• Title/Summary/Keyword: methomyl oxime

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Residue analysis of insecticide thiodicarb in sweet persimmon and its safety evaluation (살충제 thiodicarb의 단감 중 잔류분석 및 안전성 평가)

  • Lo, Seog-Cho;Hwang, Cheol-Hwan;Kim, Min-Soo;Ma, Sang-Yong;Han, Seong-Soo
    • The Korean Journal of Pesticide Science
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    • v.8 no.3
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    • pp.184-188
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    • 2004
  • The residue analysis of the insecticide thiodicarb in sweet persimmon was analyzed with a gas chromatograph equipped with nitrogen phosphorus detector(NPD) to evaluate efficacy of analysis method and safety of thiodicarb in persimmon. Minimum detectable amount of methomyl oxime, hydrolysate of thiodicarb, was 0.2 ng and detection limit of thiodicarb was 0.05 ppm. The mean recoveries evaluated from untreated samples spiked at 0.5 ppm and 2.5 ppm were $93.9{\pm}3.9$ and $92.8{\pm}2.0%$, respectively. When thiodicarb was sprayed onto the sweet persimmon two times until 40 and 30 days before harvest, three times until 40, 30 and 21 days before harvest, and four times until 40, 30, 21 and 14 days before harvesting, the mean residual amount in sweet persimmon were $1.50{\pm}0.04$, $1.86{\pm}0.04$ and $2.11{\pm}0.12$ ppm, respectively. It would be safe when thiodicarb 40% WP is treated four times 14 days before harvesting to control fruit moth in sweet persimmon.