• Title/Summary/Keyword: maximum absorption

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Effect of moisture on interlaminar fracture toughness of CFRP composites (CFRP 복합재료의 층간파괴인성치에 미치는 수분의 영향)

  • 김형진;김종훈;고성위;김엄기
    • Journal of Ocean Engineering and Technology
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    • v.10 no.4
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    • pp.75-83
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    • 1996
  • Polymeric composites can be subjected to a wide variety of environmemtal conditions in practical use. One of most important conditions to be considered in the stuctural design using such materials is the miisture envirnment. Thus the moisture effect on interlaminar fracture toughness $G_IC$ and $G_IIC$ of CFRP(carbon fiber reinforced plastic) composed of carbon fibers and epoxy resin is studied in this paper. Specimens were first processed in 25, 50, $80^{\circ}C$ flesh water and $25^{\circ}C$ sea water for various periods of time. After that, the water absorption and fracture toughness tests were performed under laboratory atmosphere. As result, the specimen processed in $80^{\circ}C$ flesh water indicates the highest misture absorbing capability, the second in $50^{\circ}C$ flesh water, the third in $25^{\circ}C$ sea water, and the specimen in $25^{\circ}C$ flesh water does the lowest. The interlaminar fracture toughness $G_IC$ increases, approaches to the maximum, and decreases as the immersion time increases. In case of interlaminar $G_IIC$, the value of the specimen processed in $80^{\circ}C$ flesh water turns out to be higher than others. In addition, the scanning electron micrographs(SEM) of fracture surfaces were also examined in order to explain the mechanism of fracture.

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Quality Characteristics of Semi-Dry Noodles Prepared with Various Dry Rice Flours (건식 쌀가루 첨가 반건면의 품질특성)

  • Park, Bock-Hee;Koh, Kyeong-Mi;Jeon, Eun-Raye
    • Human Ecology Research
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    • v.58 no.1
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    • pp.121-130
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    • 2020
  • This study evaluated the quality characteristics of semi-dried noodles prepared with various dry rice flours (0, 25, 50, 75, and 100%) in order to develop the most preferred noodle recipe and to increase rice consumption. Amylography measured the viscosity of composite dry rice flour-wheat flour and indicated that the gelatinization point and maximum viscosity decreased as the level of dry rice flour increased. Both L and a values for cooked noodle significantly increased as the dry rice flour increased; however the L value decreased for uncooked of noodles. Weight, volume and water absorption of cooked semi-dried noodles significantly decreased as the dry rice flour increased; however the turbidity of soup increased. Texture properties such as hardness, springiness, cohesiveness, and adhesiveness decreased as the level of dry rice flour increased. As the amount of rice flour added increased, large particles of gluten were reduced while smaller particles of starch increased by scanning electron microscopy (SEM). The color, taste, and overall preference of 75% noodles were the highest in the sensory characteristics. The results, showed that the addition of dry rice flour positively affects the overall sensory characteristics of semi-dried noodle with 75% representing the optimal level for addition.

Natural Dyeing Properties and Antibacterial Activity of Nylon Fabric Dyed with Cochineal (코치닐에 의한 나일론직물의 천연 염색성과 항균성)

  • Bae, Jung-Sook;Huh, Man-Woo
    • Fashion & Textile Research Journal
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    • v.8 no.6
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    • pp.702-708
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    • 2006
  • The purpose of this study was to investigate the dyeing-property and antibacterial activity on nylon fabric dyed with cochineal at variable dyeing conditions. Al, Cr, Fe, Cu and Sn were used as mordants and adsorption was compared with different mordanting methods. The maximum UV-visible absorption band of cochineal extract was 495 nm. The dyeability on nylon fabric was good because of having a amine group. The optimum dyeing conditions of nylon fabrics are dyeing concentration 1.5%(o.w.s), dyeing temperature $60^{\circ}C$, pH 3 and dyeing time 30 minutes. The pre-mordanting method is preferred for Al and Cr, and the post-mordanting one is preferred for Cu, Sn and Fe to achieve better dyeing. The optimum mordanting conditions of wool fabrics dyed with cochineal are mordanting concentration of 0.5%(o.w.s), mordanting temperature $60^{\circ}C$, and dyeing time 30 minutes. Nylon fabrics dyed with cochineal show a little antibacterial activity, but it was increased by Sn mordanting. MIC test results in antibacterial activities revealed that the antibacterial activity of Cu was the highest among mordants, but Sn mordant was the most effective in antibacterial activities after mordanting treatment of nylon fabric. The fastness properties of dyed nylon fabric showd a little worse or a similar level and there was no significant difference between a mordanted and non-mordanted fabric.

Tests on Failure of Steel Angles due to Very Low-Cycle Fatigue of Loading (극저사이클 재하하에서 앵글 강부재의 파괴실험)

  • Park, Yeon Soo;Kim, Sung Chil;Lim, Jung Soon
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.12 no.4_1
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    • pp.23-32
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    • 1992
  • The objective of this study is to identify the quantitative relationships among the important physical factors associated with failure of steel members under strong seismic excitations through very low-cycle fatigue tests. Very low-cycle fatigue is meant to be structural fatigue causing cracks and rupture in about 5~30 cycle ranges. The angle specimen was subjected to repeated axial Ioad after undergoing inelastic buckling. The test results reveal that the energy absorption capacities vary heavily with the history of loading and the failure mode. The maximum values of residual local strain at the initiation of a visible crack due to the very low-cycle fatigue were of the order of 25~40%, regardless of loading patterns, deflection modes, and width-to-thickness ratios.

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Purification and Characterization of Catalase-2 from Deinococcus radiophilus

  • Oh, Kyung-A;Lee, Young-Nam
    • BMB Reports
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    • v.31 no.2
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    • pp.144-148
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    • 1998
  • A bifunctional catalase-peroxidase, designated catalase-2, of a UV resistant Deinococcus radiophilus was purified to electrophoretic homogeneity by both chromatographic and electrophoretic methods. Its molecular weight was 310 kDa and composed of a tetramer of 80 kDa subunits. The catalase-2 exerted its optimal activity at $30^{\circ}C$ and around pH 9. Its $K_m$ value for $H_{2}0_{2} $ was about 10 mM. It showed the typical ferric heme spectrum with maximum absorption at 403 nm which shifted to 419 nm in the presence of cyanide. The ratio of A40i' A2S0 was 0.48. Fifty percent inhibition of the enzyme activity was observed at $4.6{\times}10^{-6}$, $7.7{\times}10^{-6}$, and $3.0{\times}10^{-6}$ M of NaCN, $NaN_3$, and $NH_{2}OH$, respectively. The enzyme was thermostable and not sensitive to 3-amino-1,2,4-triazole. Treatment of the enzyme with ethanol-chloroform caused a partial loss (30%) of its activity. The catalase-2 was distinct from the Deinococcal bifunctional catalase-3 in a number of properties, particularly in its molecular structure and substrate affinity.

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Chemical Modification of Residue of Lysine, Tryptophan, and Cysteine in Spinach Glycolate Oxidase

  • Lee, Duk-Gun;Cho, Nam-Jeong;Choi, Jung-Do
    • BMB Reports
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    • v.29 no.4
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    • pp.321-326
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    • 1996
  • Spinach glycolate oxidase was subjected to a series of chemical modifications aimed at identifying amino acid residues essential for catalytic activity. The oxidase was reversibly inactivated by treatment with pyridoxal 5'-phosphate (PLP). The inactivation by PLP was accompanied by the appearance of an absorption peak of around 430 nm, which was shifted to 325 nm upon reduction with $NaBH_4$. After reduction, the PLP-treated oxidase showed a fluorescence spectrum with a maximum of around 395 nm by exciting at 325 nm. The substrate-competitive inhibitors oxalate and oxaloacetate provided protection against inactivation of the oxidase by PLP. These results suggest that PLP inactivates the enzyme by fonning a Schiff base with lysyl residue(s) at an active site of the oxidase. The enzyme was also inactivated by tryptophan-specific reagent N-bromosuccinimide (NBS). However, competitive inhibitors oxalate and oxaloacetate could not protect the oxidase significantly against inactivation of the enzyme by NBS. The results implicate that the inactivation of the oxidase by NBS is not directly related to modification of the tryptophanyl residue at an active site of the enzyme. Treatments of the oxidase with cysteine-specific reagents iodoacetate, silver nitrate, and 5,5'-dithiobis-2-nitrobenzoic acid did not affect significantly the activity of the enzyme.

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Varietal Difference of Resistance to Ozone Injury in Rice Plant (벼 품종별 오존 피해 저항성 차이)

  • 손재근;이상철
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.42 no.3
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    • pp.338-343
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    • 1997
  • The response of seventy-five rice cultivars to ozone (O$_3$) were tested in the open-top chamber with ozone producing and monitoring system to determine the varietal difference of resistance to $O_3$ stress. Ozone was produced by electrostatic discharge in oxygen and was monitored by UV absorption ozone analyzer. Difference in response of rice to ozone was more clearly appeared on rice plants treated for 2 to 4 hours at 0.3 ppm concentration of $O_3$. Varietal resistance of rice to ozone was more distinctly classified at 21- to 35-day seedlings compared with 14-day rice plants. Most of indica and Tongil(indica$\times$japonica) type rice cultivars were more resistant than that of japonica cultivars based on the leaf injury to $O_3$. Eight Korean cultivars belong to japonica groups showed highly resistant reaction to $O_3$. Ozone exposure during booting stage caused lower grain fertility than exposures during seedling, maximum tillering and heading stages of rice.

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Antioxidant Activity of Amino Acid-Xylose Browning Reaction Products 2. Isolation of Antioxigenic Substrates from Browning Reaction Products by TLC and Dialysis (Amino 산-Xylose 갈변반응 물질의 항산화성 2. TLC와 투석을 이용한 항산화성 갈변물질의 분리)

  • YOU Byeong-Jin;LEE Kang-HO;LEE Jong-Ho
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.19 no.3
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    • pp.212-218
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    • 1986
  • In order to isolate antioxigenic substrates, the browning reaction products of xylose and various amino acids were analysed by TLC and dialysis. Rf values of browning reaction products of xylose and hydrophobic amino acids separated on silica gel TLC plate were shown in the range of 0.38 to 0.56 and that of basic amino acids was around 0.2. Browning reaction products made from xylose and Trp were separated on TLC into four bands with Rf values of 0.25, 0.55, 0.81 and 0.91 respectively. Among these the bands with Rf values of 0.25 and 0.55 appeared having strong antioxidant activity. The band of Rf 0.55 which showed the highest activity was positive to Prochazka reagent and had an absorption maximum at 275 nm. In dialysis of the xylose-Trp browning reaction products, the undialysed fraction (inner solution) was repsponsible to the antioxidant activity, which was separated into two bands with Rf values of 0.25 and 0.55 on TLC. The inner fractions of the browning products of xylose and His or Arg were also apparent in antioxdant activity.

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Natural Dyeing of Cotton Fabrics with Rumex crispus L. Root (소루쟁이뿌리를 이용한 면직물 천연염색)

  • Han, Mi-Ran;Lee, Jeong-Sook
    • Journal of the Korean Society of Clothing and Textiles
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    • v.33 no.2
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    • pp.222-229
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    • 2009
  • The natural dyeing of cotton fabrics with Rumex crispus L. root extract was investigated. The dyeability of Rumex crispus L. root extract was evaluated with conditions of concentration, temperature, time, repeat-numbers, pH, mordants variables, methods of mordanting, color fastness and antibacterial activity, etc. The maximum V-visible spectrum possessed absorption band of Rumex crispus L. extract appeared at 274nm and 336nm. The amount of dyes extracted was increased with extracting concentration, temperature and time. The K/S value increased with increasing dyeing concentration and repeat-numbers. The K/S value increased with increasing dyeing temperature and time, the exhaustion was saturated in $90^{\circ}C\;and\;80min$, respectively. Surface colors of fabrics dyed with pH 3, 7, 11 extract were RP-R-YR-Y range. The light fastness and washing fastness showed good results in Fe-mordanted. The dry leaning fastness appeared more than 4 grade. Rubbing fastness was better in dry methods han that in wet methods. In the result of antibacterial activity, the decrease rate was 9.9% to Staphylococcus aureus with the dyed fabric of cotton.

Natural Dyeing of Sangju Silk with Mulberry Extract Solution (오디 추출액을 이용한 상주실크의 천연염색)

  • Lee, Kwang-Woo;Lee, Jun-Hee;Eum, Su-Jang;Bae, Eun-Mi;Kim, Tae-Yeon;Yoon, Seok-Han
    • Textile Coloration and Finishing
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    • v.22 no.3
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    • pp.207-213
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    • 2010
  • Natural dyeing of Sangju silk for graveclothes with mulberry extract solution was studied. The anthocyanidin dye in the extracted mulberry solution was markedly influenced by pH condition, which resulted in the changed maximum light absorption from a $\lambda$max of 525nm in acidic condition to 380nm in alkaline condition possibly due to the irreversible transformation of anthocyanidin to cyanidin form of the dye. The color fastness properties to both light and washing were good when the fabrics were dyed at $80^{\circ}C$ with the mulberry-extracted solution upto twice extraction.