• Title/Summary/Keyword: microscopic analysis

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AN EXPERIMENTAL STUDY ON THE ALTERATIONS OF ION-BEAM-ENHANCED ADHESIONS ON A VARIETY OF CERAMIC-METAL INTERFACES (이온선 혼합법이 도재-금속 계면 변화에 미치는 영향에 관한 실험적 연구)

  • Chung Keug-Mo;Park Nam-Soo;Woo Yi-Hyung
    • The Journal of Korean Academy of Prosthodontics
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    • v.30 no.2
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    • pp.135-154
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    • 1992
  • This study was performed to analyze bond strength, the alterations of the interfaces between metal films which are populary used and considered to contribute to the chemical reaction with porcelain, according to constant ion- beam- mixing, and the relation between interfacial chemical reactions and bond strength in metal/porcelain specimens. For this study, three seperate metals : selected-gold, indium and tin were chosen ; each to be bonded to a seperate body porcelain. Bonding occurs when the metal is deposited to the body porcelain using a vacuum evaporator. The vacuum evaporator used $10^{-5}\sim10^{-6}$ Torr vacuum states for the evaporation of various metals (Au, Sn, In). Ion-beam-mixing of the porcelain/metal interfaces caused reactions when the Ar+ was implanted into thin films using a 80 KeV accelerator. These ion-beam-mixed specimens were then compared with an unmixed control group. An analysis of bond strength and ionic changes between the the metal and porcelain was performed by electron spectroscopy of chemical analysis (ESCA) and scratch test. The finding led to the following conclusions : 1. Light microscopic views of the scratch test : The ion-beam-mixed Au/porcelain specimen showed narrower scratched streams than the unmixed specimen. However, the Sn/porcelain, In/porcelain specimens showed no differences in the two conditions. 2. Acoustic emissions in scratch tests : The ion-mixed Au/porcelain, In/porcelain specimens showed signals closer to the metal/porcelain interfaces than unmixed specimens. Conversely, the ion-mixed Sn/porcelain specimen showed more critical signals in superficial portions than unmixed specimens. 3. After ion- beam-mixing, the Au/porcelain specimen showed apparently increased bond strength, and the In/porcelain specimen showed very slightly increased bond strength. However, the Sn/porcelain specimen showed no differences between ion mixed specimen and the unmixed one. 4. ESCA analysis : The ion-beam-mixed Au/porcelain specimen showed a higher peak separated value (4.3eV) than that of the unmixed specimen(3.65eV), the ion-beam-mixed In/porcelain specimen showed a higher peak separated value (9.43eV) than that of the unmixed specimen(7.6eV) and the ion-beam-mixed Sn/porcelain specimen showed a higher peak separated value (8.79eV) than that of the unmixed specimen(8.5eV). 5. Interfacial changes were observed in the ion-mixed Au/porcelain, In/porcelain and Sn/porcelain specimens. Especially, significant interfacial changes were measured in the ion- mixed Sn/porcelain specimen. Tin dioxide(SnO2) and a combination of pure tin and tin dioxide (Sn+SnO2) were produced. 6. In the Au/porcelain specimen, the interfacial chemical reaction showed increased bond strength between gold and porcelain substrate. But, in the In/porcelain, Sn/porcelain specimens, interfacial chemical reactions did not affected the bond strength between metal and porcelain substrate. Especially, bonding strength on the ion mixed Sn/porcelain specimen showed the least amount of difference.

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An Analysis on Signal Control Efficiency in a Three-Leg Intersection Adopting Pedestrian Push-Button System Following Pedestrian volume (3지 교차로에서 보행자 교통량에 따른 보행자작동신호기를 이용한 신호제어효율에 관한 분석)

  • Kim, Eung-Cheol;Cho, Han-Seon;Jung, Dong-Woo;Kim, Hyoung-Soo
    • International Journal of Highway Engineering
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    • v.11 no.3
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    • pp.121-128
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    • 2009
  • This study has proposed the signal operating system to use both semi-actuated signal control and pedestrian push-button as a way to make up for the problems of 3 leg intersections which are operated inefficiently in the signal operation, one of the methods of traffic operations. In case of the semi-actuated signal control, it can reduce delay inside the intersection by serving to uncongested traffic on the main road where there is not much traffic volume on the secondary road and push-button signal can reduce unnecessary waiting time it could happen to vehicles by operating it though there is no pedestrian. Quantitative analysis was tried regarding the average delay reduction per vehicle using VISSIM, microscopic simulation program regarding how much effect it has compared with the existing signal control system and semi-actuated signal control system when the above two advantages are collected. The field test was performed for one three-leg intersection of Incheon. According to respectively signal control method pedestrian traffic changed and executed a sensitivity analysis. The result which compares the average delay time per a vehicle of scenarios, the signal control method of using the pedestrian push-button system in comparison with the fixed signal control method showed to decrease effect of a minimum 3.7 second (10%), a maximum 5.8 second (16%). When the pedestrian traffic volume was 20% or less of the measurement traffic volume, The signal control method of using the pedestrian push-button system appeared to be more efficient the semi-actuated signal control with object intersection.

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Study on Characteristics of Corrosion Products Generated in Iron Artifacts after Conservation Treatments (보존처리 후 철제유물에 생성된 부식물 특성 연구)

  • Jeong, Ji-Hae;Yang, Hee-Jae;Ha, Jin-Uk
    • Journal of Conservation Science
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    • v.29 no.4
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    • pp.297-309
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    • 2013
  • Iron objects become corroded at fast speed from the moment when they are excavated, so it is needed to control corrosion through processes of conservation treatment. However, re-corrosion mostly takes place in excavate iron objects, although they have already gone through the process of conservation treatment, and it is more difficult to carry out the second conservation treatment of re-corroded excavated iron objects than the first conservation treatment, and it requires a longer period of time to treat them as well. In this study, aims to discover factors of re-corrosion by scientifically analyzing corrosion products generated during the process of storage after the process of conservation treatment. The finished on conservation treatment of the iron artifacts, which were unearthed from three ancient site in Gyeongju by using the same conservation method between 2002 and 2009, re-corrosion condition observed on the packaging-iron artifacts. Focused on 9 target forged iron artifacts among them, this study analyzed the physical changes by mass measurement, naked-eye and microscopic observations and the chemical changes by SEM-EDS, XRD, IC and ICP analysis. The results show that the yellowish brown corrosion products formed on the facing surface of part dropped from the artifacts had different associated forms but acicular shape. In addition, the acicular shape became clearer as the color changed from red to yellowish brown. According to the process when the conservation treatment was completed, the mass of the artifacts increased in proportion to the corrosion products and the chloride ion ($Cl^-$) concentration had a tendency to increase relatively. ${\beta}$-FeOOH (akaganeite) was confirmed in the XRD analysis for the corrosion products of all the collected samples. As a result of ICP analysis, $Na^+$ and $Ca^{2+}$ components were confirmed.

The Effect of Triamcinolone Injection on the Vocal cord during Laryngeal Microsurgery in the Patient of the Vocal Polyp (성대용종환자에서 후두미세수술시에 수술부위에 Triamcinolone 국소주입이 음성에 미치는 영향에 대한 연구)

  • Yoo, Jun;Oh, Kyung Ho;Yoon, Hee Chul;Lee, Doh Young;Woo, Jeung soo;Baek, Seung Kuk;Jung, Kwang Yoon;Kwon, Soon Young
    • Journal of the Korean Society of Laryngology, Phoniatrics and Logopedics
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    • v.26 no.2
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    • pp.122-126
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    • 2015
  • Background and Objective : Laryngeal microscopic surgery (LMS) is popular method to treat for vocal polyp. There is not always the improvement of the voice after operation. Many methods have been developed for better outcome of the surgery. The purpose of this study is to investigate the effect of the triamcinolone injection at vocal cord during LMS. Materials and Methods : The medical records of 28 patients, received LMS under diagnosis of vocal polyp, were retrospectively reviewed. The patients were divided into two groups depending on whether triamcinolone injected or not (case group : Triamcinolone-injected group, control group : Triamcinolone-not injected group). The quality of voice was evaluated by GRBAS scale, fundamental frequency (Fo), jitter, shimmer and NHR (Noise to harmonic ratio) at previous operation, 4 weeks after operation, 8 weeks after operation. Each voice analysis factor was compared between case group and control group by Independent t-test. Results : The mean differences of each voice analysis factor. The mean difference of Jitter, Shimmer, NHR in case group were lower than in control group, and mean difference of GRBAS scale in case group were higher than in control group. These differences were not significant (p>0.05). Conclusion : Though there was a tendency of better voice outcome in patients of triamcinolone-injection, it may not be concluded that the triamcinolone injection is helpful for better voice outcome in surgery of vocal polyp due to statistical insignificance.

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An Empirical Study on the Difference in Price Elasticity by Colors in the Chinese Mobile Phone Market (중국 핸드폰시장의 색상에 따른 가격탄력성 차이에 대한 실증연구)

  • Kwak, Youngsik;Hong, Jaewon;Pak, JiYoung
    • Journal of Platform Technology
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    • v.6 no.2
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    • pp.10-18
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    • 2018
  • The purpose of this study was to empirically analyze relations between color changes in the product specification and demand changes with price elasticity in the Chinese mobile phone market. In previous studies on price elasticity, the usual analysis units were product categories or SBU within a given product category. Unlike them, the this study set an analysis unit of price elasticity to focus on colors, which are investigated in the research fields of experiential marketing, aesthetic marketing, and cognitive psychology. Actual sales data according to the mobile phone price changes by the color were based on the sales volume of a sales agency at China's largest B2C site. The findings were as follows: first, price elasticity according to the six colors was higher than the absolute value of 1, which means that demands made flexible reactions to price changes. Secondly, there were differences in price elasticity according to the colors. Aroma white color made the smallest increase in sales volume at the same price discount, whereas diamond color made the biggest increase in sales in the same price discount scope. These findings indicate that more profit can be generated in mobile phone sales in China by setting different price discount or increase rates according to colors or producing different amounts of mobile phones according to colors. Distributors or sales agents can have a chance for higher profit by ordering and selling mobile phones in certain colors than others from mobile phone manufacturers. The academic findings indicates that there are differences in preference and price elasticity according to colors under the mobile phone category in the Chinese market, which means that the present study made an academic contribution by proposing a microscopic analysis unit for product price elasticity and expanding its concept.

Gibberellin A7 production by Aspergillus tubingensis YH103 and cultural characteristics of endophytic fungi isolated from Tetragonia tetragonoides in Dokdo islands (독도 번행초에서 분리된 내생균류의 배양적 특성과 Aspergillus tubingensis YH103의 gibberellin A7의 생산)

  • You, Young-Hyun;Park, Jong Myong;Lim, Sung Hwan;Kang, Sang-Mo;Park, Jong-Han;Lee, In-Jung;Kim, Jong-Guk
    • Korean Journal of Microbiology
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    • v.52 no.1
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    • pp.32-39
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    • 2016
  • Coastal plant species Tetragonia tetragonoides (Pall.) Kuntze native to the Dokdo islands was sampled and then 17 endophytic fungi were purely isolated based on morphological differences. The fungal isolates were characterized by their growth properties under NaCl concentration or pH gradient. Culture filtrates of the 17 fungal isolates were treated to Waito-c rice (WR) seedlings for verifying plant growth-promoting activity. As the results, YH103 strain showed the highest plant growth-promoting activity among them. Phylogenetic analysis of the isolates was done by the maximum likelihood method based on partial internal transcribed spacer region (ITS region: contaning ITS1, 5.8S, and ITS2), beta-tubulin (BenA), and calmodulin (CaM) gene sequences. Chromatographic analysis of the strain YH103 culture filtrate showed the existence of gibberellins ($GA_4$, $GA_7$, $GA_8$, and $GA_{19}$). Finally, the strain YH103 was identified as Aspergillus tubingensis by microscopic observation and molecular analysis and, to our knowledge, this is the first report of GAs producing A. tubingensis.

Analysis of the influence of combined use of ferronickel slag fine powder and admixture on VR sewage pipe strength development (페로니켈슬래그 미분말 및 혼화재의 복합사용이 VR 하수관 강도발현에 미치는 영향분석)

  • Nam, Sang-Koo;Chung, Tae-Jun;Jo, Seol-Ah;Yoo, Jeong-Hwan;Park, Sang-Soon
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.6 no.3
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    • pp.214-221
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    • 2018
  • In this paper, the effects of ferronickel slag powder and admixture on the strength of VR sewer pipe were analyzed. the substitution rate was tested as a variable, and the strength development was studied through the flexural strength, compressive strength and using SEM microscopic analysis. bending strength, compressive strength results and micro analysis using SEM showed the correlation in each case. the substitution rates were 20% and 30% relative to the mass of the OPC respectively, and were substituted according to a constant ratio of ferronickel slag fine powder and mixture. when the substitution ratio was 20%, the strength development was excellent. also, bending strength and compressive strength were the best when the ferronickel slag fine powder, quicklime, gypsum and calcium chloride were used as the admixture, dense microstructural patterns appeared. the possibility of progressive strength development is shown after 28 days.

Analysis on the Characteristics of Academic Achievement About 'properties of matter' and 'change of matter': Focusing on the Results of the National Assessment of Educational Achievement (NAEA) in the 2009 Revised Curriculum (물질의 성질 및 물질의 변화 영역에서 중학생들의 학업성취 특성 분석 : 2009 개정 교육과정 시기 국가수준 학업성취도 평가 결과를 중심으로)

  • Jongho, Baek;Wonho, Choi
    • Journal of the Korean Chemical Society
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    • v.66 no.6
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    • pp.493-508
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    • 2022
  • Chemistry is the subject which includes properties, change, and composition of matter. Chemistry has the system which explains observable properties and change with microscopic level, it explains them using scientific theory and laws. In the national-level curriculum, the properties and changes of matter are continuously dealt with from elementary school to high school, and the curriculum are organized so that students could strengthen their understanding about matter. In other words, understanding of the properties and changes of matter is the base to explain everyday life with the view of chemistry, and these two are classified as domains of chemistry in the 2015 revised science curriculum. In this study, we confirmed students' understanding about properties of matter and change of matter, through the analysis about results of the National Assessment of Educational Achievement (NAEA). For that purpose, this study analyzed the 12 items about properties of matter, and 19 items about change of matter, which were used in the NAEA from 2015 to 2019. According to the results of classifying and analyzing questions according to the core concept, the understanding about the two domains significantly changed between the proficient achievement-level students and basic achievement-level students. Depending on the achievement-level, there was a difference in explaining the phenomenon by using the perspective of particles, and by associating scientific concepts and models, or there was a difference in understanding the inquiry related to these two domains. Based on this analysis, this study discussed some implications to be improved on teaching-learning for 'properties of matter', and 'change of matter'.

Estimation of Incident Detection Time on Expressways Based on Market Penetration Rate of Connected Vehicles (커넥티드 차량 보급률 기반 고속도로 돌발상황 검지시간 추정)

  • Sanggi Nam;Younshik Chung;Hoekyoung Kim;Wonggil Kim
    • The Journal of The Korea Institute of Intelligent Transport Systems
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    • v.22 no.3
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    • pp.38-50
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    • 2023
  • Recent advances in artificial intelligence (AI) technology have enabled the integration of AI technology into image sensors, such as Closed-Circuit Television (CCTV), to detect specific traffic incidents. However, most incident detection methods have been carried out using fixed equipment. Therefore, there have been limitations to incident detection for all roadways. Nevertheless, the development of mobile image collection and analysis technology, such as image sensors and edge-computing, is spreading. The purpose of this study is to estimate the reducing effect of the incident detection time according to the introduction level of mobile image collection and analysis equipment (or connected vehicles). To carry out this purpose, we utilized data on the number of incidents collected by the Suwon branch of the Gyeongbu expressway in 2021. The analysis results showed that if the market penetration rate (MPR) of connected vehicles is 4% or higher for two-lane expressway and 3% or higher for three-lane expressways, the incident detection time was less than one minute. Furthermore, if the MPR is 0.4% or higher for two-lane expressways and 0.2% or higher for three-lane expressways, the incident detection time decreased compared to the average incident detection time announced by the Korea Expressway Corporation for both two-lane and three-lane expressways.

Breast Cancer Histopathological Image Classification Based on Deep Neural Network with Pre-Trained Model Architecture (사전훈련된 모델구조를 이용한 심층신경망 기반 유방암 조직병리학적 이미지 분류)

  • Mudeng, Vicky;Lee, Eonjin;Choe, Se-woon
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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    • 2022.05a
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    • pp.399-401
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    • 2022
  • A definitive diagnosis to classify the breast malignancy status may be achieved by microscopic analysis using surgical open biopsy. However, this procedure requires experts in the specializing of histopathological image analysis directing to time-consuming and high cost. To overcome these issues, deep learning is considered practically efficient to categorize breast cancer into benign and malignant from histopathological images in order to assist pathologists. This study presents a pre-trained convolutional neural network model architecture with a 100% fine-tuning scheme and Adagrad optimizer to classify the breast cancer histopathological images into benign and malignant using a 40× magnification BreaKHis dataset. The pre-trained architecture was constructed using the InceptionResNetV2 model to generate a modified InceptionResNetV2 by substituting the last layer with dense and dropout layers. The results by demonstrating training loss of 0.25%, training accuracy of 99.96%, validation loss of 3.10%, validation accuracy of 99.41%, test loss of 8.46%, and test accuracy of 98.75% indicated that the modified InceptionResNetV2 model is reliable to predict the breast malignancy type from histopathological images. Future works are necessary to focus on k-fold cross-validation, optimizer, model, hyperparameter optimization, and classification on 100×, 200×, and 400× magnification.

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