• Title/Summary/Keyword: micron size

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Texture Formation of Eletroplated Nickel and Nickel Alloy on Cu Substrate (구리 기판에 전착시킨 니켈과 니켈합금의 집합조직 형성)

  • Kim, Jae-Geun;Lee, Sun-Wang;Kim, Ho-Jin;Hong, Gye-Won;Lee, Hee-Gyoun
    • Progress in Superconductivity
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    • v.7 no.2
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    • pp.145-151
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    • 2006
  • Nickel and nickel-tungsten alloy were electroplated on a cold rolled and heat treated copper(Cu) substrate. 4 mm-thick high purity commercial grade Cu was rolled to various thicknesses of 50, 70, 100 and 150 micron. High reduction ratio of 30% was applied down to 150 micron. Rolled texture was converted into cube texture via high temperature heat treatment at $400-800^{\circ}C$. Grain size of Cu was about 50 micron which is much smaller compared to >300 micron for the Cu prepared using smaller reduction pass of 5%. 1.5 km-long 150 micron Cu was fabricated with a rolling speed of 33 m/min and texture of Cu was uniform along length. Abnormal grain growth and non-cube texture appeared for the specimen anneal above $900^{\circ}C$. 1-10 micron thick Ni and Ni-W film was electroplated onto an annealed cube-textured Cu or directly on a cold rolled Cu. Both specimens were annealed and the degree of texture was measured. For electroplating of Ni on annealed Cu, Ni layer duplicated the cube-texture of Cu substrate and the FWHM of in plane XRD measurement for annealed Cu layer and electroplated layer was $9.9^{\circ}\;and\;13.4^{\irc}$, respectively. But the FWHM of in plane XRD measurement of the specimen which electroplated Ni directly on cold rolled Cu was $8.6^{\circ}$, which is better texture than that of nickel electroplated on annealed Cu and it might be caused by the suppression of secondary recrystallization and abnormal grain growth of Cu at high temperature above $900^{\circ}C$ by electroplated nickel.

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A Study on the Fabrication of 1W Power Amplifier for IMT2000 Repeater Using Nonlinear Analysis (비선형 해석법을 이용한 IMT2000 중계기용 1W 전력증폭기 제작 연구)

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    • Journal of the Institute of Electronics Engineers of Korea TE
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    • v.37 no.2
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    • pp.83-90
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    • 2000
  • A simple low-cost and small size 1.88-198 GHz Band RF power amplifier module is developed for IMT2000 repeater. The power amplifier consists of two stage amplifiers that the first stage amplifier is drive amplifier using discrete type P-HEMT (ATF-34143, 800 micron gate width, Agilent Technologies) and the second is power amplifier with 300Bm 1dB gain compression point using GaAs FET(EFA240D-SOT89, 2400 micron gate width, Excelics Semiconductor). this power amplifier module feature a 29.5dBm 1dB gain compression point, 29.5dB gain, 42dBm 3rd order intercept point(OIP3) and -10dB/-l2dB input/output return loss over the 1880-1980 MHz. This PA module is fully integrated using MIC technology into a small size and design by full nonlinear design technologies. The dimensions of this PA module are 42(L) $\times$ 34(W) mm.

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Laser micromachining of micron-size aperture for electron beam microcolumn application using the piezo-switched Nd:YAG laser (Piezo Q-Switched Nd:YAG 레이저에 의한 초미니 전자빔 장치용 Micron-Size Aperture의 레이저 미세가공)

  • 안승준;김대욱;김호섭;최성수
    • Journal of the Korean Vacuum Society
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    • v.8 no.4A
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    • pp.456-460
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    • 1999
  • Experimental studies of laser micromachining on Mo diaphragm using piezo Q-switched Nd:YAZ laser have been performed. Application of miniaturized micorcolumn electron gun arrays as a potential electron beam lithography or portable mini-scanning electron microscope (SEM) application have recently extensively examined. The conventional microcolumn fabrication technique would give a limitation on the minimization of aberration, In this paper, we obtained 20~30 $\mu \textrm m$aperture of laser micromachining on Mo diaphragm using piezo Q-swithed Nd:YAG laser. The geometrical figures, such as the diameter and the preciseness of the drilled aperture are dependent upon the total energy of the laser pulse train, laser pulse width, and the diameter of laser spot in addition to the materials-dependent parameters.

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Nano-sized $Gd_{2}O_{3}:Eu$ phosphor particles of high brightness

  • Lee, Chang-Hee;Roh, Hyun-Sook;Kang, Yun-Chan;Park, Hee-Dong;Park, Seung-Bin
    • 한국정보디스플레이학회:학술대회논문집
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    • 2003.07a
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    • pp.791-794
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    • 2003
  • To synthesize $Gd_{2}O_{3}:Eu$ phosphor powder of nano size and high luminescence efficiency under UV (ultraviolet) and VUV (vacuum ultraviolet) light, organic additives such as citric acid and ethylene glycol and $Na_{2}CO_{3}$ flux were introduced in large-scale spray pyrolysis and critical conditions for forming nano-sized particles were investigated. The $Gd_{2}O_{3}:Eu$ phosphor particles prepared from solutions with organic additives such as citric acid and ethylene glycol had micron size and spherical shape. However, the particles prepared from polymeric precursor solution with $Na_{2}CO_{3}$ flux had nano size and non-aggregation characteristics. The as-prepared spherical particles with micron size turned into nano-sized particles during post-treatment by recrystallization process. The nano-sized $Gd_{2}O_{3}:Eu$ phosphor particles showed higher brightness than the commercial $Y_2O_3:Eu$ phosphor product under both UV light of 254nm and VUV light of 147 nm.

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Synthesis and Electrochemical Performance of Mesoporous Hollow Sphere Shape LiMn2O4 using Silica Template (실리카 템플레이트를 이용하여 다공성 중공형태를 갖는 LiMn2O4 합성 및 전기화학적 특성 연구)

  • Ryu, Seong-Hyeon;Ryu, Kwang-Sun
    • Journal of the Korean Electrochemical Society
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    • v.14 no.3
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    • pp.184-190
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    • 2011
  • $LiMn_2O_4$ with mesoporous hollow sphere shape was synthesized by precipitation method with silica template. The synthesized $LiMn_2O_4$ has nanosized first particle and mesoporous hollow sphere shape. Silica template was removed by chemical etching method using NaOH solution. When the concentration of NaOH solution was increased, first particle size of manganese oxide was decrease and confirmed mesoporous hollow shpere shape. X-ray diffraction(XRD) patterns revealed that the synthesized samples has spinel structure with Fd3m space group. In case the ratio of silica and maganese salt increased, the size of first particles was decreased. The tetragoanal $LiMn_2O_4$ with micron size was synthesized at ratio of silica and manganese salt over 1 : 9. The prepared samples were assembled as cathode materials of Li-ion battery with 2032 type coin cell and their electrochemical properties are examined by charge-discharge and cyclic performance. Electrochemical measurements show that the nano-size particles had lower capacity than micron-size particles. But, cyclic performance of nano-size particles had better than that of micron-size particles.

Discovery of a New Mechanism of Dust Destruction in Strong Radiation Fields and Implications

  • Hoang, Thiem;Tram, Le Ngoc;Lee, Hyseung;Ahn, Sang-hyeon
    • The Bulletin of The Korean Astronomical Society
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    • v.44 no.1
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    • pp.44.3-44.3
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    • 2019
  • Massive stars, supernovae, and kilonovae are among the most luminous radiation sources in the universe. Observations usually show near- to mid-infrared (NIR-MIR, 1-5~micron) emission excess from H II regions around young massive star clusters (YMSCs) and anomalous dust extinction and polarization towards Type Ia supernova (SNe Ia). The popular explanation for such NIR-MIR excess and unusual dust properties is the predominance of small grains (size a<0.05micron) relative to large grains (a>0.1micron) in the local environment of these strong radiation sources. The question of why small grains are predominant in these environments remains a mystery. Here we report a new mechanism of dust destruction based on centrifugal stress within extremely fast rotating grains spun-up by radiative torques, namely the RAdiative Torque Disruption (RATD) mechanism, which can resolve this question. We find that RATD can destroy large grains located within a distance of ~ 1 pc from a massive star of luminosity L~ 10^4L_sun and a supernova. This increases the abundance of small grains relative to large grains and successfully reproduces the observed NIR-MIR excess and anomalous dust extinction/polarization. We show that small grains produced by RATD can also explain the steep far-UV rise in extinction curves toward starburst and high redshift galaxies, as well as the decrease of the escape fraction of Ly-alpha photons observed from HII regions surrounding YMSCs.

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Development of wet-sampler for collection and fractionation of micron-sized particles (마이크로 입자의 습식 수집 및 분획 장치 개발)

  • Eum, Chul-Hun;Kang, Dong-Young;Lee, Seung-Ho
    • Analytical Science and Technology
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    • v.24 no.6
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    • pp.429-434
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    • 2011
  • In this study, a wet-sampler was developed for collection in water and simultaneous fractionation of micron-sized particles (e.g., pigment, airborne, etc.). In this new device, three cylinders (partially filled with water) through which air was forced to pass for sample collection are connected in a series. Particles of different sizes are collected in different cylinders, allowing simultaneous fractionation. An uniqueness of this new device is that it does not use any membrane filter. Microparticles are collected directly in cylinders filled partially with water. Also the particles are simultaneously fractionated within this device while they are being collected. The new device was employed for collection of airborne particles. The collected airborne particles were fractionated by using sedimentation field-flow fractionation, SdFFF), and observed with an optical microscopy (OM) for size and shape analysis. Also AAS and ICP-AES were used for composition analysis of the airborne particles. It is expected that the new device is applicable to collection and analysis of size distribution of various types of microparticles.

Recovery sub micron-graphitized carbon from oil fly ash

  • Hsieh, Ya-Min;Tsai, Min-Sing;Tsai, Shang-Lin
    • Proceedings of the IEEK Conference
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    • 2001.10a
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    • pp.633-637
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    • 2001
  • Oil fly ash is known as one source of raw materials from which vanadium and nickel metals can be recovered. The current recovery process of valuable metals from oil fly ash is mainly the hydrormetallurgy one. Nevertheless, a great amount about 50~80%, of unburned carbon remains as byproduct after hydrormetallursy process. In Taiwan, if hydrormetallursy processes have proceeded, it can be estimated that the annual production of unburned carbon is 25 thousand tons. From the viewpoint of resource recycling, this study is a preliminary study and investigates in recovery of sub micron- graphitized carbon from unburned carbon by a designed process. The designed process included the following steps: 1.selecting a portion with +400mesh size from unburned carbon; 2.treating the selected in ultrasonic waves; 3.using a 400mesh sieve to obtain the product which is under 400mesh; 4.Removal ash from the product. In regard to treatment by ultrasonic waves in the designed process, treating time of ultrasonic waves is a simple and only variance in this study. The results indicate that the production yields increase with the treating time of ultrasonic waves; the production yield in specific conditions of this study can reach about 23%, in which ash content in product is about 2.5%. According to results of SEM, TEM and XRD, the products from the designed process are flakes in shape, several microns in size and graphitized carbon in carbon crystal phase. Except to graphitized carbon, there are a little carbon blacks, which are graphite 2H in carbon crystal phase in the products. Conclusively, the designed process is possibly applicable, by which comes to the recovery of micron- graphitized carbon.

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