• 대한기계학회논문집
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• 제16권10호
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• pp.1861-1868
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• 1992

본 연구에서는 발전소의 터빈 블레이드는 물방울에 의해서 부식이 발생한다는 사실은 널리 알려져 있다. 부식을 방지하기위해서 보통 12%-Cr 강으로 만들며 표면 을 고주파 유도경화법에 의해서 표면을 경화시킨다. 고주파유도 경화법은 경화층 깊 이가 마모 특성을 가장 좋게 하는 깊이보다 훨씬 깊게 경화되며, 열응력이 과대하게 생기고, 처리시간이 많이 걸리며, 표면경화 처리후 기계가공이 필요하다. 12%-Cr 강 의 레이저 표면경화를 연속파 3kw CO$_{2}$ 레이저로 실험하여 금속조직과 경도분포에 대해서 연구하여 레이저 표면경화 가능성을 고찰하였다.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2013년도 제44회 동계 정기학술대회 초록집
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• pp.94-94
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• 2013

The Cr-Zr-N films have much improved mechanical properties and very smooth surface roughness. However, in spite of their outstanding properties, the Cr-Zr-N coatings revealed their mechanical properties deteriorated severely with increasing Zr content at $500^{\circ}C$ ecause of very rapid oxidation. Recently oxynitride films have been widely studied due to their excellent unique mechanical properties and oxidation resistance. In this work, CrZr-O-N films with various O contents were synthesized by unbalanced magnetron sputtering with Cr-Zr segment targets (Cr:Zr volume ratios is 1：1) and all films were prepared in a nitrogen rich mixture of N2 and O2. Characteristics such as crystalline structure, hardness and chemical composition as a function of the O content were investigated by X-ray diffraction (XRD), field emission scanning electron microscope (FE-SEM), microhardness testing system and energy dispersive spectroscopy (EDS). Results showed that the thin films had dense and compact microstructure as O content in the films increases. The microstructure of the thin films consisted of mainly crystalline Cr (Zr)N phase and Cr2O3 phase. The maximum hardness and elastic modulus of the films was measured to be approximately 33.2 GPa and 280.6 GPa from the films with low content of O elements. Detailed experimental results will be presented.

• 열처리공학회지
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• 제16권6호
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• pp.329-334
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• 2003

Microstructure and mechanical properties of $(Ti_{1-x}Alx)N$ films, Produced by the the Ion Beam Sputtering(IBS) method, were studied by changing the Ti, Al contents. The compositions of films determined by RBS were $(Ti_{0.75}Al_{0.25})N$, $(Ti_{0.61}Al_{0.39})N$ and $(Ti_{0.5}Al_{0.5})N$, and XPS binding energies of Ti2P, A12p and N1s shifted to higher energies than those of pure Ti, Al and N, which indicated that nitrides were formed. XRD results indicated that the NaCl structure for $$x{\leq_-}0.39$$ changed into amorphous structure at x=0.5. For films with $$x{\leq_-}0.39$$, the lattice parameter decreased in proportion to the Al content. Nanoindentation hardness value were above HV=3300 at Al content up to x=0.39. However, the hardness of films with x=0.5 abruptly decreased to HV=1800, and this lower hardness values were attributed to different crystal structure. Critical load(Lc) in scratch test showed 23N at x=0.25, 22N at x=0.39 and 22N at x=0.5, which indicated that films with different Al contents showed similar adhesion behavior.

• 한국산학기술학회논문지
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• 제18권11호
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• pp.124-129
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• 2017

본 연구에서는 철도차량의 경량 차체 소재로 주로 사용되는 알루미늄 합금 (Al-6005-T6) 압출재에 대한 마찰교반접합 적용 연구를 수행하였다. 용접속도를 300 mm/min으로 고정시킨 채 회전 공구의 회전속도를 600, 900, 1200, 1600 rpm으로 변화시킬 때 미세구조 및 기계적 특성의 변화에 대해 평가하였다. 특히, 동일 소재에 대해 전통적인 용접방법인 MIG 용접된 시편과의 비교를 통해 마찰교반접합법의 철도차량 적용성에 대해 논하였다. MIG 용접방법과는 달리, 마찰교반접합부에는 미세기공이 발견되지 않았으며, 경도 측정 결과 공구의 회전속도가 빨라질수록 높아진 입열량에 따라 heat affected zone (HAZ)의 범위가 넓어지고 결정립 조대화에 따라 HAZ의 경도 또한 낮아지는 것을 확인하였다. 인장시험 결과 HAZ지역에서 파단이 발생하였으며, 본 연구에서 설정한 공구의 회전속도 범위에서는 nugget 부의 경도 변화는 발견되지 않았으나 rpm이 올라갈수록 인장강도와 항복강도가 떨어지는 경향을 보였으며 이는 경도 시험에서와 같이 HAZ지역의 결정립 크기의 증가로 인한 현상으로 판단된다.

• Korean Chemical Engineering Research
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• 제49권2호
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• pp.206-210
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• 2011

다양한 방식의 등통로각압축공정으로 생분해성 고분자인 폴리젖산수지 시편을 가공하여 각 공정 방식에 따른 시편들의 열 및 기계적 물성의 변화를 조사하였다. 각각 A, BC, C 세 가지의 시편 재 주입 방식과 1, 2, 4의 가공 횟수를 조합한 7개의 시편들을 제작하고, 각 시편의 녹는점, 열분해온도와 같은 열물성을 시차주사열량분석기와 열무게분석기를 사용하여 측정하였다. 시편의 응력변형의 변화를 경도 시험기를 사용하여 측정하고, 각 시편 절단면의 내부 미세구조를 주사전자현미경을 사용하여 관찰하였다. 관찰된 내부 미세구조는 경도시험결과를 설명하는데 정성적인 뒷받침이 되었다. 그 결과 PLA-P2A의 내부 미세 구조가 가장 치밀하고 촘촘히 겹쳐져 있음으로 인하여 내부 응력변형도 가장 많이 관찰되었다.

• 한국정밀공학회지
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• 제22권11호
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• pp.45-50
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• 2005

In this study, the casting/forging process was applied in manufacturing a low control arm, in order to prove that application of casting/forging process to Al6061 is likely to get the effect of light weight compared with existing steel products and to reduce the cost of materials. Firstly, In order to set up the optimum casting condition of the forging material, Al6061, casting experiments were carried out by controlling pouring temperature of the aluminum for casting, mold temperature, and pouring time. $700^{\circ}C$ pouring temperature, $300^{\circ}C$ mold temperature and 10-second pouring time were taken into account as the optimum casting conditions. With respect to a hot forging test, it is practiced on the basis of a temperature of materials, strain rate, and reduction rate so as to observe each microstructure and examine strain-stress curve simultaneously; examine tensile test and hardness test; eventually set up the optimum hot forging condition. A hot forging test, tensile test, hardness experiment, and microstructure observation were carried out on condition of $70\%$ reduction rate, $500^{\circ}C$ temperature of materials, and 1 strain rate. As a result of those experiments, 330MPa tensile strength, $16.4\%$ elongation, and 122.8Hv hardness were recorded. In oder to get a sound preform which has no unfitting cavity and less flash, two preforms were proposed on the basis of volume rate of the final product; the optimum volume rate of preform for the low control arm was $115\%$. In conclusion, it is confirmed that using the forging material rather than casting materials in casting/forging process is likely to get more superior mechanical properties. Compared with Al6061, performed by means of general forging, moreover, cast/forged Al6061 can not only stimulate productivity by reducing production processes, but cut down the cost of materials by reusing forging scraps.

• 한국재료학회지
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• 제9권8호
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• pp.775-781
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• 1999

균일하고 치밀한 미세구조를 갖는 Pd박막이$ PdCl_2$를 사용하는 전기도금방법으로 제조되었다. 본 연구에서는 도금온도와 전류밀도가 주요 공정변수로서 고려되었고 이에 따른 음극효율 및 제조된 Pd도금막의 결정성, 형상 및 경도 등의 특성이 측정되었고, 이들간의 상호관계성이 검토되었다. 연구결과에 따르면, $PdCl_2$를 사용하는 본 Pd전기도금 시스템에서는 5$0^{\circ}C$와 5mA/$\textrm{cm}^2$의 조건이 도금막의 형상으로 볼 때, 최적의 도금조건이라고 간주된다. 최적 조건에서 제조된 Pd도금막의 경도는 약 600kg/$\textrm{mm}^2$이었다. 변수 및 특성간의 관계성 검토 결과, Pd막의 경도는 미세구조에 의해 큰 영향을 받지만, 결정의 배향성과의 연관성은 작은 것으로 해석된다.

• 한국분말재료학회지
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• 제22권6호
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• pp.408-412
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• 2015

This study attempts to manufacture a Ni-Cr-Al-Y coating layer using a kinetic spray process and investigates the microstructure and physical properties of the manufactured layer. The Ni-22Cr-10Al-1Y (wt.%) composition powder is used, and it has a spherical shape with an average diameter of $23.7{\mu}m$. Cu plate is used as the substrate. Optical microscope, X-ray diffraction, scanning electron microscope and Vickers hardness test are carried out to characterize the macroscopic properties of the coating layer. Furthermore, the coating layer underwent vacuum heat treatment at temperatures of $400^{\circ}C$ and $600^{\circ}C$ for 1 hour to check the effect of heat treatment temperature on the properties. The manufactured coating layer is 1.5 mm thick, and featured identical phases to those found in the powder. The porosity of the coating layer is measured at 2.99%, and the hardness is obtained at $490.57H_v$. The layer shows reduced porosity as heat treatment temperature increased, and hardness is reduced at $400^{\circ}C$ but shows a slight increase at $600^{\circ}C$. Based on the findings described above, this study also discusses possible manufacturing methods for a Ni-Cr-Al-Y coating layer using the kinetic spray process.

• 한국표면공학회:학술대회논문집
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• 한국표면공학회 2018년도 춘계학술대회 논문집
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• pp.129-129
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• 2018

Hard coating application is effective way of cutting tool for hard-to-machine materials such as Inconel, Ti and composite materials focused on high-tech industries which are widely employed in aerospace, automobile and the medical device industry also Information Technology. In cutting tool for hard-to-machine materials, high hardness is one of necessary condition along with high temperature stability and wear resistance. In recent years, high-entropy alloys (HEAs) which consist of five or more principal elements having an equi-atomic percentage were reported by Yeh. The main features of novel HEAs reveal thermodynamically stable, high strength, corrosion resistance and wear resistance by four characteristic features called high entropy, sluggish diffusion, several-lattice distortion and cocktail effect. It can be possible to significantly extend the field of application such as cutting tool for difficult-to-machine materials in extreme conditions. Base on this understanding, surface coatings using HEAs more recently have been developed with considerable interest due to their useful properties such as high hardness and phase transformation stability of high temperature. In present study, the nanocomposite coating layers with high hardness on WC substrate are investigated using high entropy alloy target made a powder metallurgy. Among the many surface coating methods, reactive magnetron sputtering is considered to be a proper process because of homogeneity of microstructure, improvement of productivity and simplicity of independent control for several critical deposition parameters. The N2 is applied to reactive gas to make nitride system with transition metals which is much harder than only alloy systems. The acceleration voltage from 100W to 300W is controlled by direct current power with various deposition times. The coating layers are systemically investigated by structural identification (XRD), evaluation of microstructure (FE-SEM, TEM) and mechanical properties (Nano-indenter).

• 한국주조공학회지
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• 제20권4호
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• pp.254-259
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• 2000

Metal matrix composites(MMCs) reinforced with hard particles have many potential application in aerospace structures, auto parts, semiconductor package, heat resistant panels, wear resistant materials and so on. In this work, the effect of SiC partioel sizes(50 and 100 ${\mu}m$) and additional elements such as Si, Cu and Ti on the microstructure and the wear property of $Al-5Mg-X(Si,Cu,Ti)/SiC_p$ composites produced by pressureless infiltration method have been investigated using optical microscopy, scanning eletron microcopy(SEM) with EDS(energy dispersive spectrometry), hardness test, X-ray diffractometer(XRD) and wear test. In present study, the sound $Al-5Mg-X(Si,Cu,Ti)/SiC_p$(50 and 100 ${\mu}m$) composites were fabricated by pressureless infiltration method. The $Al-5Mg-0.3Si-O.1Cu-O.1Ti/SiC_p$ composite with $50 {\mu}m$ size of SiC particle has higher hardness and better wear property than any other composite with $100{\mu}m$ size of SiC particle produced by pressureless infiltration method. The hardness and wear property of $Al-5Mg/SiC_p$(50 and 100 ${\mu}m$) composites were enhanced by the addition of Si, Cu and Ti in Al-5%Mg matrix alloy.