• Korea-Australia Rheology Journal
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• v.15 no.2
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• pp.63-73
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• 2003

An experimental technique was developed to determine the strain-rate in a tensile specimen. Then one can calculate the transient isothermal elongational viscosity. Both shear and elongational viscosities were measured to study the effect of shear and elongational fields on the flow properties. The comparison between these viscosities shows that the onset of rapid viscosity growth as crystallization solidification proceeds occurs at about the same value of time at very small deformation rates (0.0028 and 0.0047 $s^{-1}$). The comparison of these measured viscosities as functions of shear and elongational Hencky strains also reveals that the onset of rapid viscosity growths starts at critical Hencky strain values. The behaviour of steady shear viscosity as function of temperature sweep was also explored at three different low shear rates. Finally, the influence of changing oscillatory frequencies and strain rates was also investigated.

• Proceedings of the KSME Conference
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• 2002.08a
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• pp.317-320
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• 2002

The effect of vibration on the viscosity of a shear-thinning fluid was investigated with a newly designed pressure-scanning capillary viscometer. The viscometer was designed to measure non-Newtonian viscosity continuously over a range of shear rates at a time. Low frequency vibration was applied perpendicularly to the direction of the flow. The effect of the transversal vibration was investigated for both Newtonian fluids and non-Newtonian fluids. The experimental results showed that the vibration had no effect on the viscosity of the Newtonian fluids. However, the vibration caused a significant reduction of the shear-thinning fluid viscosity. The viscosity reduction was strongly dependent on both vibration frequency and shear rate. In addition, the viscosity reduction was affected by the amplitude of vibration, and, the bigger amplitude applied, the more viscosity reduction occurred.

• Journal of Mechanical Science and Technology
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• v.16 no.2
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• pp.255-261
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• 2002

A newly designed mass-detecting capillary viscometer uses a novel concept to continuously measure non-Newtonian fluids viscosity over a range of shear rates. A single measurement of liquid-mass variation with time replaces the now rate and pressure drop measurements that are usually required by capillary tube viscometers. Using a load cell and a capillary, we measured change in the mass flow rate through a capillary tube with respect to the time, m(t), from which viscosity and shear rate were mathematically calculated. For aqueous polymer solutions, excellent agreement was found between the results from the mass-detecting capillary viscometer and those from a commercially available rotating viscometer. This new method overcomes the drawbacks of conventional capillary viscometers meassuring non-Newtonian fluid viscosity. First, the mass-detecting capillary viscometer can accurately and consistently measure non -Newtonian viscosity over a wide range of shear rate extending as low as 1 s$\^$-1/. Second, this design provides simplicity (i. e., ease of operation, no moving parts), and low cost.

• International Journal of Industrial Entomology and Biomaterials
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• v.22 no.1
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• pp.5-10
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• 2011

The effect of sample handling condition on the rheological measurement of regenerated silk fibroin formic acid solution using parallel plate geometry was investigated. In case of loading method, the loading by pouring sample solution resulted in the best reproducibility of rheological measurement. Loading with spoon showed a high variance of viscosity value at low shear rate region ($0.01{\sim}1sec^{-1}$) while loading with syringe exhibited a low reproducibility of viscosity at high shear region ($1{\sim}100sec^{-1}$) with a disappearance of shear thinning phenomenon. It was revealed that the sample loading with small extra amount lead to the most reproducible result. The sample loading with the exact amount for the measuring plate resulted in a lack of reproducibility of high shear viscosity, while the loading with large extra volume produced a limited consistency of low shear viscosity. It was turned out that 3 min. of waiting time before measurement was the optimum condition for reliable result. When the waiting time was less than 1 min., the low shear viscosity was obtained with a lack of consistency. On the other hand, the sample solution started drying when the waiting time increased up to 5 min.

• International Journal of Vascular Biomedical Engineering
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• v.4 no.2
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• pp.7-12
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• 2006

The present study investigated the effects of the osmotic environment on the rheological properties of erythrocytes and their suspensions. In an iso-osmotic medium, erythrocytes forming a biconcave discocyte under resting conditions, exhibited high deformability. In a low-osmotic medium, the deformability of erythrocytes, which swelled and exhibited a spherical shape, significantly decreased at a high shear stress and the high-shear viscosity of the cell suspension was slightly higher than that of normal blood. Hyper-osmotic stress, however, which caused to form echinocytes, decreased cell deformability but exhibited smaller viscosity in low shear rates than iso-osmotic blood viscosity. These results showed a close relation with the aggregability measurements, in that hypertonic blood showed lower aggregability than the hypotonic and isotonic RBC suspensions. These findings indicate that the physicochemical environment has a strong influence on the rheological properties of the erythrocyte and its suspensions.

• Journal of the Korean Wood Science and Technology
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• v.24 no.4
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• pp.82-86
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• 1996

This study was performed to elucidate the effect of degree of substitution and degree of polymerization of CMC on the rheological characteristics of coating color which is consisted of calcium carbonate as pigment. The results were as follows: 1. It appeared that DP of CMC rather DS has an effect on the low shear viscosity of coating color. 2. According as shear rate increased, the effect of DP and DS on high shear viscosity of coating color decreased. 3. According to increasing DS and DP, the water retention of coating color increased.

• Korea-Australia Rheology Journal
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• v.19 no.2
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• pp.75-80
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• 2007

The slotted plate technique has previously been shown to be a successful method for directly measuring the static yield stress of suspensions. In this study, we further establish the usefulness of the slotted plate device as a rheometer especially at low shear rates, taking advantage of the extremely low speeds of the slotted plate technique. Newtonian fluids, a shear thinning fluid, and yield stress fluids were tested using the slotted plate device and the results were compared with those from a commercial rheometer using different standard flow geometries. The relationship between the stress on the plate and the viscosity for the slotted plate device obtained by dimensional analysis (drag) predicts a linear relationship between the force at the plate and the plate speed, consistent with the experimental data. The slotted plate device can measure viscosities at very low shear rates. The apparent viscosity - shear-rate data obtained from the slotted plate device are complementary to those obtained using a commercial rheometer. That is : the slotted plate can measure viscosity in the shear rate range $10^{-7}<\dot{\gamma}<10^{-3}\;s^{-1}$, while the commercial rheometer measures viscosity at shear rates higher than $10^{-3}\;s^{-1}$.

• Proceedings of the KSME Conference
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• 2004.04a
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• pp.1678-1681
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• 2004

The light-transmission technique has been applied to a slit rheometer for measuring red blood cell aggregation as well as blood viscosity over a range of shear rates. For measurement of blood viscosity and aggregation, instantaneous pressure and transmit-light intensity are measured with time. Using a precision pressure measurement, one can determine the shear stress and shear rate. In addition, a transmitted light through a blood sample indicates degree of RBC aggregation. With abruptly flowing with high shear rate, RBCs rapidly disaggregate and the intensity of the transmitted light becomes low. When continuously flowing with decreasing shear rate, RBCs tend to re-aggregate and the corresponding transmit-intensity gradually increases with time. The light intensity as a degree of RBC aggregation is plotted against shear rate and compared with blood viscosity. The advantages of this design are dual measurement at a time, simplicity, i.e., ease of operation and no moving parts, low cost, short operating time, and the disposable kit which is contacted with blood sample.

• Tribology and Lubricants
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• v.30 no.3
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• pp.189-198
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• 2014

This paper presents the results of an experimental investigation of the correlation between the lubrication characteristics of an engine and its fuel economy. Improving the lubrication characteristics of the engine oil is one of the most efficient ways to improve a car's fuel economy. The methods to accomplish this include lowering the viscosity, adding a friction modifier and optimizing the shear stability index of a viscosity index improver. In addition, it is necessary to use different methods to reduce the friction to individual lubrication areas, because different lubrication regimes are used for different engine parts. The experimental investigation in this study is based on design of experiments ; this paper presents the results of a modified Sequence VID test, which is an ASTM standard test used to measure the effects of automotive engine oils on the fuel economy of passenger cars. The results demonstrate the effects of the following lubrication factors on the fuel economy : the low temperature cranking viscosity, high-temperature high shear (HTHS) viscosity, friction modifier, polymer type and shear stability index of the viscosity index improver. Moreover, this study involves an analysis of variance based on design of experiments. The test results show that the HTHS viscosity, friction modifier and shear stability index of the viscosity index improver are more effective than the other factors. Therefore, lowering the viscosity, adding a friction modifier and optimizing the shear stability index of a viscosity index improver should be considered to improve fuel economy.

• Journal of ILASS-Korea
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• v.14 no.3
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• pp.131-138
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• 2009

In the present study, spread-recoil behavior of a drop of shear-thinning liquid (xanthan solution) on a dry wall (polished stainless-steel plate) was examined and compared with that of Newtonian liquid (glycerin solution). Nine different kinds of xanthan and glycerin solutions were tested, including three pairs of xanthan and glycerin solutions, each having the same viscosity in low shear rate region ($10^{-2}-10^0\;l/s$). The drop behavior was visualized and recorded using a CCD camera. The maximum diameter and the spreading velocity of the xanthan drops turned out to be significantly larger and the time to reach their final shape was much shorter compared to the cases with the glycerin solutions, due to the smaller viscous dissipation resulted from lower viscosity in the higher shear rate region (>$10^0\;l/s$). As a result, the maximum diameters were measured to be larger than the predicted values based on the model proposed for Newtonian liquids, and the deviation was more pronounced with the solution with the larger viscosity variation. Consequently, viscosity variation with the shear rate was found to be a dominant factor governing the spread-recoil behavior of shear-thinning drops.