siebold et Zuccarini flower and bark are shown as yellow color series. And dyeing result of fruits is pink color series. Silk shows the best dyeing property. As the point of view for dyeing property, Ti, Sn, Fe would be the properchoice for mordant. Following results are extracted in this study. Yellow color is resulted in dyeing with Cornus officinalis flower as non-mordanting condition. Yellowish red color is come from dyeing with Comus officinalis fruit as non-mordanting condition. Grayish yellow tone is resulted in dyeing with bark as non-mordanting condition. Orange tone color with Ti-mordanting, green tone color with Sn-mordanting and gray tone color with Fe-mordanting is resulted respectively. However light-fastness of Comus officinalis(flower, fruit, bark) is very low as 1 or 2 level in non-mordanting condition, Comus officinalis flower dyeing is turned out 3 or 4 level and fruit dyeing is 4 or 5 level, bark dyeing is 2 or 3 level with Ti-mordanting respectively. Eventually Comus officinalis fruit has the best light-colorfastness property among all of dyes. dry cleaning colorfastness of Cornus officinalis(flower, fruit, bark) is good as 4 or 5 level in Ti-mordanting condition, perspiration-colorfastness of Cornus officinalis(flower, fruit, bark) is good as 4 or 5 level in Ti-mordanting condition, With these results, this study could conclude that dye-ability, colorfastness problem is getting better after mordanting process and practical usage would be possible.

• Journal of the Korean Society of Costume
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• v.56 no.1 s.100
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• pp.143-149
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• 2006

For the purpose of standardization and practicability of natural dyeing, the mordanting and dyeing properties of Acorn Shell was studied. Appropriate extraction, dyeing and mordanting condition of Acorn Shell were determined, and the effect of mordanting method on dye uptake and color fastness of dyed fabric was investigated. The maximum absorbance of Acorn Shell solution was at 287.5nm and 294nm. The pH effect was stable in the color difference changes. The optimum temperature to extract Acorn Shell was during 1 hour in $60^{\circ}C$. The effective dyeing temperature and time of silk were $80{\sim}100^{\circ}C$, 1hour. The silk fabrics dyed with Acorn Shell appeared yellow-brown. K/S value of dyeing fabrics was increased by mordant treatment. K/S value of post-mordanting was higher than pre-mordanting. Mordanting treatment attected color change of the dyed silk. In the case of Acorn Shell light fastness of appeared more than 3-5grades by post-mordanting. Abrasion fastness of appeared more than 3-5grades. Perspiration fastness of appered more than $3{\sim}5grades$ by mordant treatment but Cu mordant treatment was $2-5{\sim}4grades$. Dry-cleaning Fastness appered more than 4 grades except Cu mordant treatment. These fastness improvement were generally effective for mordant treatment, specially Al, Sn, Cr.

• Journal of the Korean Society of Clothing and Textiles
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• v.22 no.8
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• pp.971-977
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• 1998

For the purpose of standardization and practicability of nautral dyeing, the mordanting and dyeing properties of Rhusjara ica was studied. Appropriate extraction, dyeing and mordanting condition of Rhusjara ica were determined, and the effect of mordanting method on dye uptake and color fastness of dyed fabric was investigated. The most absorbance of Rhusjara ica solution was 299 nm. The color of Rhusjara ica solution was affected by pH 8~9. The optimum temperature to extract Rhusjara ica was 6$0^{\circ}C$ and dyeing solution for 1 hour. Effective dyeing time to silk was 60min. Effective mordanting temperature was 80~10$0^{\circ}C$, and its time was 30 min. K/S value of dyeing fabrics was recoginazed by mordanting treatment, specially Fe, Al, Cu. K/S value of pre-mordanting was higher than post-mordanting. In the case of Rhusjara ica fastness was increased by mordanting treatment.

• Fashion & Textile Research Journal
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• v.20 no.2
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• pp.210-218
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• 2018

The natural dye product market is expanding due to the recent interest in environmentally friendly products. This study examines dyeing using natural Coptidis Rhizoma. Chitosan and Tannin was treated to improve dyeability of Coptidis Rhizoma after finding the proper dyeing condition. In addition, dyeing characteristics were compared according to mordant types along with the mordanting methods for dye fixing and color change. The results indicated that the optimum dyeing condition was to treat the concentration of 5% (o.w.b.) at $80^{\circ}C$ for 90 minutes. By the chitosan and tannin treatments, K/S value of cotton fabrics by 3 times and those of wool fabrics by 2 times increased and color depthing of dyed fabrics was achieved after 2 cycles repetition. To improve dyeability, iron mordanting was most effective; in addition, the K/S Value of pre-mordanting fabrics versus post-mordanting fabrics increased the most. The color of the surface was changed to reddish yellow when Sn, Cu mordanting, and to greenish blue when Fe mordanting. The lightfastness of dyeing fabric with mordanting was weak at 1-2 grades, but the washing fastness was good for 4 grades and the rubbing fastness and sweat fastness were as good as those of the 3-4 grades. As a result, this study could help improve the dyeability of expensive Coptidis Rhizoma.

• Journal of the Korean Society of Costume
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• v.36
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• pp.109-119
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• 1998

For the purpose of standardization and practicability of natural dyeing, the mordanting and dyeing properties of Caseaslpinia Sappan, L. and Brazilin were studied. Appropriate extraction, dyeing and mordanting condition of Caeaslpinia Sappan, L. were determined, and the effect of mordanting method on dye up-take adn color fastness of dyed fabric was investigated. The most absorbance of Caeaslpinia Sappan, L. solution was 445nm, Brazilin was 448nm. The color of bazilin solution was affected by pH 7~9. The optimum temperature to extract Caesalpinia Sappan, L. was 10$0^{\circ}C$ adn dyeing solution for 1 hour. In case mordants concentration, the most absorbance was 0.3%. In case mordanting test, the best and proper temperature to quantities of absorbed mordants in silk was 8$0^{\circ}C$ and the most quantities of absorbed mordants in silk was mordant treatment by Cu. Effective dyeing time to silk was 60min. Effective mordanting temperature was 8$0^{\circ}C$, and its time was 30min. K/S value of dyeing fabrics was recoginazed by mordanting treat-ment, specially Fe, Sn, Al, Cu. K/S value of pre-mordanting was higher than post-mordanting. After soaping treatment K/S value of pre- and post-mordanting silk was decreased and 0.1%(W/V) quantity of mordant was sufficient for treatment. In the case of Caeaslpinia Sappan, L. fastness was increased by mordanting treatment. Mordants and mordanting treatment method affected the amount of absorption and color change of dyed silk.

• Journal of the Korean Society of Costume
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• v.52 no.3
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• pp.19-27
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• 2002

This paper surveys the mordanting and dyeing properties of Sophora japonica L. Appropriate extraction, dyeing and mordanting condition of Sophora japonica L. were determined, and the effect of mordanting method on dye uptake and color fastness of dyed fabric was investigated. The maximum absorbance of Sophora japonica L. solution was 367.6mn, rutin solution was 365.6mn. The color of Sophora japonica L. solution was affected at pH 2 and pH 8~9. The optimum temperature to extract Sophora japonica L. was during 1 hour in 8$0^{\circ}C$. The effective dyeing temperature and time of silk were 10$0^{\circ}C$, 60min. K/S value of dyeing fabrics was increased by pre-mordanting treatment, especially Fe, Sn, Cr. In the case of Sophora japonica L. light fastness was increased by Fe mordanting. Perspiration fastness was better in acidic solution than that in alkaline solution. Fastness to rubbing and dry-cleaning were good in general.

• Journal of the Korean Society of Costume
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• v.55 no.8 s.99
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• pp.154-160
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• 2005

For the purpose of standardization and practicability of natural dyeing, the mordanting and dyeing properties of Puerariae Radix was studied. Appropriate extraction, dyeing and mordanting condition of Puerariae Radix were determined, and the effect of mordanting method on dye uptake and color fastness of dyed fabric was investigated. The maximum absorbance of Puerariae Radix solution was at 290nm and 301nm. The pH effect was stable in the color difference changes. The optimum temperature to extract Puerariae Radix was during 1 hour in loot. The effective dyeing temperature and time of silk were 80$\~$ 100$^{circ}C$, 1hour. The silk fabrics dyed with Puerariae Radix appeared yellow-brown. US value of dyeing fabrics was increased by Fe, and Cu mordant treatment. Mordanting treatment method affected color change of the dyed silk. In the case of Puerariae Radix light fastness of appeared more than 2-5 grades by mordant treatment. Perspiration fastness of appered more than 4 grades by Al, Sn, Cr mordant treatment. Fastness of abrasion and dry-cleaning appered more than 4-5 grades. These fastness improvement were generally effective for mordant treatment, specially Al, Sn, Cr.

• Journal of the Korean Home Economics Association
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• v.42 no.7
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• pp.63-72
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• 2004

This study discussed the dyeing of wool and cotton fabrics with Betel Palm Tree White woolen fabrics and cotton fabrics purchased from HATH (Korea Apparel Testing ＆ Research Institute) were used as experimental fabrics. Using dyeing powder extracted from dyeing material, various temperatures, dyeing times, and pH were used in the dyeing process. Al, Cr, Fe, Cu, and Sn were used as mordant and the absorption was compared with different mordanting methods. The optimum condition for pre-mordanting dyeing was dye concentration of 25% (o.w.f) and mordant concentration of 0.5$^{\circ}$∼1%. Woolen fabric showed an increase of absorption and the maximum absorption was achieved at weak acidity. According to the mordanting methods, woolen fabrics and cotton fabrics were treated with various mordanting agents, a mordant rate of 1:100, at 60$^{\circ}C$, for 30 minutes and dyed with a dyeing material concentration of 25% (o.w.f), at a rate of 1:100, at 60$^{\circ}C$ for 60 minutes. The best dyeing effect w3s achieved at the temperature of 60$^{\circ}C$ for cotton and 80$^{\circ}C$ for wool fabrics. The light fastness of cotton and wool fabrics was low and particularly the fastness to perspiration was decreased with Fe mordanting. I concluded that pre-mordanting method was better than post-mordanting method for cotton and woolen fabrics.

• Journal of Fashion Business
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• v.16 no.4
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• pp.100-106
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• 2012

This research was carried out to find the mordant effect of Chestnut's inner skin on the cow leather dyed by Turmeric powder. The best proper mordanting conditions were examined by changing mordant method, concentration, temperature, bath ratio, time, and repetition. Also dyeability and surface color changes were evaluated by various mordanting methods. The optimum mordanting conditions of chestnut's inner skin extract on the cow leather were pre mordant, 80%, $50^{\circ}C$, 50:1, 40minutes, 4 repetition. The K/S values as a mordant were higher in pre mordant than post mordanting condition. Although the ${\Delta}E$ was slightly higher in post mordant than pre mordant, it was too small to find any means. The surface colors of all dyed cow leathers were yellow. Among light, dry cleaning, and abrasion fastnesses, only light fastness was increased one degree, others were same degrees.

• Fibers and Polymers
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• v.7 no.3
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• pp.255-261
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• 2006

There is increasing interest in the many beneficial aspects of green tea to human such as anti-carcinogenic, anti-aggregant, anti-allergic, anti-bacterial, anti-mutagenic, and anti-oxidant activities. Besides these beneficial aspects, it has been reported that green tea ingredients, especially polyphenolic families (i.e., catechin), have some UV protection property both in vivo and in topical applications. In this study, green tea extract was used as a dyeing stock for cotton and the UV protection property of the dyed cotton fabric was examined. To increase the affinity of cotton fiber to the polyphenolic components in the green tea extract, a natural biopolymer, chitosan, was used as mordanting agent. The effects of chitosan concentration in mordanting on the dyeing characteristics and the UV protection property were examined. Chitosan mordanted green tea dyed cotton showed better dyeing characteristic and higher UV protection property compared with the unmordanted green tea dyed cotton. As the chitosan concentration in mordanting increased, the dyeing efficiency and the UV protection property also increased. Therefore, adapting chitosan mordanting in green tea dyeing can increase the UV protection property of cotton fabrics to some extent.