• 한국표면공학회지
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• 제36권2호
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• pp.155-160
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• 2003

The effect of the temperature, current density and deposit time on hard chromium deposition in trivalent chromium bath was investigated. Cathode current efficiency increased with increasing current density. Increasing bath temperature from $20^{\circ}C$ to $50^{\circ}C$, chromium deposits were produced in higher current density and the maximum current efficiency was increased. At the plating conditions of $40^{\circ}C$, $30A/dm\m^2$, the deposition thickness increased in proportion to increasing electrolysis time The rate is$ 90\mu\textrm{m}$/hrs. for 2 hours. Microhardness of chromium deposits increased with increasing bath temperature and decreasing current density, and it was constant with electrolysis time. All of bath conditions, microstructure of chromium deposits has nodular structure with some cracking pattern and nodule size increased with increasing deposit thickness.

• 한국표면공학회:학술대회논문집
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• 한국표면공학회 2016년도 추계학술대회 논문집
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• pp.111-111
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• 2016

Two step PEO ceramic coatings were formed on AZ91 magnesium alloy in $ZrO_2$ nanoparticles and $K_2ZrF_6$ based colloidal electrolyte solution for various voltages. Surface and layers tructure of the coatings was analyzed using SEM (ScanningElectronMicroscope). Structure analysis revealed that surface of the coating was transferred from individual pancake or craters-based structure to cluster-based structure with increasing the voltage of the secondary step process. Further, it was confirmed that the cluster zone was richin Zr-based complexes and formed due to high intensives parks. Increase in the Zr contents as discovered from the EDS analysis confirmed the rise in amorphous form of the Zr-based species, which justified the results of XRD where no increase in the intensity of Zr-based species was observed with increase in voltage. Potentiodynamic polarizariotion and impedance spectroscopy techniques were used to evaluate the corrosion performance of the coatings. The highest corrosion resistance was found for coatings prepared at 240V. The same specimen was found having highest and uniform vickers hardness ~1070.5 HV. The superior mechanical and electrochemical properties of the said coating can be attributed to the defect-less microstructure and the optimal role of $ZrO_2$ nanoparticles in the secondary PEO process at 240V.

• 한국분말재료학회지
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• 제5권1호
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• pp.28-34
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• 1998

Plasma sprayed ceramic coatings are widely used in various industrial fields to improve their properties or to reduce the production cost. The ceramic powders for plasma spray coating have been mainly manufactured by spray drying or fused+crushed process. In this study, chromium oxide which has better mechanical properties than those of the other ceramic was selected and agglomerated chromium oxide powders for plasma spray coating were produced by spray drying process with a various processing condition. The large hollow powders and the harsh surfaced powders are formed at high slurry feed rate more than 163 g/min. and low binder concentration less than 2wt%, respectively. These powders cause the considerable decrease of flowability and apparent density. The powders produced by spray drying process have the spherical shape with the mean size of 45 ${\mu}m$, but these are shown lower apparent density and flowability than the powders produced by fused+crushed powders. The plasma spray coated layers by spray dried powders are shown a different microstructure with that by fused+crushed powders in porosity shape, but their properties such as density, hardness and bond strength are similar.

• 한국주조공학회지
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• 제35권1호
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• pp.1-7
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• 2015

In this study, we investigated the effect of carbon on mechanical properties with different austempering conditions of high carbon(0.7~1.3wt.%C)-2.0wt.%Si steels. The specimens were austenitized at 850, 925 and $1020^{\circ}C$, and austempered at 260, 320 and $380^{\circ}C$ for the various period of time from 3 min to 300 min. After heat treatment, the evolution of stage I and stage II was identified with optical microscope, XRD and hardness test. When the austempering temperature was $260^{\circ}C$, the microstructure consisted of the lower ausferrite while the upper ausferrite micro-structure was formed at $380^{\circ}C$. As the austempering temperature increases from 260 to $380^{\circ}C$, the tensile strength decreases and elongation increases. In addition, when carbon content increases, tensile strength and elongation decrease.

• 한국주조공학회지
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• 제35권6호
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• pp.163-169
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• 2015

This study reports the influence of gadolinium (Gd) addition on mechanical and corrosion properties of 2205 duplex stainless steel. In all alloys produced, regardless of the initial Gd content, Gd-based inclusions were well distributed in the duplex stainless steel matrix. As the Gd content increased from 0 wt% to 0.19 wt%, the ultimate tensile strength and hardness of the alloy increased from 630 MPa to 977 MPa and from 57 to 61, respectively, while elastic modulus, tensile elongation and impact energy of the alloy decreased. The critical crevice temperatures of Alloy1, Alloy2 and Alloy3 were $20^{\circ}C$, $20^{\circ}C$ and $15^{\circ}C$, respectively.

• 한국주조공학회지
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• 제31권4호
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• pp.205-211
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• 2011

Al-Si alloys have been steadily used as a potential material for the achievement of an efficient weight reduction in the automobile and aerospace industries due to its excellent castability and high strength-to-weight ratio. In this study, riser effect and mechanical properties were investigated according to the size of the sleeve. In addition, the effects of riser size on mechanical properties of castings were investigated. On the other hand flow and solidification process were simulated with a hybrid FDM/FEM package named ZCast. As a result, results of simulation and experiments were comparable regarding to the yield strength, tensile strength, elongation and hardness of casting. It proves the reliability of the simulation. It is expected that the proper size of riser can improve the recycling rate of metallic materials and reduce the cost of casting.

• 한국주조공학회지
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• 제28권6호
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• pp.268-272
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• 2008

Interfacial characteristics of aluminum borate whisker reinforced AS52 matrix composite was investigated. Peak hardness of AS52 composite was obtained aging at $170^{\circ}C$ for 15h and the aging process was accelerated by the presence of the aluminium borate whisker. The MgO layer, which was the interfacial reaction product between the reinforcement and the Mg matrix, was produced with 20 nm thickness in as-cast condition. As the aging time increased, the thickness of the interfacial reaction layer increased to 50 nm in peak aged condition. The nano-indentation test results indicated that the strength of interface was improved by the aging but over-aging degraded the reinforcement and decreased the interfacial strength which resulted in the decrease of overall composite strength.

• Journal of Welding and Joining
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• 제35권3호
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• pp.35-43
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• 2017

A 3D transient heat transfer model is developed by ABAQUS software to study the temperature distribution during friction stir welding process at different rotational speeds. Furthermore, AA 5083-O plates were joined by FSW technique. For this purpose, a universal milling machine was used to perform the welding process and a mechanical vice was used to fix the work pieces in the proper position. The joints were friction stir welded at a constant travel speed 50 mm/min and two rotational speed values; 400 rpm and 630 rpm using two types of tools; cylindrical threaded pin and tapered smooth one. At each welding condition the temperature was measured using infra-red thermal image camera to verify the simulated temperature distribution. The welded joints were visually inspected as well as by macro- and microstructure evolutions. In addition, the welded joints were mechanically tested for hardness and tensile strength. The maximum peak temperature obtained was at higher rotational speed using the threaded tool pin profile. The results showed that the rotational speed affects the peak temperature, defects formation and sizes, and the mechanical properties of friction stir welded joints. Moreover, the threaded tool gives superior mechanical properties than the tapered one at lower rotational speed.

• 한국세라믹학회지
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• 제36권5호
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• pp.471-477
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• 1999

Fe and Fe-Mo binder were used to produce TiB2 based cermet by a pressureless sintering. The densification behaviour of TiB2-Fe-Mo cermet during liquid-phase sintering in argon was studied in relation to binder phase charactertics. The effects of Mo addition and sintering condition on the sintering behaviour and mechanical properties were also investigated. TiB2-based cermets with Fe-Mo binder composition showed a better sinterability than the cermets with only Fe binder. In TiB2-Fe-Mo cermet higher densities in the wide temperature range were obtained and also fully densified sintered cermet were obtained at 1873K The enhancement in the densification phenomenon of TiB2-Fe-Mo system can be explained by improved liquid phase wettability associated with the roles of Mo components as solute atoms. When Fe-Mo binders were used cermets with a finer grain size and enhanced mechanical properties wereproduced and new phases such as Fe2B and Mo2FeB2 were observed in the sintered cermet. The highest bending strength was obtained from the 20vol% Fe-Mo cermet and these hardness-fracture toughness combination in the wide binder compositions is better than that of TiB2-Fe cermet. In order to improve mechanical properties microstructure control with high purity powders is desirable because high purity powders prevent the formation of Fe2B and Mo2FeB2 phase which comsume the ductile binder phase.

• 한국세라믹학회지
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• 제28권5호
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• pp.422-428
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• 1991

The reaction sintering of Al2O3-ZrO2-Nb composite has been investigated using Al2O3, and ZrAl2 powders. Two kinds of specimens, 78.3Al2O3-14.0Nb2O5-7.7ZrAl2 in wt.% (AZN-5) and 72.3Al2O3-13.8Nb2O5-7.5ZrAl2-6.4ZrO2(AZN-10), were prepared. Powder compacts were sintered at various temperatures between 1$600^{\circ}C$ and 1$700^{\circ}C$ for 30 min in Ar. DTA and X-ray analysis have showen that a reaction between Nb2O5 and ZrAl2 started at 149$0^{\circ}C$ to form Al2O3, ZrO2, and Nb. The sintered density increased with the sintering temperature. AZN-10 specimen showed higher density than AZN-5 specimen for almost all the experimental conditions. Al2O3-ZrO2-Nb composite hot pressed after reaction sintering showed higher toughness and lower hardness than hot pressed Al2O3-ZrO2. The crack propagated through many metallic Nb particles which showed plastic deformation, and this is the cause of the increase in toughness of Al2O3-ZrO2-Nb composite over Al2O3-ZrO2.