• Title/Summary/Keyword: microstructure hardness

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Electroplating on the Lead Frames Fabricated from Domestic Copper Plate (국산동판을 사용한 리드프레임 도금기술에 관한 연구)

  • Jang, Hyeon-Gu;Lee, Dae-Seung
    • Journal of the Korean institute of surface engineering
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    • v.19 no.3
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    • pp.92-108
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    • 1986
  • An electroplating on the lead frame fabricated from domestic copper plate was studied experimentally. In this study, nickel was plated on the thin copper lead frame and silver layer was coated on the nickel film in the cyanide electrolyte. The effect of process variables such as current density, plating time, coating thickness and flow rate of electrolytic solution on the properties of coating was investigated. Some samples on each step were fabricated during electroplating. The results obtained from polarization measurement, observation of SEM photograph, adhesion test of coating and microhardness test are as follows. On silver plating, polarization resistance of potentiostatic cathodic polarization curve is reduced as the flow rate of Ag electrolytic solution increases. And above resistance is also reduced when the minor chemicals of sodium cyanide and sodium carbonate are added in potassium silver cyanide bath. The reduced polarization resistance makes silver deposition on the cathode easy. An increase in the current density and the coating thickness causes the particle size of deposit to coarsen, and consequently the Knoop microhardness of the coating decreases. On selective plating an increase in the flow rate of plating solution lead to do high speed plating with high current density. In this case, the surface morphology of deposit is of fine microstructure with high Knoop hardness. An increasing trend of the adhesion of coating was shown with increasing the current density and flow rate of electrolytic solution.

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Application of the Murakami Approach for Prediction of Surface Fatigue of Cemented Carbides

  • Sergejev, Fjodor;Kubarsepp, Jakob;Preis, Irina
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.633-634
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    • 2006
  • The aim of present work is to link geometrical parameter of maximum area of structural defect $\sqrt{area}\;_{max}$ (proposed by Y. Murakami, 1983) with surface fatigue mechanisms. Determined relations allow making predictions of surface fatigue properties of cemented carbides (WC-Co hardmetal - H15 - 85wt% WC and 15wt %Co, TiC-based cermets - T60/8 - 60wt %TiC and Fe/8wt% Ni and T70/14 - 70wt %TiC and Fe/14wt% Ni) in conditions of rolling contact and impact cycling loading. Pores considered being equivalent to small defects. Three comparative defects conditions are distinguished: surface pore, just below free surface and interior pores. The Vickers hardness of binder (as main responsible for the fracture mechanism of hardmetal and cermets) assumed to be the basis of such assumption. The estimate of this prediction has been done by analyzing the pore sizes using the statistics of extremes. The lower bound of fatigue properties can be correctly predicted by considering the maximum occurring pore size.

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Fabrication and Properties of Reaction Squeeze Cast $(Al_2O_3+Si)/Mg$ Hybrid Metal Matrix Composites (반응용탕단조법에 의한 $(Al_2O_3+Si)/Mg$ 하이브리드 금속복합재료의 제조 및 특성평가)

  • Oh, Dong-Hyun;Jeon, Sang-Hyuk;Park, Ik-Min;Cho, Kyung-Mox;Choi, Il-Dong
    • Journal of Korea Foundry Society
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    • v.20 no.1
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    • pp.13-20
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    • 2000
  • In the present study,($10%Al_2O_3+5%Si$)/AZ91 Mg hybrid composite was fabricated using the squeeze casting method. During squeeze casting, Molten Mg was infiltrated into the preform of $10%Al_2O_3+5%Si$ and reaction product of $Mg_2Si$ intermetallic compound was formed by the reaction between molten Mg and Si Powder. Microstructure has been observed and mechanical properties were evaluated for the reaction squeeze cast(RSC) hybrid composite. It was found that Si powder totally reacted with molten Mg to form $Mg_2Si$. Reinforcement($Al_2O_3$) and the reaction product ($Mg_2Si$) are fairly uniformly distributed in Mg Matrix for the squeeze cast hybrid composite. Mechanical Properties were improved with hybridization of reinforcements, namely higher hardness and enhanced wear resistance comparing squeeze cast($15%Al_2O_3$)/AZ91 Mg composite.

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Effect of Austempering Temperatures on the Fractures Characteristic of Grey Cast Iron (오스템퍼링 처리한 회주철의 파괴특성에 미치는 오스템퍼링 온도의 영향에 관한 연구)

  • Kim, Chang-Gyu;Lee, Sung-Yul;Choi, Chang-Ock
    • Journal of Korea Foundry Society
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    • v.12 no.6
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    • pp.442-449
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    • 1992
  • Grey cast iron containing a small amount of Cu and Mo to improve the effect of heat treatment and microstructure were cast and them austenitized. After austenitizing the specimens of castings were austempered at 250$^{\circ}C$, 300$^{\circ}C$ and 350$^{\circ}C$. The effects of matrix structures on mechanical properties and fracture characteristics at the different austempering temperature were investigated. Tensile strength, hardness and impact toughness of austempered grey cast iron showed maximum valve 359 MPa, 321 HB, 3.9 CVN respectively at the lowest austempering temperature, 250$^{\circ}C$. $K_{IC}$ of gref cast iron at a austempering temperature, 250$^{\circ}C$, showed maximum 44 MPa.$m^{1/2}$ even though the amount of retained austenite in it is only 16%. This mainly comes from the refinement of the retained austenite. Quasi-cleavage pattern with a little fit of fibrous pattern was shown on the fractured surface of austempered grey cast iron at all of the temperatures tested.

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Development of Control Technology of Austempered Ductile Iron with High Strength and High Toughness for Gear Parts. (고강도 ADI의 기어부품 개발에 관한 연구)

  • Kim, Won-Yong;Kim, Kwang-Bae;Kang, In-Chan;An, Sang-Uk
    • Journal of Korea Foundry Society
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    • v.13 no.2
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    • pp.187-193
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    • 1993
  • In this study, it was examined the relationship between the microstructure, fatigue properties, mechanical properties and retained austenite volume of Mo-Ni ADI corresponding to various austempering temperatures. When the austempering temperature is increased to $370^{\circ}C$, acicular bainite structure was found to be transformed to feathery bainite structure. But at the austempering temperature of $420^{\circ}C$, the dissolved bainite lath was showned. Up to the austempering temperature of $370^{\circ}C$, the volume of retained austenite was increased. However at the austempering temperature of $420^{\circ}C$ a large amount of retained austenite was decreased. In this study, the retained austenite volume was determined by XRD(X-ray diffraction). It was observed that the optimum fatigue properties can be obtained at the condition of austempering temperature $370^{\circ}C$. Under the such conditions, fatigue limit determined as the value of 290 MPa, tensile strength 877MPa elongation 6%, hardness 285(BHN), impact values(CVN) 9.2J and retained austenite volume 30.3%, respectively.

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A Study on the Direct Synthesis of TaC by Cast-bonding (주조접합법에 의한 TaC 직접합성에 관한 연구)

  • Park, Heung-Il;Lee, Sung-Youl
    • Journal of Korea Foundry Society
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    • v.17 no.4
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    • pp.371-378
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    • 1997
  • The study for direct synthesis of TaC carbide which was a reaction product of tantalum and carbon in the cast iron was performed. Cast iron which has hypo-eutectic composition was cast bonded in the metal mold with tantalum thin sheet of thickness of $100{\mu}m$. The contents of carbon and silicon of cast iron matrix was controlled to have constant carbon equivalent of 3.6. The chracteristics of microstructure and the formation mechanism of TaC carbide in the interfacial reaction layer in the cast iron/tantalum thin sheet heat treated isothermally at $950^{\circ}C$ for various time were examined. TaC carbide reaction layer was grown to the dendritic morphology in the cast iron/tantalum thin sheet interface by the isothermal heat treatment. The composition of TaC carbide was 48.5 at.% $Ti{\sim}48.6$ at.% C-2.8 at.% Fe. The hardness of reaction layer was MHV $1100{\sim}1200$. The thickness of reaction layer linearly increased with increasing the total content of carbon in the cast iron matrix and isothermal heat treating time. The growth constant for TaC reaction layer was proportional to the log[C] of the matrix. The formation mechanism of TaC reaction layer at the interface of cast iron/tantalum thin sheet was proved to be the interfacial reaction.

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Study on the Effect of Mo Addition and Casting Thickness on the Mechanical Properties of Thin Ductile Cast Iron (박육구상흑연주철에 있어서 Mo 첨가 및 주물두께의 영향에 관한 연구)

  • Song, Byeong-Woo;Choi, Yang-Jin;Kim, Yong-Hwan;Park, Yong-Jin
    • Journal of Korea Foundry Society
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    • v.13 no.2
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    • pp.175-186
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    • 1993
  • In this study, the effect of Mo addition on the microstructure and mechanical properties of ductile cast iron have been investigated. The amounts of Mo and the thickness of specimen have been varied from 0 to 4.79wt% and 13mm, 10mm and 6mm, respectively. As the casting thickness decreases, the average size of spheroidal graphite is decreased and the hardness increases. By increasing the Mo content, the tensile strength of ferrite and pearlite matrix increases and shows maximum which is about $30{\sim}40%$ higher than ordinary ductile cast iron. After the maximum, adding more Mo results in gradual transformation of ferrite and pearlite to bainite and thus tensile strength decreases again. The elongation decreases continueously with Mo content. The addition of Mo about $0.5{\sim}1.0wt%$ improves the wear resistance and tensile strength of thin ductile cast iron.

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The Hydrogen Behavior of Surface Layers of High Strength DP Thin Sheet Steels for Automobile (자동차 박강판용 고강도 DP강 표면층의 수소거동)

  • Park, Jae-Woo;Kang, Kae-Myung
    • Journal of the Korean Institute of Gas
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    • v.14 no.6
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    • pp.38-43
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    • 2010
  • According to the lack of resources and the stringency of environmental regulations, a study of the high strength thin plate sheet steels for automobile have been become an important issue for automobile industry. However, the problem of hydrogen embrittlement of high strength sheet steels was concerned with the degradation of mechanical properties. Therefore, we studied the hydrogen behavior of surface layers of 590MPa DP sheet steels on development using by relationship the microstructure of subsurface and the distribution of micro hardnesses. Hydrogen was charged into the specimens using by the cathodic electrolytic method. The behavors of under surface layers were investigated by the observation of microstructures and the micro vickers hardness test with the amount of hydrogen charging with hydrogen charging conditions.

Compression D/B for Liquid Segregation Control in Semi-Solid Forming Process and Its Application (반용융 성형공정에 있어서 액상편석제어를 위한 압축 D/B 및 응용)

  • 정경득
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 1999.06a
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    • pp.15-32
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    • 1999
  • A relationship between stress and stain is very important to design a die to avoid defects of products during semi-solid forming process. Since the liquid will be of eutectic composition in alloys liquid segregation will result in significant or undesirable situation. The materials used in this experiment are A 357. A390, Al2024 alloys that is fabricated by the electro-magnetic stirring process from Pechiney in France. The compression test was performed by induction heating equipment and MTS. In order to prevent the liquid segregation these measured temperature would be useful to control of strain rate during compression test. The liquid segregation is controlled as change of the strain rate and solid fraction during the compression process, The characteristics of flow between solid and liquid phase considering liquid segregation is examined through the above experiments. In the case of medium and high volume fractions of solid the distribution of strain rate is calculated by using compression test data of semi-solid materials (SSM). The thixoforming experiments with the designed die are carried out successfully. The die filling patterns of SSM for variation of die temperature and pressing force have been investigated. The hardness of the thixoformed scroll products is evaluated in terms of the microstructure for each position.

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Properties of a Helical Gear Due to the Manufacturing Process - Forged versus Machined Product (헬리컬기어 제조공정에 따른 특성 비교 -단조품과 기계가공품-)

  • Jung, H.C.;Kang, B.S.;Lee, I.H.;Choi, S.T.;Sin, S.J.;Kang, S.H.;Lee, Y.S.
    • Transactions of Materials Processing
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    • v.21 no.1
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    • pp.67-74
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    • 2012
  • Although high productivity is possible, cold forged helical gears have not been widely used due to difficulty in achieving mechanical properties as well as dimensional accuracy of the product. Confidence in the gear characteristics also is very important in heavy-duty gear applications. Therefore, the properties of forged gears must be compared to the properties of conventional machined gears. The properties might be different due to the different fabrication processes. In this study, machined and forged products both before and after heat-treated have been compared by measuring the residual stress and involute curve of the tooth. Characteristics of hardness and microstructure were also compared. Additionally, tooth fracture strength was compared for the heat-treated products. Moreover, the tooth strength and the fracture pattern were compared between the machined and forged gears. The forged gear showed decreased changes in residual stress and decreased changes in dimensions when compared to the machined gear before and after heat treatment. The forged gear was over 10% better than the machined gear in tooth strength.