• Title/Summary/Keyword: micro-component

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Evaluation of Antimicrobial, Antithrombin, and Antioxidant Activity of Fritillaria thunbergii Miquel (패모(Fritillaria thunbergii Miquel)의 항균,항혈전 및 항산화 활성 평가)

  • Shin, Yong-Kyu;Jang, Han-Su;Kim, Jee-In;Sohn, Ho-Yong
    • Journal of Life Science
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    • v.19 no.9
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    • pp.1245-1250
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    • 2009
  • Beimu (Fritillaria thunbergii Miquel), a bulbous plant of Liliaceae found in Korea, Japan and China, has been used as an antitussive and expectorant agent, and is also useful in alleviating stonsillitis and bronchiolitis. Most researches have been focused on micro-propagation and plant regeneration, component analysis, and dormancy relieving of beimu. Reports regarding the biological activity of beimu, such as anti-Helicobacter pyroli or platelet aggregation inhibition activity, are few and not widely available. In this study, methanol extract and its organic solvent fractions were prepared from Fritillaria thunbergii Miquel and their antimicrobial, antithrombin, and antioxidant activities were evaluated, respectively. The methanol extract contained lots of water-soluble materials (58.98%) and hexane-soluble oils (14.85%). The ethylacetate and butanol fraction at $500{\mu}g$/disc concentration showed strong antibacterial activity against tested bacteria, except Escherichia coli. Antifungal activity was not observed in methanol extract and its fractions. The hexane, ethylacetate and butanol fractions showed strong antithrombin activity at 4.8 mg/ml concentration. Especially, the ethylacetate fraction showed 95.4 sec of thrombin time at a concentration of 1.2 mg/ml, which is comparable to aspirin, a widely used antithrombosis agent. For antioxidation activity, the ethylacetate and butanol fraction showed good 1,1-diphenyl-2-picryl hydrazyl scavenging activity ($IC_{50}$ of $344{\sim}368{\mu}g$/ml). In superoxide dismutase-like activity and reducing power, the fractions showed $20{\sim}25%$ of vitamin C, and $51{\sim}54%$ of butyl hydroxytoluene, respectively.

A Study on Analysis Technique for Chloride Penetration in Cracked Concrete under Combined Deterioration (복합열화에 노출된 균열부 콘크리트 내의 염화물 침투 해석 기법에 대한 연구)

  • Kwon, Seung-Jun;Song, Ha-Won;Byun, Keun-Joo
    • Journal of the Korea Concrete Institute
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    • v.19 no.3
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    • pp.359-366
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    • 2007
  • Recently, analysis researches on durability are focused on chloride attack and carbonation due to increased social and engineering significance. Generally, chloride penetration and carbonation occur simultaneously except for in submerged condition and chloride behavior in carbonated concrete is evaluated to be different from that in normal concrete. Furthermore, if unavoidable crack occurs in concrete, it influences not only single attack but also coupled deterioration more severely. This is a study on analysis technique with system dynamics for chloride penetration in concrete structures exposed to coupled chloride attack and carbonation through chloride diffusion, permeation, and carbonation reaction. For the purpose, a modeling for chloride behavior considering diffusion and permeation is performed through previous models for early-aged concrete such as MCHHM (multi component hydration heat model) and MPSFM (micro pore structure formation). Then model for combined deterioration is developed considering changed characteristics such as pore distribution, saturation and dissociation of bound chloride content under carbonation. The developed model is verified through comparison with previous experimental data. Additionally, simulation for combined deterioration in cracked concrete is carried out through utilizing previously developed models for chloride penetration and carbonation in cracked concrete. From the simulated results, CCTZ (chloride-carbonation transition zone) for evaluating combined deterioration is proposed. It is numerically verified that concrete with slag has better resistance to combined deterioration than concrete with OPC in sound and cracked concrete.

Monitoring of Fracture Occurrence During Carbon Dioxide Injection at the Meruap Oil Reservoir, Indonesia (인도네시아 머루압 유전에 이산화탄소 주입 시 균열대 생성 여부 모니터링)

  • Kim, Dowan;Byun, Joongmoo;Kim, Kiseog;Ahn, Taewoong
    • Geophysics and Geophysical Exploration
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    • v.19 no.1
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    • pp.37-44
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    • 2016
  • $CO_2$-EOR (Carbon Dioxide-Enhanced Oil Recovery), one of the enhanced oil recovery methods, helps to not only enhance the production of oil, but also store carbon dioxide in underground. However, if micro fractures occur when during the injection of $CO_2$, it is difficult to make permanent storage of $CO_2$ in reservoir and can cause contamination of groundwater and soil. Therefore, in this study, we performed microseismic monitoring to investigate the occurrence of fractures during the $CO_2$ injection at the Meruap oil reservoir, Indonesia. To pick the first arrivals of microseismic events, Improved MER (Modified Energy Ratio) method was used. After picking the first arrivals, hodogram analysis was carried out by using the data recorded at three component geophones to calculate the back azimuth of events. Finally, locations of microseismic events were decided by using the results of first arrival picking and hodogram analysis. Estimated locations showed that all microseismic events were occurred at surface and any fracture did not occur around the reservoir. Moreover, by analyzing noise characteristic, we confirmed that almost of picked first arrivals were due to the repetitive mechanical noise.

Evaluation on Weathering Characterization on Rock Types Using Artificial Weathering Test (인공풍화시험을 이용한 암종별 풍화특성 평가)

  • Heo, Yeul;Kang, Changwoo;Kwon, Youngcheul;Bae, Wooseok
    • Journal of the Korean GEO-environmental Society
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    • v.18 no.8
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    • pp.23-32
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    • 2017
  • For exposed slopes, the weathering degree over time has a major effect on the engineering properties of rocks and the slope stability. Rocks are gradually changed by weathering into soil over time, and the resulting physical, chemical and mechanical changes of rocks affect the engineering stability of the slope. However, there are not many ways to objectively evaluate the weathering degree of a slope. In this study, therefore, to investigate the weathering characteristics of rocks, granite, gneiss and shale distributed in the Chungbuk region were sampled by weathering stage and changes in their component minerals and tissues were investigated. Furthermore, artificial weathering was induced using the freezing and thawing test and quantitatively investigated through porosity and absorption rate. In addition, the changes of microcracks due to artificial weathering were evaluated through box fractal dimension ($D_B$). Through mineralogical study the phase change of constituting minerals, the growth of secondary minerals, the development of micro-cracks and the fabric changes due to weathering were observed. The mineralogical, chemical and engineering evaluations of the weathering degree through the experimental results in this study are expected to be useful for analyzing the weathering characteristics and causes by rock type and for proposing a methodology to evaluate the degradation of physical properties comparatively and quantitatively.

Organic Acids, Free Sugars, and Volatile Flavor Compounds by Type of Jerusalem Artichoke (돼지감자의 품종별 유기산, 유리당 및 휘발성 향기성분)

  • Jung, Bok-Mi;Shin, Tai-Sun
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.46 no.7
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    • pp.822-832
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    • 2017
  • This study analyzed contents of organic acids, free sugars, and volatile flavor compounds by type of Jerusalem artichoke (Helianthus tuberosus L.). Organic acids in dried Jerusalem artichoke were mainly composed of malic acid, citric acid, and succinic acid. Sucrose, fructose, and glucose were the major sugar components of dried Jerusalem artichoke. Free sugars were more abundant in the white colored sample than in the purple colored sample. In contrast, purple colored sample contained more organic acids than the white colored one. Volatile compounds in Jerusalem artichoke were investigated using the solid-phase micro-extraction method of gas chromatography/mass spectrometry. A total of 117 volatile compounds were identified in Jerusalem artichoke, and chemical classification was as follows: 5 acids, 13 alcohols, 19 aldehydes, 12 hydrocarbons, 15 ketones, 8 miscellaneous, 27 pyrazines, and 18 terpenes in all samples. Terpene was the most abundant in Jerusalem artichoke, and ${\beta}$-bisabolene was the main component in terpenes. The second most common compound was aldehyde, and hexanal was the highest. Pyrazines were the most abundant in the roasted samples, and 2,5-dimethyl-3-ethylpyrazine was present at the highest level, followed by 2,5-dimethylpyrazine. Compared with purple samples, main compounds contained in white samples were aldehydes and hydrocarbons, whereas the major compounds in purple samples were terpenes and alcohols.

Lightweight Aggregate Bloating Mechanism of Clay/Incinerated Ash/Additive System (점토/소각재/첨가제계 인공 경량골재의 발포기구)

  • Kwon, Yong-Joon;Kim, Yoo-Taek;Lee, Ki-Gang;Kim, Young-Jin;Kang, Seung-Gu;Kim, Jung-Hwan;Park, Myoung-Sik
    • Journal of the Korean Ceramic Society
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    • v.38 no.9
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    • pp.811-816
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    • 2001
  • The influence of the incinerated ash and additives on glass phase formation of lightweight aggregate, weight-lightening, and the bloating mechanism was investigated. Clay was used as base materials and incinerated ash was added from 0 to 30wt%. The additives such as $Na_2CO_3,\;CaCo_3,\;K_2CO_3,\;MgCO_3$, and a little amount of waste oil were added to the mixed body. In clay/incinerated ash/additive system, it turned out that $CaCO_3\;and\;MgCO_3$ were the components for glass phase formation and $Na_2CO_3$ was the component for both glass phase formation and weight-lightening. The small addition of waste oil from 0.5wt% to 3.0wt% affect on the bloating of aggregate. Incinerated ash had a good effect on the glass phase controlling. The most effective condition controlling glass phase and bloating of aggregate was 10wt% incinerated ash, 2wt% waste oil at 1200$^{\circ}$C. The bloating mechanism of lightweight aggregate is as follows; 1) micro-crack formation caused by thermal-shock and gas generation from inside of aggregate, 2) volume expansion by glass phase formation on the aggregate surface and rapid gas bloating inside of aggregate, 3) densification after bloating.

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A Geomorphological Study on the Distribution Areas of Freezing during Summer Season in Korea (한국의 하계 동결현상 분포지에 관한 지형학적 연구)

  • Jeon, Young-Gweon
    • Journal of the Korean association of regional geographers
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    • v.7 no.1
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    • pp.97-106
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    • 2001
  • There are a few interesting areas which show freezing during summer season in Korea, three of them are especially important. They are located at Milyang(Gyungnam province), Uisung and Chungsong(Gyungbook province). They are named Eoleumgol(ice-valley) or Binghyul(ice-cave). The purpose of this study is to clarify geomorphological and geological characteristics about the distribution areas of freezing during summer season in Korea in relation to previous works, which have been studied in hydrological or micro-climatological viewpoints. The main results are summarized as follows. 1) The main geomorphological and geological characteristics in the distribution areas of freezing during summer season (1) Thick debris accumulated slope within deep valley (2) North facing slope (3) The component debris of volcanic rock such as andesite or rhyolite 2) The ice-cave as a system that give rise to freezing phenomenon in summer season is closely related to talus slope. The ice-cave has thick accumulated debris and lots of vacant spaces within the rock deposits, some of vacant spaces are very big and connected with underground water system. 3) A partly freezing within underground water system is required freezing phenomenon in summer season. Judging from this point of view, two ideas are suggested; one is the evaporation theory, another is that the frozen condition in winter remains untill late summer.

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Material Characteristic of Slags and Iron Bloom Produced by Smelting Process Using Sand Iron (사철 제련을 통해 생산된 슬래그와 괴련철의 재료과학적 특성 비교)

  • Cho, Sung Mo;Cho, Hyun Kyung;Kwon, In Cheol;Cho, Nam Chul
    • Journal of Conservation Science
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    • v.34 no.1
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    • pp.39-50
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    • 2018
  • This study replicated traditional smelting methods to produce iron blooms from sand iron. The metallurgical properties of the slag and the iron blooms were analyzed. The sand iron materials used in the smelting experiments, which were based on ancient documents, were collected from Gyeong-Ju and Pohang. Analysis by WD-XRF and XRD showed that Gyeong-Ju's sand iron contains a high-titanium, with magnetite, and Pohang's sand iron contains a low-titanium, which magnetite and ilmenite were mixed. Analysis of the slag with XRD, and the micro-structure with metal microscopes and SEM-EDS, confirmed that the major compounds in the slag of the Gyeong-Ju's sand iron were fayalite and $w\ddot{u}stite$, and those in the slag of the Pohang's sand iron were titanomagnetite and fayalite. The differences in the main constituents were confirmed according to the Ti quantity. Finally, we observed the microstructures of the iron blooms. In the case of the iron bloom produced from Gyeong-Ju's sand iron, the outside was found to be dominantly a pearlite of eutectoid steel, while the inside was a hypo-eutectoid steel where ferrite and pearlite were mixed together. While, the major component of the iron bloom produced from Pohang's sand iron was ferrite, which is almost like pure iron. However, there were many impurities inside the iron blooms. Therefore, this experiment confirmed that making ironware required a process that involved removing internal impurities, refining, and welding. It will be an important data to identify the characteristics of iron by-products and the site through traditional iron-making experiments under various conditions.

Strength Characteristics of Sedimentary Rock in Daegu-Gyungbuk Area Followed by Saturation and Crack Initiation (대구경북지역 퇴적암의 포화 및 균열 유발에 따른 강도 특성)

  • Park, Sung-Sik;Kim, Seong-Heon;Bae, Do-Han
    • Journal of the Korean Geotechnical Society
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    • v.34 no.12
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    • pp.29-42
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    • 2018
  • Shale and mudstone in Daegu-Gyungbuk area have low strength and resistance to weathering compared to other rocks. Therefore, it is necessary to evaluate their strength depending on the degree of saturation and crack development. In this study, shales and mudstones were collected from several construction sites in Daegu-Gyungbuk area. Their basic material properties such as porosity, SEM, chemical component, and durability were tested. A porosity (absorptivity) of mudstone was 31% (25%), which was 6 (8) times higher than that of shale. Some mudstone was easily disintegrated with water and it consisted of highly-active clay mineral such as smectite type. These rocks were prepared by small cube specimens for unconfined compression test. An unconfined compressive strength of dry rock was compared with saturated one. Microwave oven was operated step by step to stimulate void water within a saturated rock, which resulted into high temperature and micro crack initiation within rocks. A strength of microwaved rocks was compared with operation time and crack initiation. As a result, the average unconfined compressive strength of dry and saturated shale was 62 and 33 MPa, respectively. The strength of mudstone for each condition was 11 and 4 MPa. When a rock became saturated, its strength decreased by 47% and 64% for shale and mudstone at average. In addition to saturation, a rock was in the microwave for 15 secs, its strength decreased into 49% for shale and 52% for mudstone. When a microwave oven operated up to 20 sec, a rock was crushed into several pieces and its temperature was approximately 200 degrees.

A Study of Scientific Research on the Ancient Roof Tiles in Korea Related to Cheonwangsa Temple of Hanam City (고대기와의 자연과학적 분석 연구 경기도 하남시 천왕사지출토기와를 중심으로)

  • Hong, Jong-Ouk
    • Korean Journal of Heritage: History & Science
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    • v.37
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    • pp.349-369
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    • 2004
  • Today, in the cultural properties research, there are several methods for knowing the culture of the past through a lot of information that remains and relics contain. Especially, statistical method like presumption of producing center were introduced from computer development at the early 20th century. This study showed the characteristic about firing historic sites presumed as a tile-kiln in the remains of Cheonwang temple sites, Hanam, Gyeonggi province. Also, I used nature scientific methods for correlation between tiles excavated at historic sites and circumference building and obtained there results as follows. First, soft tile parts showed similar water suction ratio(over 10%) like another tiles, except hard tile parts. Second, identification about mineral crystallization in a sample showing low water suction ratio confirmed a result that Mullite, Tridymite, Cristobalite as high temperature crystal form were presented. I know that firing temperature was higher than the other tile parts from this result. Third, statistical analysis from micro-component resulted that tiles excavated at firing historic sites and Cheonwang temple sites were closely connected. As the results, I knew that the tiles got a supply after the establishment of tile-kiln, not at a long distance at the period of Cheonwang temple construction.