• Title/Summary/Keyword: metallurgy

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Consolidation of Iron Nanopowder by Nanopowder-Agglomerate Sintering at Elevated Temperature

  • Lee, Jai-Sung;Yun, Joon-Chul;Choi, Joon-Phil;Lee, Geon-Yong
    • Journal of Powder Materials
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    • v.20 no.1
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    • pp.1-6
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    • 2013
  • The key concept of nanopowder agglomerate sintering (NAS) is to enhance material transport by controlling the powder interface volume of nanopowder agglomerates. Using this concept, we developed a new approach to full density processing for the fabrication of pure iron nanomaterial using Fe nanopowder agglomerates from oxide powders. Full density processing of pure iron nanopowders was introduced in which the powder interface volume is manipulated in order to control the densification process and its corresponding microstructures. The full density sintering behavior of Fe nanopowders optimally size-controlled by wet-milling treatment was discussed in terms of densification process and microstructures.

Carbon-nanofiber Reinforced Copper Composites Prepared by Powder Metallurgy for Thermal Management of Electronic Devices

  • Weidmueller, H.;Weissgaerber, T.;Hutsch, T.;Huenert, R.;Schmitt, T.;Mauthner, K.;Schulz-Harder, J.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.844-845
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    • 2006
  • For microelectronic circuits, the main type of failure is thermal fatigue. Therefore, the search for matched coefficients of thermal expansion (CTE) of packaging materials in combination with a high thermal conductivity is the main task for developments of heat sink materials electronics, and good mechanical properties are also required. The aim of this work is to develop copper matrix composites reinforced with carbon nanofibers to meet these requirements. In this paper, a technology for obtaining a homogeneous mixture of copper and nanofibers will be presented and the microstructure and properties of consolidated samples will be discussed.

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Fabrication of Pure Refractory Metals by Resistance Sintering under Ultra High Pressure

  • Zhou, Zhang-Jian;Du, Juan;Song, Shu-Xiang;Ge, Chang-Chun
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.1323-1324
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    • 2006
  • Refractory materials, such as W and Mo, are very useful elements for use in high-temperature applications. But it is not easy to fabricat pure W and Mo with very high density and retaining very fine grain size because of their high melting point. In this paper, a newly developed method named as resistance sintering under ultra high pressure was use to fabricate pure fine-grained W and Mo. The microstructure was analysis by SEM. The sintering mechanism is primary analyzed. Basic physical property of these sintered pure W and Mo, such as hardness, bend strength, are tested.

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Densification Behavior and Microstructural Development of Nano-agglomerate Powder during Singering

  • Kang, Yun-Sung;Cha, Berm-Ha;Kang, Hyun-Goo;Lee, Jai-Sung
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.282-283
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    • 2006
  • Densification behavior of nano-agglomerate powder during pressureless sintering of Fe-Ni nanopowder was investigated in terms of diffusion kinetics and microstructural development. To understand the role of agglomerate boundary for sintering process, densification kinetics of Fe-Ni nano-agglomerate powder with different agglomerate size was investigated. It was found that activation energy for densification was lower in the small-sized agglomerate powder. The increase in the volume fraction of inter-agglomerate boundary acting as high diffusion path might be responsible for the enhanced diffusion process.

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Capabilities of Two Chromium Powder Metallurgy Steels for High Performance Applications at Conventional Sintering Temperatures

  • Kinga, Patrick;Lindsley, Bruce
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.134-135
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    • 2006
  • Ancorsteel 4300, a high performance Cr-Si-Ni-Mo steel, was unveiled two years ago as the first in a series of powder metallurgy alloys that will simulate wrought steel compositions. Advantages of this alloy include good compressibility, high hardenability, and excellent dimensional stability. More important, however, is that this alloy has the ability to be effectively sintered at $1120^{\circ}C$ and maintain oxygen contents below 500 ppm. This unique blend of performance and processing capabilities provides static and dynamic properties that exceed those of conventional powder metallurgy alloys and approach wrought gearing materials. A second Cr-Si-Ni-Mo alloy has now been developed that offers complimentary performance levels at a lower Mo content. This manuscript reviews properties of the two chromium steels with comparisons to traditional sinter-hardened and heat-treated powder metallurgy alloys.

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Micro-porous Nickel Produced by Powder Metallurgy

  • Yamada, Y.;Li, Y.C.;Banno, T.;Xie, Z.K.;Wen, C.E.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.602-603
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    • 2006
  • Micro-porous nickel (Ni) with an open cell structure was fabricated by powder metallurgy. The pore size of the micro-porous Ni approximated $30{\mu}m$ and $150{\mu}m$. For comparison, porous Ni with a macro-porous structure were also prepared by both powder metallurgy (pore size $800{\mu}m$) and the traditional chemical vapour deposition method (pore size $1300{\mu}m$). The mechanical properties of the micro-and macro-porous Ni samples were evaluated using compressive tests. Results indicate that the micro-porous Ni samples exhibited significantly enhanced mechanical properties, compared to those of the macro-porous Ni samples.

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Sintering Behavior of the Net-shaped Fe-8wt%Ni Nanoalloy Powder and Related Mechanical Property

  • Cha, Berm-Ha;Kang, Yun-Sung;Lee, Sung-Ho;Lee, Jai-Sung
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.501-502
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    • 2006
  • The present investigation has been performed on full densification behavior and mechanical property of the powder injection molded Fe-8wt%Ni nanoalloy powder. The net shaping process of the nanopowder was conducted by powder injection molding (PIM) process. The key-process for fabricating fully densified net-shaped nanopowder by pressureless sintering is an optimal control of agglomerate size of nanopowder. Enhanced mechanical property of PIMed Fe-Ni nanopowder is explained by grain refinement and microstructural uniformity.

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Preparation and Characterization of $Ag/TiO_{2-x}N_x$ Nanoparticles

  • Liu, Z.Q.;Li, Z.H.;Zhou, Y.P.;Ge, C.C.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.436-437
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    • 2006
  • The $Ag/TiO_{2-x}N_x$ nanoparticles were synthesized by photochemical deposition in a $TiO_{2-X}N_X$ suspension system. The prepared products were characterized by means of XRD, Uv-vis and photoluminescence spectra (PL). Its photocatalytic activity was investigated by the decomposition of methylene blue (MB) solution under illumination of visible and ultraviolet light, respectively. Compared to $TiO_{2-x}N_x$, the photocatalytic activity of the as-prepared $Ag/TiO_{2-x}N_x$ is obviously enhanced due to the decreasing recombination of a photoexcitated electron-hole pairs. The Mechanism in which photocatalytic activity is enhanced has been discussed in detail.

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Microstructure, Properties and Heat Treatment of Steel Bonded TiC Cermets

  • Farid, Akhtar;Guo, Shiju;Shah, Jawad Ali;Feng, Peizhong
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.618-619
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    • 2006
  • The binder phase for TiC reinforced steel matrix composite was added in the form of elemental powders and master alloy powders. The microstructures, binder phase variation with TiC content and mechanical properties were evaluated. The addition of a type of binder phase largely effects the microstructure and mechanical properties. The binder phase variation from starting composition was observed with increase in wt% TiC content and this variation was higher when the master alloy powders were used as a binder. The response to heat treatment was decreased with an increase in TiC content due to the shift of binder phase from the starting composition.

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