• Title/Summary/Keyword: microcracks

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A Study on Thermal Shock, Thermal Expansion and Thermal Cracking of Rocks under High Temperature (고온하에서 암석의 열충격, 열팽창 및 열파괴에 관한 연구)

  • 이형원;이정인
    • Tunnel and Underground Space
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    • v.5 no.1
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    • pp.22-40
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    • 1995
  • Thermomechanical characteristics of rocks such as thermal shock, thermal expansion, thermal cracking were experimentally investigaed using Iksan granite, Cheonan tonalite and Chung-ju dolomite to obtain the basic data for proper design and Chung-ju dolomite to obtain the basic data for proper design and stability analysis of underground structures subjected to temperature changes. The effect of thermal shock did not appear when the heating speed was under 3$^{\circ}C$/min. and there existed little difference between multi-staged cyclic heating and single-cycled heating. Thermal expansion of rocks was affected by mineral composition, crack porosity and the degree of thermal craking. In quartz-beraring multimineralic rocks such as Iksan granite and Cheonan tonalite, the thermal expansion coefficient increaseed continuously with temperature rise, but that of Chung-ju dolomite which was a monomineralic rock showed a constant value for the temperature above 250$^{\circ}C$, Chung-ju dolomite yielded the lowest critical threshold temperature(Tc) of 100$^{\circ}C$ and unstable thermal cracking was initiated above the new threshold temperature(Tc')of 300$^{\circ}C$. Above Tc' thermal cracks grew but they were not interconnected. Iksan granite showed closing of microcracks to the temperature of 100$^{\circ}C$, then expanded linearly to Tc of 200$^{\circ}C$. Above Tc, thermal cracking was initiated and progressed rapidly and almost all the grain boundaries were cracked at 600$^{\circ}C$. Cheonan tonalite also showed similar behavior to iksan granite except that Tc was 350$^{\circ}C$ and that thermal cracks propagated more rapidly. Thermal expansions calculated by Turner's equation were found to be valid in predicting the thermal expansion and cracking behavior of rocks.

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Aluminium Aluminium Titanate-Mullite Composites: Part2. Thermal Shock Resistance (Aluminium Aluminium Titanate-Mullite 복합체: Part2. 열충격성)

  • Kim, Ik-Jin;Gang, Won-Ho;Go, Yeong-Sin
    • Korean Journal of Materials Research
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    • v.4 no.2
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    • pp.206-212
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    • 1994
  • Aluminium titanate-mullite composites with varying chemical compositions were prepared by the stepwise hydrolysis of $Si(OC_2H_5)_4$, and $Ti(OC_2H_5)_4$in $AI_2O_3$ ethanolic colloidal dispersion. Sintered bodies having 20-50~01% mullite at $1600^{\circ}C$ for 2h have shown, that it is possible to develop an aluminium titanate with moderately high strength and low thermal expansion coefficient. This was obtained by inhibiting grain site of aluminium titanate with mullite and microcracks. Those with 80-70vol % aluminium titanate have excellent thermal shock resistance and has room-temperature strengths of 31-45MPa. The relation between thermal shock resistance and strength, Young's modulus, sound velocity and thermal expansion coefficient was discussed.

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Thermo-Mechanical Properties of Al2TiO5 Ceramics Stabilized with MgO and ZrO2 Additives (MgO와 ZrO2가 첨가된 Al2TiO5 세라믹의 열·기계적 물성)

  • Kim, Da-Mi;Kim, Hyung-Tae;Kim, Hyeong-Jun;Kim, Ik-Jin;Choi, Seong-Cheol;Kim, Yong-Chan;NamKung, Jung;Ryu, Sung-Soo
    • Journal of Powder Materials
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    • v.19 no.4
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    • pp.253-258
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    • 2012
  • The characteristics of $Al_2TiO_5$ ceramics were influenced by the additives and the heat treatment that controls the microcrack behavior at grain boundaries. The effect of additives on $Al_2TiO_5$ ceramics were investigated in terms of mechanical properties and thermal expansion at high temperature. The $Al_2TiO_5$ were synthesized at $1500^{\circ}C$, $1550^{\circ}C$ and $1600^{\circ}C$ for 2h by reaction sintering. The formation of $Al_2TiO_5$ phase was increased by additives that enhanced the volume of the microcrack that can lead to low thermal expansion. The mechanical properties of the stabilized $Al_2TiO_5$ ceramics were increased remarkably at $1100^{\circ}C$, $1200^{\circ}C$ and $1300^{\circ}C$ due to the oneset of mechanical healing of grain-bondary microcracks at a high temperature. The amount of microcrack was decreased at lower sintering temperature that causes the increase of mechanical properties at high temperature.

Effects of Injection and Temperature Variations on the Breakdown Pressure of Rocks (암석의 수압파쇄특성에 미치는 주입률과 온도의 영향)

  • 이찬구;송무영;최원학;장천중;이종옥
    • The Journal of Engineering Geology
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    • v.5 no.2
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    • pp.129-138
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    • 1995
  • To elucidate the effects of flow rate on the hydraulic fracturing property of andesite, the hydraulic fracturing tests were conducted under three flow rates. As the tests are conducted with 1ml/min, 2ml/min and 3 ml/min under the constant axial load of 40 kN, the breakdown pressures of andesite seem to be constant as 163kg/cm$^2$. The hydraulic fracturing tests were carried out under the temperatures of five stages to elucidate the effects of temperature variation on hydraulic fracturing property of granite. As the tests are carried out under the constant flow rate of 1.7ml/min, with the axial load of 40kN, the breakdown pressures of granite are 168kg/cm$^2$ at room temperature, and 124kg/cm$^2$ at 20$0^{\circ}C$. The breakdown pressure decreases about 25% than that of room temperature with increasing the temperature. Under the controlled flow rates, the initiation pressures of the microcracks of granite are well coincided with the breakdown pressures and these results are also confirmed by the levels of acoustic emission.

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Numerical Analysis of ECC Uniaxial Tension Behavior (ECC의 1축 인장 거동 해석)

  • Kim, Yun-Yong;Lee, Bang-Yeon;Kwon, Seung-Hee;Kim, Jeong-Su
    • Proceedings of the Korea Concrete Institute Conference
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    • 2008.04a
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    • pp.917-920
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    • 2008
  • ECC is a special kind of high performance cementititous composite which exhibits typically more than 2% tensile strain capacity by bridging microcracks at a crack section. Therefore, micromechanics should be adopted to obtain multiple cracking and strain hardening behavior. This paper propose a linear elastic analysis method to simulate the multiple cracking and strain hardening behavior of ECC. In an analysis, the stress-crack opening relation modified considering the orientation of fibers and the number of effective fibers is adopted. Furthermore, to account for uncertainty of materials and interface between materials, the randomness is assigned to the tensile strength(${\sigma}_{fci}$), elastic modulus($E_{ci}$), peak bridging stress(${\sigma}_{Bi}$) and crack opening at peak bridging stress(${\delta}_{Bi}$), initial stress at a crack section due to chemical bonding, (${\sigma}_{0i}$), and crack spacing(${\alpha}_cX_d$). Test results shows the number of cracking and stiffness of cracked section are important parameters and strain hardening behavior and maximum strain capacity can be simulated using the proposed method.

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AN IN-VITRO WEAR STUDY OF CEROMER AND HUMAN ENAMEL (Ceromer (Targis)에 의한 법랑질 마모에 관한 연구)

  • Kim, Jeong-Min;Lee, Sun-Hyung;Yang, Jae-Ho
    • The Journal of Korean Academy of Prosthodontics
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    • v.38 no.4
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    • pp.438-445
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    • 2000
  • The ideal restorative material should mimic the properties of the tissues it replaces. Dental composite resins have been used widely as restorative materials due to its advantages such as excellent esthetics and ease of manipulation. But inadequate wear resistance has been a major factor limiting the use of composite restorative materials. Improved manufacturing techniques have allowed the development of hybrid composites, with a greater percentage volume filler loading, which have improved physical and mechanical properties. However they are lacking in the study of wear resistance. The purpose of this study was to evaluate the wear of human enamel against ceromer by the use of a pin-on-disk type wear testers. Discs of ceromer(Targis ; lvoclar Vivadent, Amherst. NY) and discs of type III gold alloy as a control were used f9r test specimens. Intact cusp of premolar and molar were used for enamel specimens. The wear of enamel was determined by weigh-ing the cusp before and after each test, and the weight converted to volumes by average densi-ty of enamel. Surface profilometer was used to quantify wear of the ceromer and gold specimens. Vicker's hardness tester was used to evaluate the surface hardness of test specimens. The SEM was used to evaluate the wear surfaces The results were as follows; 1. Ceromer produced less enamel wear than gold(p<0.05) 2. The wear volume of ceromer was greater than that of gold(p<0.01) 3. The hardess of ceromer was lower than that of gold, but there was no correlation between the hardness and wear of the ceromer and gold. 4. SEM analysis revealed that there were many voids and microcracks in the wear tract of ceromer In gold group, many minute V-shaped grooves were examined.

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The Effect of Surface Treatment Systems on Chloride Penetration in Cracked Concrete (표면도장공법에 의한 균열부 콘크리트의 염소이온 침투제어 특성)

  • Chae, Gyu-Bong;Yoon, In-Seok;Lee, Chang-Soo
    • Proceedings of the Korea Concrete Institute Conference
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    • 2008.04a
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    • pp.525-528
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    • 2008
  • For well-constructed concrete, its service life is a long term and it has an enough durability performance. However, for cracked concrete, it is clear that cracks should be preferential channel for the penetration of aggressive substance such as chloride ions according to author's previous researches. In order to enhance the lifetime of cracked concrete, critical issues in the performance of the concrete is the risk of chloride-induced corrosion. Even though crack width can be reduced due to the high reinforcement ratio, the question is to which extend these cracks may jeopardize the durability of cracked concrete. If the size of crack is small, surface treatment system can be considered as one of the best options to extend the service life of concrete structures exposed to marine environment simply in terms of cost effectiveness versus durability performance. Thus, it should be decided to undertake an experimental study on the effect of different types of surface treatment system, which are expected to seal the concrete and the cracks to chloride-induced corrosion in particular. In this study, it is examined the effect of surfaced treated systems on chloride penetration through microcracks. Single surface treatments of penetrant or coating and double application were considered as an experimental variation. RCM (Rapid Chloride Migration) testing is accomplished to visualize chloride penetration via cracks.

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Performance Evaluation of a Connection Joint using a High-Ductility Concrete (고인성 콘크리트를 사용한 연결조인트의 성능평가)

  • Kim, Byeong-Ki;Kim, Jae Hwan;Yang, Il-Seung;Lee, Sang-Soo
    • Journal of the Korea Institute of Building Construction
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    • v.15 no.2
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    • pp.185-192
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    • 2015
  • Expansion joint is the essential element of the bridge in many cases. When the bridge faces chloride of preventing freezing on the surface of the bridge, the expansion joints is damaged significantly, thus this reduces service life and increases maintenance cost of the bridge. As a solution of this problem, new technology using high ductile materials for the joint without expansion joint was developed and in this research, crack control performance, preventing leaking after the cracking, and chloride resistance were experimentally evaluated. As a result of the experiment, with PCM and FRC materials, the connecting joint suffered poor crack dispersion and severe damage by the chloride penetration while with high-ductile material, the connecting joint dispersed the tensile deformation to microcracks stably up to 7.5mm. Furthermore, under the sever conditions, the leaking was prevented and penetration of chloride ions was prevented after the crack occurred.

EFFECT OF LASER IRRADIATION ON DENTIN SURFACE STRUCTURE AND SHEAR BOND STRENGTH OF LIGHT-CURED GLASS IONOMER. (상아질 표면 구조와 광중합형 글라스 아이오노머의 전단강도에 대한 레이저 조사의 효과)

  • Park, Mi-Ryoung;Kim, Jong-Soo;Kim, Yong-Kee
    • Journal of the korean academy of Pediatric Dentistry
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    • v.25 no.1
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    • pp.76-92
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    • 1998
  • The purpose of this study was to evaluate the possible efficacy of Nd-YAG laser as a dentin conditioner by observing the laser irradiation dentin surface under scanning electron micrograph and measuring shear bond strength of restored light-cured glass ionomer mold. Fifty intact premolars were prepared for shear bond strength tests. The teeth were randomly divided into five groups as follows; Group I. no treatment Group II. 10% poly acrylic acid, 20 sec Group III. laser treatment 2 w, 20 Hz, 2 sec Group IV. laser treatment 2 w, 20 Hz, 5 sec Group V. laser treatment 2 w, 20 Hz, 10 sec Samples of each group were restored with light-cured glass ionomer cement after dentin conditioning and then measuring the shear bond strength of each specimen were measured using universal testing machine. Additional ten premolars were prepared for SEM analysis The result from the this study can be summarized as follows. 1. Shear bond strength of polyacrylic acid-treated group (II) was significantly higher than other groups (p<0.05). 2. No statistically significant difference could be found between three laser-treated groups (III, IV, V) in shear bond strength(p>0.05) 3. According to the result of observation under SEM, Polyacrylic acid was shown to have removed the smear layer effectively and opened the dentinal tubules, whereas the laser has produced the irregular surface mainly composed of melted and fused structure. The microcracks found in laser-treated groups increased in number with irradiation time and formed the regular mesh-type in 10 sec-irradiation group. 4. The ultrastructural change of dentin surface created by laser irradiation was found to the improper for bonding of the glass ionomer restorative materials. And the lower shear bond strength of laser irradiated group might have been due to the failure to form the suit able dentin surface for the glass ionomer to penetrated into and form the proper micromechanical retention.

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Evaluation of Mechanical Properties of Glass Substrate Strengthened by Ulatrashort Laser Pulse(1) (극초단파 레이저 강화 유리 기판의 기계적 특성평가(1))

  • Moon Pil Yong;Yoon Duk ki;Lee Kang Taek;Yoo Byung Heon;Cho Sung Hak;Ryu Bong Ki
    • Korean Journal of Materials Research
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    • v.15 no.12
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    • pp.796-801
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    • 2005
  • In order to reduce the weight of glass in architecture, automobile, bottles, displays, a new technique that can strengthen glass was developed using various method. Generally, the strength achieved of glass-ceramics is higher as is 1.he fracture toughness by the formation of a crystalline phase inside glass. In this study, $70SiO_2-20Na_2O-10CaO-10TiO_2$ glasses were irradiated to strengthen by heterogeneous phase using femto-second laser pulse. Laser pulse irradiation of samples was analyzed by DTA, TMA, XRD, nano-indenter and SEM. Samples irradiated by laser had lower value$(3\~4\times10^{-3}Pa)$ of nano indentation which related with mother glass$(8\times10-3Pa)$ than values. Microcracks were occurred around laser irradiation area when femtosecond laser with the repetition rate of 1kHz was used as the light source to induced heterogeneous phase.