• Title/Summary/Keyword: microstructural analysis

검색결과 532건 처리시간 1.057초

Successive recycled coarse aggregate effect on mechanical behavior and microstructural characteristics of concrete

  • Ashish, Deepankar K.;Saini, Preeti
    • Computers and Concrete
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    • 제21권1호
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    • pp.39-46
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    • 2018
  • With the increase in industrialization and urbanization, growing demand has enhanced rate of new constructions and old demolitions. To avoid serious environmental impacts and hazards recycled concrete aggregates (RCA) is being adopted in all over the world. This paper investigates successive recycled coarse aggregates (SRCA) in which old concrete made with RCA in form of concrete cubes was used. The cubes were crushed to prepare new concrete using aggregates from crushing of old concrete, used as SRCA. The mechanical behavior of concrete was determined containing SRCA; the properties of SRCA were evaluated and then compared with natural aggregates (NA). Replacement of NA with SRCA in ratio upto 100% by weight was studied for workability, mechanical properties and microstructural analysis. It was observed that with the increase in replacement ratio workability and compressive strength decreased but in acceptable limits so SRCA can be used in low strength concretes rather than high strength concrete structures.

침탄처리된 엔진 부품의 미세조직학적 파손원인 분석 (Failure Analysis of the Carburized Engine Parts by Microstructural Observation)

  • 손경숙;이상기;정인상
    • 열처리공학회지
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    • 제18권2호
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    • pp.83-90
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    • 2005
  • Failure cause of the fractured engine parts was analyzed by microstructural observation. These parts were failed far earlier than the expected service life. By the stereoscope and SEM examinations of the fractured surface, the fracture modes have been identified as wear and fatigue failure. From the observation of microstructure and microhardness measurements of the failed gears, the probable cause for failures are internal oxidation during using and retained austenite and carbide networks due to heat-treatment, respectively. These defected structures at near surface contributed to the wear and fatigue failure.

열간압연중 발생하는 미세조직 변화에 관한 연구 (A Study On The Microstructural Evolution In Hot Rolling)

  • 조현중;김낙수
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 1995년도 추계학술대회논문집
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    • pp.16-29
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    • 1995
  • A full three-dimensional thermo-coupled rigid-viscoplastic finite element method and the currently developed microstructural evolution system which includes semi-empirical mathematical equations suggested by different research groups were used together to form an integrated system of process and microstructure simulation of hot rolling. The distribution and time history of thermomechanical variables such as temperature, strain, strain rate, and time during pass and between passes were obtained FEM analysis of multipass hot rolling processes. Then distribution of metallurgical variables were calculated successfully on the basis of instantaneous thermomechanical data. For the verification of this method the evolution of microstructure in plate rolling and shape rolling was simulated and their results were compared with the data available in literature. Consequently, this approach makes it passible to describe the realistic evolution of microstructure by avoiding the use of erroneous average value and can be used in CAE of multipass hot rolling.

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미세구조 분석을 이용한 저밀도 결함을 가진 GaN계 반도체 연구 (The study of GaN-based semiconductors with low-defect density by microstructural characterization)

  • 조형균
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2003년도 하계학술대회 논문집 Vol.4 No.1
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    • pp.424-427
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    • 2003
  • We have investigated the microstructural analysis of epitaxial lateral overgrowth (ELO), pendeoepitaxy (PE), and superlattice structures used as technology for the reduction of structural defects like dislocation in nitride semiconductors using transmission electron microscopy. We confirmed that the regrowth process such as ELO and PE is very effective technique on the reduction of threading dislocation (less than $10^6/cm^2$) in the specific area. However, to decrease the defect density in the whole nitride films and the suppress the generation of defect by regrowth, we should find the optimized conditions. Besides, the process using double PE and AlGaN/GaN superlattice structure showed no effect on the defect reduction up to now.

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기계적 합금화 방법에 의한 Cu-C계 복합금속분말의 제조 및 미세구조 제어 특성 (Synthesis and Microstructural Characterization of Cu-C Composite Metal Powder by Mechanical Alloying)

  • 이광민
    • 한국분말재료학회지
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    • 제4권1호
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    • pp.42-47
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    • 1997
  • It was investigated whether mechanical alloying (MA) processing could be more effective to the formation of metallic composite powder in Cu-C system. Elemental powder mixtures of Cu-70vo1.%C were mechanically alloyed with an attritor in an argon atmosphere and microstructural evolution was examined by X-ray diffraction analysis, scanning electron microscopy and transmission electron microscopy. It has been found that even with the high volume fraction of immiscible graphite in Cu-C system, the refinement with a few ten nanometer size as well as the highly uniform distribution of copper phases have been achieved by the MA processing.

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미세조직기반 구성모델을 이용한 고크롬강의 크리프 거동 해석 (Creep Behavior Analysis of High Cr Steel Using the Constitutive Model Based on Microstructure)

  • 윤승채;서민홍;백경호;김성호;류우석;김형섭
    • 소성∙가공
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    • 제13권2호
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    • pp.160-167
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    • 2004
  • In order to theoretically analyze the creep behavior of high Cr steel at $600^{\circ}C$, a unified elasto-viscoplastic constitutive model based on the consideration of dislocation density is proposed. A combination of a kinetic equation describing the mechanical response of a material at a given microstructure in terms of dislocation glide and evolution equations for internal variables characterizing the microstructure provides the constitutive equations of the model. Microstructural features of the material such as the grain size and spacing between second phase particles are directly implemented in the constitutive equations. The internal variables are associated with the total dislocation density in a simple model. The model has a modular structure and can be adjusted to describe a creep behavior using the material parameters obtained from uniaxial tensile tests.

질화알루미늄과 금속간 계면접합에 관한 연구: 계면반응과 미세구조 형성이 접합체 강도에 미치는 영향 (Joining of AIN Ceramics to Metals: Effect of Reactions and Microstructural Developments in the Bonded Interface on the Joint Strength)

  • 박성계
    • 한국분말재료학회지
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    • 제4권3호
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    • pp.196-204
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    • 1997
  • Joining of AIN ceramics to W and Cu by active-metal brazing method was tried with use of (Ag-Cu)-Ti alloy as insert-metal. Joints were produced under various conditions of temperature, holding time and Ti-content in (Ag-Cu) alloy Reaction and microstructural development in bonded interface were investigated through observation and analysis by SEM/EDS, EPMA and XRD. Joint strengths were measured by shear test. Bonded interface consists of two layers: an insert-metal layer of eutectic Ag- and Cu-rich phases and a reaction layer of TiN. Thickness of reaction layer increases with bonding temperature, holding time and Ti-content of insert-metal. It was confirmed that the growth of reaction layer is a diffusion-controlled process. Activation energy for this process was 260 KJ/mol which is lower than that for N diffusion in TiN. Maximum shear strength of 108 MPa and 72 MPa were obtained for AIN/W and AIN/Cu joints, respectively. Relationship between processing variables, joint strength and thickness of reaction layer was also explained.

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계면활성제/1-Hoxanol/물 혼합물의 상태도와 전기 전도도에 관한 연구

  • 오성근;김종득
    • 대한화장품학회지
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    • 제12권1호
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    • pp.34-61
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    • 1986
  • The microstructural transitions of aqueous micellar solutions of cetyltrime-thylammonium bromide and sodiumdodecyl sulfate by adding 1-hexanol were investigated, measuring the concentrations of equilibrated phases and the electrical conductivities at the low concentrations of surfactants, where the solobilities of 1-hexanol varied significantly, at 3$0^{\circ}C$ and 45$^{\circ}C$. Ternary phase diagrams of multiphase regions, constructed by liquid chromatography analysis and by counting the number of phase of samples, consisted of one three-phase region and three two-phase regions. One of the two-phase regions was found to equilibrate an aqueous micellar solution and a liquid crystal, and had a critical point between them. Near this region, the solubility curve varied abruptly, and the isotropic solution turned birefrigent. The conductivities of the single phase regions above the critical point increased up to a certain point as 1-hexanol added, and then decreased, representing the microstructural transition at the supercritical region. Further, the solubility of 1-hexanol in aqueous micellar solution was found to increase as temperature and the number of hydrophilelipophile balance of surfactants increase.

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The Effect of Cr and Mo Additions on the Improvement in Microstructural Homogeneity and Mechanical Properties of Ni-containing P/M Steels

  • Wu, Ming-Wei;Hwang, Kuen-Shyang;Huang, Hung-Shang
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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    • pp.931-932
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    • 2006
  • The microstructures of Ni-containing P/M steels produced by admixed powders or diffusion alloyed powders are usually heterogeneous. To improve the microstructure homogeneity, the effects of Mo and Cr additions in the prealloyed powder form were examined. The results showed that the microstructural homogeneity was improved and superior mechanical properties were achieved with increases in the alloy content, particularly for the Cr. Such a beneficial effect was attained due to the reduction of the repelling effect between Ni and C, as was demonstrated through thermodynamic analysis using the Thermo-Calc software.

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A Study of Debinding Behavior and Microstructural Development of Sintered Al-Cu-Sn Alloy

  • Kim, J.S.;Chang, I.T.;Falticeanu, C.L.;Davies, G.J.;Jiang, K.C.
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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    • pp.722-723
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    • 2006
  • A new method has been developed to fabricate microcomponents by a combination of photolithography and sintering of metallic powder mixtures, without the need for compression and the addition of Mg. This involves (1) the fabrication of a micromould, (2) mould filling of the powder/binder mixture, (3) debinding and (3) sintering. The starting powdered materials consisted of a mixture of aluminium powder(average size of 2.5 um) and alloying elemental powder of Cu and Sn(less than 70nm), at appropriate proportions to achieve nominal compositions of Al-6wt%Cu, Al-6wt%Cu-3wt%Sn. This paper presents detailed investigation of debinding behaviour and microstructural development.

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