• 제목/요약/키워드: mini-SEM

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소형주사전자현미경용 전자공학계의 개발 (A Development of Electron Optics System of Mini-Sized SEM)

  • 박만진;김일해;김동환;장동영;한동철
    • 한국공작기계학회논문집
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    • 제16권5호
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    • pp.140-144
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    • 2007
  • As an electron scanning microscopes has traditionally required a considerably large room equipped with several service and pipe lines due to its inherent size. As an alternative, a small sized SEM, simply called a mini-SEM, is introduced even if the performance in terms of magnification and resolution is a little inferior to a classical thermal SEM. However, the size and fabrication cost is dramatically reduced, dedicating to opening a new market. The optical system in the mini-SEM is redesigned and specimen stage is quitely reduced and vertical axis is excluded. The design tools and calibration techniques to develope the mini-SEM are introduced and its performance is verified through numerical analysis experiments.

미니형 주사전자 현미경의 설계 및 제어 (Design and Control of Mini-Scanning Electron Microscope)

  • 박만진;김동환;김영대;장동영;한동철
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2007년도 춘계학술대회A
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    • pp.1271-1276
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    • 2007
  • The most powerful analytical equipment usually comes at the cost of having the highest demand for space. Where electron microscopes has traditionally required a room to themselves, not just for reasons of their size but because of ancillary demands for pipes and service. The simple optical microscopes, of course, can occupy the desk-top, but because their performance is limited by the wavelength of light, their powers of magnification and resolution are inferior to that of the electron microscope. Mini SEM will sit comfortably on a desk-top but offers magnification and resolution performances much closer to that of a standard SEM. This new technique extends the scope of SEM as a high-resolution microscope, relatively cheap and widely available imaging tool, for a wider variety of samples.

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Bone cutting capacity and osseointegration of surface-treated orthodontic mini-implants

  • Kim, Ho-Young;Kim, Sang-Cheol
    • 대한치과교정학회지
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    • 제46권6호
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    • pp.386-394
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    • 2016
  • Objective: The objective of the study was to evaluate the practicality and the validity of different surface treatments of self-drilling orthodontic mini-implants (OMIs) by comparing bone cutting capacity and osseointegration. Methods: Self-drilling OMIs were surface-treated in three ways: Acid etched (Etched), resorbable blasting media (RBM), partially resorbabla balsting media (Hybrid). We compared the bone cutting capacity by measuring insertion depths into artificial bone (polyurethane foam). To compare osseointegration, OMIs were placed in the tibia of 25 rabbits and the removal torque value was measured at 1, 2, 4, and 8 weeks after placement. The specimens were analyzed by optical microscopy, scanning electron microscopy (SEM), and energy dispersive X-ray spectroscopy (EDS). Results: The bone cutting capacity of the etched and hybrid group was lower than the machined (control) group, and was most inhibited in the RBM group (p < 0.05). At 4 weeks, the removal torque in the machined group was significantly decreased (p < 0.05), but was increased in the etched group (p < 0.05). In the hybrid group, the removal torque significantly increased at 2 weeks, and was the highest among all measured values at 8 weeks (p < 0.05). The infiltration of bone-like tissue surface was evaluated by SEM, and calcium and phosphorus were detected via EDS only in the hybrid group. Conclusions: Partial RBM surface treatment (hybrid type in this study) produced the most stable self-drilling OMIs, without a corresponding reduction in bone cutting capacity.

ZrN 및 TiN 코팅된 치과교정 용 미니나사의 표면특성과 전기화학적 거동 (Surface Characteristics and Electrochemical Behaviors of TiN and ZrN Coated Orthodontic Mini-screw)

  • 김신영;문영필;박근형;조호형;김원기;손미경;최한철
    • 한국표면공학회지
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    • 제41권5호
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    • pp.232-239
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    • 2008
  • The dental orthodontic mini-screw requires good mechanical properties and high corrosion resistance for implantation in the bone. The purpose of this study was to investigate the electrochemical characteristics of TiN and ZrN coated orthodontic mini-screws, mini-screws were used for experiment. Ion plating was carried out for mini-screw using Ti and Zr coating materials with nitrogen gas. Ion plated surface of each specimen w as o bserved with f ield emission scanning e lectron microscopy ( FE-SEM), e nergy dispersive x-ray spectroscopy (EDX), and electrochemical tester. The surface of TiN and ZrN coated mini-screw were more smooth than that of other kinds of non-coated mini-screw due to dercrease of machined defects. The corrosion current density of the TiN and ZrN coated mini-screw decreased compared to non-coated sample. The corrosion potential of TiN and ZrN coated mini-screw were higher than that of non-coated mini-screw in 0.9% NaCl solution. The pitting corrosion resistance increased in the order of ZrN coated, TiN coated and non-coated wire. Pitting potential of ZrN coated mini-screw was the highest in the other specimens.

COMPARATIVE ANALYSIS OF STRUCTURAL CHANGES IN U-MO DISPERSED FUEL OF FULL-SIZE FUEL ELEMENTS AND MINI-RODS IRRADIATED IN THE MIR REACTOR

  • Izhutov, Aleksey.L.;Iakovlev, Valeriy.V.;Novoselov, Andrey.E.;Starkov, Vladimir.A.;Sheldyakov, Aleksey.A.;Shishin, Valeriy.Yu.;Kosenkov, Vladimir.M.;Vatulin, Aleksandr.V.;Dobrikova, Irina.V.;Suprun, Vladimir.B.;Kulakov, Gennadiy.V.
    • Nuclear Engineering and Technology
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    • 제45권7호
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    • pp.859-870
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    • 2013
  • The paper summarizes the irradiation test and post-irradiation examination (PIE) data for the U-Mo low-enriched fuel that was irradiated in the MIR reactor under the RERTR Program. The PIE data were analyzed for both full-size fuel rods and mini-rods with atomized powder dispersed in Al matrix as well as with additions of 2%, 5% and 13% of silicon in the matrix and ZrN protective coating on the fuel particles. The full-size fuel rods were irradiated up to an average burnup of ${\sim}60%^{235}U$; the mini-rods were irradiated to an average burnup of ${\sim}85%^{235}U$. The presented data show a significant increase of the void fraction in the U-Mo alloy as the U-235 burnup rises from ~ 40% up to ~ 85%. The effect of irradiation test conditions and U-235 burnup were analyzed with regard to the formation of an interaction layer between the matrix and fuel particles as well as generation of porosity in the U-Mo alloy. Shown here are changes in distribution of U fission products as the U-235 burnup increases from ~ 40% up to ~ 85%.

Preparation of Silica Hollow Composite Particles

  • Lee, Dong Hoon;Lee, Chang Hyun
    • Bulletin of the Korean Chemical Society
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    • 제35권11호
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    • pp.3303-3306
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    • 2014
  • A facile and effective approach has been developed to prepare hybrid hollow microspheres, via consecutive processes of pickering mini-emulsion polymerization for core-shell formation, and calcination of the sacrificial core. The resulting hollow composite particles have mono-layered shells. The morphology and size characteristics of synthesized composite particles were investigated, using dynamic light scattering (DLS) and scanning electron microscopy (SEM) measurements.

안구 운동이 노인의 인지능력 변화에 미치는 융합적 분석 (Convergent Analysis of Old People Eye Movement Training on Change of Cognitive Ability)

  • 배세현;김경윤
    • 한국융합학회논문지
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    • 제9권5호
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    • pp.121-127
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    • 2018
  • 본 연구는 55명의 노인 대상자를 무작위로 급속안구운동(saccadic eye movement, SEM)군과 원활추종눈운동(smooth pursuit eye movement, SPEM) 두 군으로 구분하여 4주 동안 안구운동을 실시한 후 사건관련 전위(event-related potentials)중 P300의 전위값과 잠복기 그리고 MMSE-DS를 사용하여 안구운동이 인지능력에 미치는 영향을 알아보고자 하였다. 그 결과 SEM과 SPEM 군의 P300 전위값은 유의하게 상승하였으며, P300의 잠복기는 유의하게 짧아졌다. MMSE-DS 결과 두 군 모두 유의한 상승을 나타냈으며, 군간 비교 시 SEM군은 지남력, SPEM군은 주의력에서 유의한 차이를 나타내었다. 결론적으로 SEM과 SPEM은 노인의 인지능력을 향상 및 유지를 시킬 수 있으며 치매예방과 경도 치매에 대한 치료 도구로 사용될 수 있을 것으로 생각된다.

결합재와 혼화재 종류에 따른 콘크리트의 수화반응 특성 (Hydration Reaction Properties of Concrete With Binders and Admixtures)

  • 조일호;성찬용
    • 한국농공학회논문집
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    • 제50권2호
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    • pp.27-34
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    • 2008
  • Recently, owing to the development of industry and improvement of building techniques, concrete structures are becoming larger and higher. This study was performed to analyze hydration reation properties of concrete with binders and admixtures, such as OPC, low heat cement, belite rich cement, slag powder, lime powder and fly ash. To investigate effects of PC type superplasticizer on the hydration, experiments involving FT-IR, XRD, DSC, SEM were analyzed at the curing age 1day, 3days and 28days. The hydration reaction rate of OPC concrete slightly delayed at the curing age 1day, blast furnace slag powder and fly ash were more effective. BRC and LHC concretes can be used for concrete structures in winter season.

황사의 오염원분류포 개발을 위한 개별입자분석 (Individual Particle Analysis for Developing a Source Profile of Yellow Sands)

  • 강승우;김동술
    • 한국대기환경학회지
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    • 제16권6호
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    • pp.565-572
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    • 2000
  • To quantitatively estimate mass contribution of long-range transported yellow sand, their sources should be separated independently from various local soil sources having similar elemental compositions. While it is difficult to estimate total mass loadings of pure yellow sand by traditional bulk analysis, it can be clearly solved by an particle-by-particle analysis. To perform this study, two yellow sand samples and three local soil samples were collected by a mini-volume sampler. These samples were three analyzed using a scanning electron microscope(SEM) equipped with an energy dispersive x-ray analyser (EDX) was used to obtain basic chemical information of individual yellow san particles. A total of 19 elements in a single particle were measured to develop a source profile with newly created homogeneous particle classes (HPCs) as chemical variables. The present study showed that the yellow sand samples as well as three local soil samples were characterized with reasonably well created HPCs. Finally the mass fraction of each HPC in each sample was calculated and then compared each other.

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비글견에서 급속수술교정 치료 후 생물학적 효과에 대한 조직평가: 예비연구 (Histologic assessment of the biological effects after speedy surgical orthodontics in a beagle animal model: a preliminary study)

  • 김홍석;이영준;박영국;정규림;강윤구;추혜란;김성훈
    • 대한치과교정학회지
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    • 제41권5호
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    • pp.361-370
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    • 2011
  • Objective: Speedy surgical orthodontics (SSO), an innovative orthodontic treatment, involves the application of orthopedic forces against temporary skeletal anchorage devices following perisegmental corticotomy to induce movement of specific dental segments. Herein, we report the biological effects of SSO on the teeth and periodontal structures. Methods: Five beagle dogs were divided into 2 groups and their 6 maxillary incisors were retracted $en$ $masse$ by applying 500 g orthopedic force against a single palatal mini-plate. Retraction was performed without and with perisegmental corticotomy in groups I and II, respectively. All animals were killed on the 70th day, and their periodontal structures were processed for histologic analyses and scanning electronic microscopy (SEM). The linear distance between the third maxillary incisor and canine was used as a benchmark to quantify the retraction amount. Results: Retraction was markedly faster and retraction amount greater in group II than in Group I. Surprisingly, Group II did not show any root resorption despite extensive retraction, while Group I showed prominent root surface irregularities. Similarly, SEM showed multiple resorption lacunae in Group I, but not in Group II. Conclusions: SSO is an effective and favorable orthodontic approach for major en masse retraction of the maxillary anterior teeth.