• 제목/요약/키워드: microstructure

검색결과 8,113건 처리시간 0.031초

Dynamics of silicon nanobeams with axial motion subjected to transverse and longitudinal loads considering nonlocal and surface effects

  • Shen, J.P.;Li, C.;Fan, X.L.;Jung, C.M.
    • Smart Structures and Systems
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    • 제19권1호
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    • pp.105-113
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    • 2017
  • A microstructure-dependent dynamic model for silicon nanobeams with axial motion is developed by considering the effects of nonlocal elasticity and surface energy. The nanobeam is considered to subject to both transverse and longitudinal loads arising from nanostructural surface effect and all positive directions of physical quantities are defined clearly prior to modeling so as to clarify the confusions of sign in governing equations of previous work. The nonlocal and surface effects are taken into consideration in the dynamic behaviors of silicon nanobeams with axial motion including circular natural frequency, vibration mode, transverse displacement and critical speed. Various supporting conditions are presented to investigate the circular frequencies by a numerical method and the effects of many variables such as nonlocal nanoscale, axial velocity and external loads on non-dimensional circular frequencies are addressed. It is found that both nonlocal and surface effects play remarkable roles on the dynamics of nanobeams with axial motion and cause the frequencies and critical speed to decrease compared with the classical continuum results. The comparisons of the non-dimensional calculation values by present and previous studies validate the correctness of the present work. Additionally, numerical examples for silicon nanobeams with axial motion are addressed to show the nonlocal and surface effects on circular frequencies intuitively. Results obtained in this paper are helpful for the design and optimization of nanobeam-like microstructures based sensors and oscillators at nanoscale with desired dynamic mechanical properties.

소성 구배의 영향을 고려한 다결정 고체 내부의 결정 거동 분석 (Evaluation of Effect of Plastic Gradient on the Behavior of Single Grain inside Polycrystalline Solids)

  • 정상엽;한동석
    • 한국방재학회 논문집
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    • 제11권2호
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    • pp.39-44
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    • 2011
  • 마이크로 스케일에서 다결정 재료의 소성 거동을 살펴볼 때, 결정의 geometrically necessary dislocation(GND) 효과에 의한 소성 구배(plastic gradient)를 고려하는 것은 재료의 소성 거동에 큰 영향을 줄 수 있다. 이러한 영향을 확인하기 위하여, 본 연구에서는 소성 구배의 영향을 고려한 다결정 고체(polycrystalline solids)의 거동을 유한요소해석을 이용하여 살펴보았다. 소성 구배의 영향을 살펴보기 위해 구배 경화 계수(gradient hardness coefficient)와 먼 거리 변형률에 대한 재료 길이 변수 (material length parameter)가 사용되었다. 재료 길이 변수에 의한 영향을 확인하기 위해, 재료 길이 변수의 차이에 따른 다결정 고체의 거동을 분석하였다. 또한 소성 구배 효과의 고려 및 재료 길이 변수에 따른 다결정 고체 내부에 위치한 단결정이 받는 영향을 살펴보았다. 재료 길이 변수에 따라 결정이 받는 영향을 비교하여, GND에 의한 다결정 고체 거동의 영향을 확인하였다.

역학적 등방성을 가진 2상 다결정 미세구조의 재구성 기법 (Reconstruction of Two-phase Polycrystalline Microstructures of Mechanical Isotropy)

  • 정상엽;한동석
    • 한국방재학회 논문집
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    • 제11권2호
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    • pp.31-37
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    • 2011
  • 다상 재료는 상(phase) 분포의 차이에 따라 재료의 특성이 다르기 때문에 상 분포 상태의 특성을 이해하는 것이 중요하다. 본 연구에서는 확률 분포 함수를 사용하여 미세구조의 상 분포 상태를 나타내고, 이를 사용한 미세구조 재구성 방법을 이용해서 특정 2상 미세구조와 통계적으로 유사한 상 분포를 가진 미세구조를 생성하여 기존의 미세구조와 재구성된 미세구조의 특성을 비교하였다. 그리고 서로 다른 임의의 상 분포를 가진 미세구조들에 유한요소해석 기법을 적용하여 서로 다른 하중 방향에 대한 미세구조의 역학적 거동을 분석하였다. 이를 통해, 미세구조 재구성 방법을 사용하여, 제한된 정보만을 이용해서 통계적으로 유사한 특성을 나타내는 미세구조를 모델링 할 수 있음을 확인하였고, 확률 분포 함수와 미세구조의 역학적 거동이 방향에 따라 동일함을 통하여 재생성 된 재료의 등방성을 확인하였다.

빌렛 형상 제어를 통한 Mg-5Bi 합금 압출재의 조직 균일도 및 기계적 물성 변화 (Variation in Microstructural Homogeneity and Mechanical Properties of Extruded Mg-5Bi Alloy Via Controlling Billet Shape)

  • 진상철;차재원;박성혁
    • 소성∙가공
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    • 제31권6호
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    • pp.344-350
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    • 2022
  • Extruded Mg-Bi binary alloys are known to have an undesirable bimodal grain structure containing a large amount of coarse unrecrystallized grains. Accordingly, to improve the microstructural homogeneity of extruded Mg-Bi alloys, it is necessary to promote the dynamic recrystallization (DRX) behavior during hot extrusion. An effective way to promote DRX is an increase in nucleation sites for DRX through a pre-deformation process before extrusion, such as cold pre-forging and hot pre-compression. However, the application of these pre-deformation processes increases the cost of final extruded Mg products because of an increase in energy consumption and decrease in productivity. Therefore, a low-cost new continuous process with high productivity is required to improve the microstructural homogeneity and mechanical properties of extruded Mg alloys without a drastic increase in the entire process cost. This study proposes a new extrusion method using an extrusion billet with a truncated cone shape (i.e., tapered billet) instead of a conventional extrusion billet with a cylindrical shape. When the hot extrusion of a Mg-5Bi alloy is conducted using the tapered billet, the DRX behavior during extrusion is considerably promoted. The DRX fraction and average grain size of the extruded alloy significantly increase and decrease from 65% to 91% and from 225 ㎛ to 49 ㎛, respectively. Consequently, the extruded Mg-5Bi alloy fabricated using the tapered billet has a finer homogeneous grain structure and higher tensile elongation than the extruded counterpart fabricated using the cylindrical billet.

Low-Molecular-Weight Collagen Peptide Ameliorates Osteoarthritis Progression through Promoting Extracellular Matrix Synthesis by Chondrocytes in a Rabbit Anterior Cruciate Ligament Transection Model

  • Lee, Mun-Hoe;Kim, Hyeong-Min;Chung, Hee-Chul;Kim, Do-Un;Lee, Jin-Hee
    • Journal of Microbiology and Biotechnology
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    • 제31권10호
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    • pp.1401-1408
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    • 2021
  • This study examined whether the oral administration of low-molecular-weight collagen peptide (LMCP) containing 3% Gly-Pro-Hyp with >15% tripeptide (Gly-X-Y) content could ameliorate osteoarthritis (OA) progression using a rabbit anterior cruciate ligament transection (ACLT) model of induced OA and chondrocytes isolated from a patient with OA. Oral LMCP administration (100 or 200 mg/kg/day) for 12 weeks ameliorated cartilage damage and reduced the loss of proteoglycan compared to the findings in the ACLT control group, resulting in dose-dependent (p < 0.05) improvements of the OARSI score in hematoxylin & eosin (H&E) and Safranin O staining. In micro-computed tomography analysis, LMCP also significantly (p < 0.05) suppressed the deterioration of the microstructure in tibial subchondral bone during OA progression. The elevation of IL-1β and IL-6 concentrations in synovial fluid following OA induction was dose-dependently (p < 0.05) reduced by LMCP treatment. Furthermore, immunohistochemistry illustrated that LMCP significantly (p < 0.05) upregulated type II collagen and downregulated matrix metalloproteinase-13 in cartilage tissue. Consistent with the in vivo results, LMCP significantly (p < 0.05) increased the mRNA expression of COL2A1 and ACAN in chondrocytes isolated from a patient with OA regardless of the conditions for IL-1β induction. These findings suggest that LMCP has potential as a therapeutic treatment for OA that stimulates cartilage regeneration.

직접식 에너지 용착 공정을 활용한 축 보수 방법 및 활용 사례 연구 (A Study on the Method and Application of Shaft Repair using Directed Energy Deposition Process)

  • 이윤선;이민규;성지현;홍명표;손용;안석;정외철;이호진
    • 한국기계가공학회지
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    • 제20권9호
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    • pp.1-10
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    • 2021
  • Recently, the repair and recycling of damaged mechanical parts via metal additive manufacturing processes have been industrial points of interest. This is because the repair and recycling of damaged mechanical parts can reduce energy and resource consumption. The directed energy deposition(DED) process has various advantages such as the possibility of selective deposition, large building space, and a small heat-affected zone. Hence, it is a suitable process for repairing damaged mechanical parts. The shaft is a core component of various mechanical systems. Although there is a high demand for the repair of the shaft, it is difficult to repair with traditional welding processes because of the thermal deformation problem. The objective of this study is to propose a repair procedure for a damaged shaft using the DED process and discuss its applications. Three types of cases, including a small shaft with a damaged surface, a medium-size shaft with a worn bearing joint, and a large shaft with serious damage, were repaired using the proposed procedure. The microstructure and hardness were examined to discuss the characteristics of the repaired component. The efficiency of the repair of the damaged shaft is also discussed.

Wear evaluation of CAD-CAM dental ceramic materials by chewing simulation

  • Turker, Izim;Kursoglu, Pinar
    • The Journal of Advanced Prosthodontics
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    • 제13권5호
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    • pp.281-291
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    • 2021
  • PURPOSE. To evaluate the wear of computer-aided design/computer-aided manufacturing (CAD-CAM) dental ceramic materials opposed by enamel as a function of increased chewing forces. MATERIALS AND METHODS. The enamel cusps of healthy human third molar teeth (n = 40) opposed by materials from CAD-CAM dental ceramic groups (n = 10), including Vita Enamic® (ENA), a polymer-infiltrated ceramic network (PICN); GC Cerasmart® (CERA), a resin nanoceramic; Celtra® Duo (DUO), a zirconia-reinforced lithium silicate (ZLS) ceramic; and IPS e.max ZirCAD (ZIR), a polycrystalline zirconia, were exposed to chewing simulation (1,200,000 cycles; 120 N load; 1 Hz frequency; 0.7 mm lateral and 2 mm vertical motion). The wear of both enamel cusps and materials was quantified using a 3D laser scanner, and the wear mechanisms were evaluated by scanning electron microscopy (SEM). The results were analysed using Welch ANOVA and Kruskal Wallis test (α = .05). RESULTS. ZIR showed lower volume loss (0.02 ± 0.01 mm3) than ENA, CERA and DUO (P = .001, P = .018 and P = .005, respectively). The wear of cusp/DUO [0.59 mm3 (0.50-1.63 mm3)] was higher than cusp/CERA [0.17 mm3 (0.04-0.41 mm3)] (P = .007). ZIR showed completely different wear mechanism in SEM. CONCLUSION. Composite structured materials such as PICN and ZLS ceramic exhibit more abrasive effect on opposing enamel due to their loss against wear, compared to uniform structured zirconia. The resin nano-ceramic causes the lowest enamel wear thanks to its flexible nano-ceramic microstructure. While zirconia appears to be an enamel-friendly material in wear volume loss, it can cause microstructural defects of enamel.

Evaluation of 475 ℃ embrittlement in UNS S32750 super duplex stainless steel using four-point electric conductivity measurements

  • Gutierrez-Vargas, Gildardo;Ruiz, Alberto;Lopez-Morelos, Victor H.;Kim, Jin-Yeon;Gonzalez-Sanchez, Jorge;Medina-Flores, Ariosto
    • Nuclear Engineering and Technology
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    • 제53권9호
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    • pp.2982-2989
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    • 2021
  • One of the consequences of the 475 ℃ embrittlement of duplex stainless steels is the reduction of the resistance to localized corrosion. Therefore, the detection of this type of embrittlement before the material exhibits significant loss in toughness, and corrosion resistance is important to ensure the structural integrity of critical components under corrosion threats. In this research, conductivity measurements are performed using the alternating current potential drop (ACPD) technique with using a portable four-point probe as a nondestructive evaluation (NDE) method for detecting the embrittlement in a 2507 (UNS S32750) super duplex stainless steel (SDSS) aged at 475 ℃ from as-received condition to 300 h. The electric conductivity results were compared against two electrochemical tests namely double loop electrochemical potentiokinetic reactivation (DL-EPR) and critical pitting temperature (CPT). Mechanical tests and the microstructure characterized using scanning electron microscopy (SEM) imaging are conducted to track the progress of embrittlement. It is shown that the electric conductivity correlates with the changes in impact energy, microhardness, and CPT corrosion tests result demonstrating the feasibility of the four-point probe as a possible field-deployable method for evaluating the 475 ℃ embrittlement of 2507 SDSS.

열확산 프로세스에 의한 초전도 벌크 합성 (Fabrication of the Bulk Superconductor by Thermal Diffusion Process)

  • 이상헌
    • 한국전기전자재료학회논문지
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    • 제34권6호
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    • pp.461-465
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    • 2021
  • A diffusion heat treatment process for YBa2Cu3O7-y bulk superconductor in a Gd2O3 powder was attempted. As a result of measuring the critical temperature of the superconducting bulk, there was no change in the superconducting transition temperature as the Gd particles diffused into the YBa2Cu3O7-y lattice, resulting in dense microstructure. As a result of measuring the critical current, the critical current density (Jc) of the superconducting bulk having treated by the Gd thermal diffusion treatment at 0 T increased to 3×104 A/cm2 at 0 T, which was higher than that of the superconducting bulk without thermal diffusion treatment. The surface magnetic force of the superconducting bulk with Gd thermal diffusion treatment was observed at the center of the superconducting bulk with the maximum trapped magnetic force (Hmax) of 1.51 kG. This result means that the Gd thermal diffusion treatment contributes to improving the critical current density Jc of YBa2Cu3O7-y, and it is believed that Gd particles migrating into the superconducting bulk through thermal diffusion either fill the surface pores of YBa2Cu3O7-y superconductors or act as a flux pinning center.

압출 출구 온도에 따른 Al 6061 합금의 표면 재결정층 두께 변화 및 기계적 특성 변화 (The Thickness of Recrystallization Layer and Mechanical Properties According to Extrusion Exit Temperature)

  • 김수빈;박태희;김현기;이상목;김희국
    • 소성∙가공
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    • 제30권5호
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    • pp.219-225
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    • 2021
  • When extruding Al6061 alloys, deformation energy is deposited inside the extruded alloy depending on the deformation and the temperature of extrusion. This creates a Peripheral Coarse Grain (PCG) on the surface, where relatively more deformation energy. of the extruded alloy has been accumulated. Furthermore, since the deformation of materials continues while the materials recrystallize, it is important to examine the effect of deformation energy on dynamic recrystallization in the process of extruding Al alloys along with their microstructure. Prior studies explain the theory behind PCG growth though quantitative analysis on PCG growth of Al alloys during extrusion processes has not yet been addressed. This study aims to measure the generated PCG thickness which determines the correlation between extrusion outlet temperature and its effect on mechanical properties. Surface structure observations were performed using Optical Microscope (OM) and mechanical properties were evaluated through tensile strength and hardness measurement. Throughout this study, we endevoured to find the optimum condition of extrusion exit temperature of Al6061 and confirmed improved d reliability. This study describes the effect of the complex process variables such as exit temperature on the thickness of PCG layer for the Al6061 alloy using the 200 tons extrusion press. We therefore, discovered that the PCG layer thickness was 117 ㎛ at temperatures between 460 ℃ to 520 ℃.